PL10656B1 - A method of treating salt in order to use it as a fertilizer. - Google Patents

A method of treating salt in order to use it as a fertilizer. Download PDF

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Publication number
PL10656B1
PL10656B1 PL10656A PL1065628A PL10656B1 PL 10656 B1 PL10656 B1 PL 10656B1 PL 10656 A PL10656 A PL 10656A PL 1065628 A PL1065628 A PL 1065628A PL 10656 B1 PL10656 B1 PL 10656B1
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PL
Poland
Prior art keywords
salts
fertilizer
order
treating salt
gases
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Application number
PL10656A
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Polish (pl)
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Publication date
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Publication of PL10656B1 publication Critical patent/PL10656B1/en

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Wynalazek niniejszy dotyczy sposobu obróbki soli w celu ich zastosowania jako nawozów i dotyczy szczególniej tych soli, które dzieki sposobowi ich otrzymywania zawieraja pewna ilosc lotnych cial a- monjaikalnych, nie dajacych sie calkowicie usunac przez wymywanie, jak np. wegla¬ ny anionu, siarczek amonu i L p. Ma to miejsce np. przy wyrobie chlorku amonowe¬ go, przez reakcje amonjaku, kwasu weglo¬ wego i chlorku sodowego w obecnosci wody albo przy wyrobie nawozu, zawierajacego chlorek potasu i chlorek amonu, otrzyma¬ nego przez reakcje analogiczna lecz w o- becnosci isoli potasowych.Podczas suszenia, któremu normalnie poddaje sie wymienione sole przed wypu¬ szczeniem ich na rynek, zawarte w nich lotne sole anionowe uchodza razem z pa¬ ra wodna, jako takie albo mniej lub wie¬ cej zdysocjowane, zas ich odzyskiwanie jest dosc trudne i niecalkowite skutkiem obec¬ nosci duzych mais gazów obcych, któremi sa rozcienczone.Wynalazek niniejszy ma na celu zapo¬ bieganie tym stratom i polega na trakto¬ waniu wymienionych soli dwutlenkiem siarki czystym albo zmieszanym z gazami obojetnemi; traktowanie to wykonywa sie albo przed suszeniem albo tez podczas nie¬ go; wtedy sole amonowe jeszcze wilgotne pochlaniaja dwutlenek siarki i przetwa-rzaja sie na siarczyn amonowy, sól trwa¬ la, która nie ulega rozkladowi podczas su¬ szeniai ,mies#a 'sie z ianemi solami.Zreszta siarczyn, sól rozpuszczalna i latwo sie utleniajaca, przetwarza sie na siarczan, czesciowo juz podczas suszenia, czesciowo zas w ziemi, przy uzyciu wymie^ nionych soli jako nawozów. Widocznem wiec jesit, ze dzieki niniejszemu wynalazko¬ wi unika sie kosztów przy odzyskiwaniu strat azotu, a jednoczesnie zwieksza sie ilosc azotu w wytworzonych solach, co sta¬ nowi dodatkowa korzysc/ Szczególniej wazaiem zródlem dwutlen¬ ku siarki, dajacego sie zuzytkowac przy stosowaniu niniejszego sposobu, sa gazy pozostale po stracaniu dwuweglanu sodo¬ wego zapoimoca dwutlenku wegla, zawie¬ rajacego siarkowodór, jak to ma miejsce naprzyklad gdy ten dwutlenek wegla po¬ chodzi z oczyszczania gazów z pieców koksowych, gazu wodnego albo innych ga¬ zów, zawierajacych jednoczesnie siarko¬ wodór i kwas weglowy, roztworem amo- njaku, przyczem po takiem oczyszcza¬ niu nastepuje destylacja otrzymanego roztworu amonjakalnego; te pozostalo¬ sci gazowe zawieraja tylko siarkowo¬ dór i nieznaczna ilosc dwutlenku we¬ gla. W tym przypadku wszystkie albo tyl¬ ko czesc tych pozostalosci gazowych do¬ prowadza sie do paleniska albo do pajkii- ka urzadzenia, suszacego obrabiane sole, albo tez do niezaleznego paleniska czy pal¬ nika w razie suszenia para. Siaritowodór przetwarza sie w ten sposób na bezwod¬ nik siarkawy, otrzymane spaliny przepro¬ wadza sie nastepnie nad obrabianemu so¬ lami. PL PL PL PL PL PL PL PL PLThe present invention relates to a method of treating salts for their use as fertilizers and relates in particular to those salts which, due to the method of their preparation, contain a certain amount of volatile ammoniacal bodies which cannot be completely removed by washing, such as, for example, carbonates of anions, ammonium sulphide and Lp. This occurs, for example, in the production of ammonium chloride by the reaction of ammonia, carbonic acid and sodium chloride in the presence of water, or in the production of a fertilizer containing potassium chloride and ammonium chloride obtained by an analogous reaction but in the presence of potassium salts. During the drying to which the above-mentioned salts are normally subjected before they are released on the market, the volatile anion salts contained therein escape together with the water vapor, as such or more or less dissociated, and their recovery is quite difficult and This is not entirely due to the presence of large masses of foreign gases with which they are diluted. The present invention aims to prevent these losses and consists in treating the above-mentioned salts with sulfur dioxide, pure or mixed with inert gases. This treatment is carried out either before or during drying. Then, the ammonium salts, while still moist, absorb sulfur dioxide and are converted into ammonium sulfite, a stable salt that does not decompose during drying and mixing with other salts. Furthermore, sulfite, a soluble and easily oxidized salt, is converted into sulfate, partly during drying and partly in the ground, using the above-mentioned salts as fertilizers. It is therefore apparent that the present invention avoids the costs of recovering nitrogen losses and at the same time increases the amount of nitrogen in the salts produced, which is an additional advantage. A particularly important source of sulphur dioxide which can be utilized in the present method is the gases remaining after the precipitation of sodium bicarbonate by means of carbon dioxide containing hydrogen sulphide, as occurs, for example, when this carbon dioxide is obtained from the purification of coke oven gases, water gas or other gases containing both hydrogen sulphide and carbonic acid, with an ammonia solution, such purification being followed by distillation of the ammonia solution obtained; These gaseous residues contain only hydrogen sulfide and a small amount of carbon dioxide. In this case, all or only a portion of these gaseous residues are fed to the furnace or to the paddle of the device drying the treated salts, or to a separate furnace or burner in the case of steam drying. The hydrogen sulfide is thus converted into sulfurous anhydride, and the resulting exhaust gases are then passed over the treated salts. PL PL PL PL PL PL PL PL PL PL

Claims (1)

1.1.
PL10656A 1928-03-16 A method of treating salt in order to use it as a fertilizer. PL10656B1 (en)

Publications (1)

Publication Number Publication Date
PL10656B1 true PL10656B1 (en) 1929-08-31

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