PL106044B1 - Sposob wytwarzania katalizatorow wanadowych do utleniania naftalenu - Google Patents
Sposob wytwarzania katalizatorow wanadowych do utleniania naftalenu Download PDFInfo
- Publication number
- PL106044B1 PL106044B1 PL19658977A PL19658977A PL106044B1 PL 106044 B1 PL106044 B1 PL 106044B1 PL 19658977 A PL19658977 A PL 19658977A PL 19658977 A PL19658977 A PL 19658977A PL 106044 B1 PL106044 B1 PL 106044B1
- Authority
- PL
- Poland
- Prior art keywords
- carrier
- temperature
- suspension
- catalysts
- mass
- Prior art date
Links
- 239000003054 catalyst Substances 0.000 title claims description 26
- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 title claims description 20
- 238000007254 oxidation reaction Methods 0.000 title claims description 11
- 230000003647 oxidation Effects 0.000 title claims description 10
- 238000004519 manufacturing process Methods 0.000 title description 4
- 238000000034 method Methods 0.000 claims description 32
- 239000000725 suspension Substances 0.000 claims description 19
- 239000000126 substance Substances 0.000 claims description 18
- 230000003197 catalytic effect Effects 0.000 claims description 16
- 239000002904 solvent Substances 0.000 claims description 14
- 239000013543 active substance Substances 0.000 claims description 8
- 238000009835 boiling Methods 0.000 claims description 6
- 238000000354 decomposition reaction Methods 0.000 claims description 5
- 230000009466 transformation Effects 0.000 claims description 5
- 238000002360 preparation method Methods 0.000 claims description 4
- 229910052720 vanadium Inorganic materials 0.000 claims description 4
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 claims description 3
- 239000000203 mixture Substances 0.000 description 10
- 239000002609 medium Substances 0.000 description 9
- GNTDGMZSJNCJKK-UHFFFAOYSA-N divanadium pentaoxide Chemical compound O=[V](=O)O[V](=O)=O GNTDGMZSJNCJKK-UHFFFAOYSA-N 0.000 description 6
- LGRFSURHDFAFJT-UHFFFAOYSA-N Phthalic anhydride Natural products C1=CC=C2C(=O)OC(=O)C2=C1 LGRFSURHDFAFJT-UHFFFAOYSA-N 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 5
- 238000001704 evaporation Methods 0.000 description 5
- 239000012071 phase Substances 0.000 description 5
- JHIWVOJDXOSYLW-UHFFFAOYSA-N butyl 2,2-difluorocyclopropane-1-carboxylate Chemical compound CCCCOC(=O)C1CC1(F)F JHIWVOJDXOSYLW-UHFFFAOYSA-N 0.000 description 4
- 230000008020 evaporation Effects 0.000 description 4
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
- 239000012072 active phase Substances 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 239000006185 dispersion Substances 0.000 description 3
- 238000007493 shaping process Methods 0.000 description 3
- 239000007858 starting material Substances 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 229910045601 alloy Inorganic materials 0.000 description 2
- 239000000956 alloy Substances 0.000 description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
- 239000012736 aqueous medium Substances 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 230000008021 deposition Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 2
- XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical compound OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 239000002002 slurry Substances 0.000 description 2
- UMGDCJDMYOKAJW-UHFFFAOYSA-N thiourea Chemical compound NC(N)=S UMGDCJDMYOKAJW-UHFFFAOYSA-N 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 229910004809 Na2 SO4 Inorganic materials 0.000 description 1
- 229910017895 Sb2 O3 Inorganic materials 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Natural products NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
- XHCLAFWTIXFWPH-UHFFFAOYSA-N [O-2].[O-2].[O-2].[O-2].[O-2].[V+5].[V+5] Chemical class [O-2].[O-2].[O-2].[O-2].[O-2].[V+5].[V+5] XHCLAFWTIXFWPH-UHFFFAOYSA-N 0.000 description 1
- 150000008064 anhydrides Chemical class 0.000 description 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
- MYKZLATVIJZNTH-UHFFFAOYSA-N azane;cyano thiocyanate Chemical compound N.N#CSC#N MYKZLATVIJZNTH-UHFFFAOYSA-N 0.000 description 1
- UNTBPXHCXVWYOI-UHFFFAOYSA-O azanium;oxido(dioxo)vanadium Chemical compound [NH4+].[O-][V](=O)=O UNTBPXHCXVWYOI-UHFFFAOYSA-O 0.000 description 1
- 229910052797 bismuth Inorganic materials 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000001747 exhibiting effect Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 229910052748 manganese Inorganic materials 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 150000004706 metal oxides Chemical class 0.000 description 1
- 229910052750 molybdenum Inorganic materials 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 150000002823 nitrates Chemical class 0.000 description 1
- 150000003891 oxalate salts Chemical class 0.000 description 1
- 235000006408 oxalic acid Nutrition 0.000 description 1
- OGUCKKLSDGRKSH-UHFFFAOYSA-N oxalic acid oxovanadium Chemical compound [V].[O].C(C(=O)O)(=O)O OGUCKKLSDGRKSH-UHFFFAOYSA-N 0.000 description 1
- 238000002203 pretreatment Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- -1 salts metals Chemical class 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000011973 solid acid Substances 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 238000007669 thermal treatment Methods 0.000 description 1
- 229910052718 tin Inorganic materials 0.000 description 1
- 229910052721 tungsten Inorganic materials 0.000 description 1
- 238000009827 uniform distribution Methods 0.000 description 1
- 150000003681 vanadium Chemical class 0.000 description 1
- 150000003682 vanadium compounds Chemical class 0.000 description 1
- 229910001935 vanadium oxide Inorganic materials 0.000 description 1
- 239000003039 volatile agent Substances 0.000 description 1
Landscapes
- Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL19658977A PL106044B1 (pl) | 1977-03-11 | 1977-03-11 | Sposob wytwarzania katalizatorow wanadowych do utleniania naftalenu |
| YU55178A YU55178A (en) | 1977-03-11 | 1978-03-09 | Process for obtaining catalysts for the oxidation of naphthalene |
| HUII000261 HU177108B (hu) | 1977-03-11 | 1978-03-10 | Eljárás katalizátor előállítására naftalin-oxidációjához |
| CS152478A CS199720B2 (cs) | 1977-03-11 | 1978-03-10 | Způsob výroby katalyzátoru pro oxidaci naftalenu |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL19658977A PL106044B1 (pl) | 1977-03-11 | 1977-03-11 | Sposob wytwarzania katalizatorow wanadowych do utleniania naftalenu |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| PL196589A1 PL196589A1 (pl) | 1978-10-09 |
| PL106044B1 true PL106044B1 (pl) | 1979-11-30 |
Family
ID=19981375
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL19658977A PL106044B1 (pl) | 1977-03-11 | 1977-03-11 | Sposob wytwarzania katalizatorow wanadowych do utleniania naftalenu |
Country Status (4)
| Country | Link |
|---|---|
| CS (1) | CS199720B2 (cs) |
| HU (1) | HU177108B (cs) |
| PL (1) | PL106044B1 (cs) |
| YU (1) | YU55178A (cs) |
-
1977
- 1977-03-11 PL PL19658977A patent/PL106044B1/pl not_active IP Right Cessation
-
1978
- 1978-03-09 YU YU55178A patent/YU55178A/xx unknown
- 1978-03-10 HU HUII000261 patent/HU177108B/hu unknown
- 1978-03-10 CS CS152478A patent/CS199720B2/cs unknown
Also Published As
| Publication number | Publication date |
|---|---|
| PL196589A1 (pl) | 1978-10-09 |
| YU55178A (en) | 1982-06-30 |
| CS199720B2 (cs) | 1980-07-31 |
| HU177108B (hu) | 1981-07-28 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| LAPS | Decisions on the lapse of the protection rights |
Effective date: 20080203 |