PH12016501880A1 - Purification method and purification device for target gas - Google Patents

Purification method and purification device for target gas

Info

Publication number
PH12016501880A1
PH12016501880A1 PH12016501880A PH12016501880A PH12016501880A1 PH 12016501880 A1 PH12016501880 A1 PH 12016501880A1 PH 12016501880 A PH12016501880 A PH 12016501880A PH 12016501880 A PH12016501880 A PH 12016501880A PH 12016501880 A1 PH12016501880 A1 PH 12016501880A1
Authority
PH
Philippines
Prior art keywords
adsorption
gas
units
pressure
adsorbent
Prior art date
Application number
PH12016501880A
Other versions
PH12016501880B1 (en
Inventor
Iwamoto Jun-Ichi
Kishii Mitsuru
shima Koichi
Original Assignee
Sumitomo Seika Chemicals
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sumitomo Seika Chemicals filed Critical Sumitomo Seika Chemicals
Publication of PH12016501880A1 publication Critical patent/PH12016501880A1/en
Publication of PH12016501880B1 publication Critical patent/PH12016501880B1/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/50—Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification
    • C01B3/56—Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification by contacting with solids; Regeneration of used solids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/047—Pressure swing adsorption
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10—Inorganic adsorbents
    • B01D2253/102—Carbon
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10—Inorganic adsorbents
    • B01D2253/104—Alumina
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10—Inorganic adsorbents
    • B01D2253/106—Silica or silicates
    • B01D2253/108—Zeolites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2256/00—Main component in the product gas stream after treatment
    • B01D2256/16—Hydrogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2256/00—Main component in the product gas stream after treatment
    • B01D2256/18—Noble gases
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/30—Sulfur compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/50—Carbon oxides
    • B01D2257/502—Carbon monoxide
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/50—Carbon oxides
    • B01D2257/504—Carbon dioxide
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/70—Organic compounds not provided for in groups B01D2257/00 - B01D2257/602
    • B01D2257/702—Hydrocarbons
    • B01D2257/7022—Aliphatic hydrocarbons
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/70—Organic compounds not provided for in groups B01D2257/00 - B01D2257/602
    • B01D2257/702—Hydrocarbons
    • B01D2257/7022—Aliphatic hydrocarbons
    • B01D2257/7025—Methane
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/70—Organic compounds not provided for in groups B01D2257/00 - B01D2257/602
    • B01D2257/702—Hydrocarbons
    • B01D2257/7027—Aromatic hydrocarbons
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/80—Water
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2258/00—Sources of waste gases
    • B01D2258/02—Other waste gases
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40058—Number of sequence steps, including sub-steps, per cycle
    • B01D2259/40075—More than ten
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/404—Further details for adsorption processes and devices using four beds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/41—Further details for adsorption processes and devices using plural beds of the same adsorbent in series
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02C—CAPTURE, STORAGE, SEQUESTRATION OR DISPOSAL OF GREENHOUSE GASES [GHG]
    • Y02C20/00—Capture or disposal of greenhouse gases
    • Y02C20/20—Capture or disposal of greenhouse gases of methane
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02C—CAPTURE, STORAGE, SEQUESTRATION OR DISPOSAL OF GREENHOUSE GASES [GHG]
    • Y02C20/00—Capture or disposal of greenhouse gases
    • Y02C20/40—Capture or disposal of greenhouse gases of CO2
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/151—Reduction of greenhouse gas [GHG] emissions, e.g. CO2
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/151—Reduction of greenhouse gas [GHG] emissions, e.g. CO2
    • Y02P20/156—Methane [CH4]

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Combustion & Propulsion (AREA)
  • Inorganic Chemistry (AREA)
  • Separation Of Gases By Adsorption (AREA)
  • Hydrogen, Water And Hydrids (AREA)
  • Industrial Gases (AREA)

Abstract

The problem addressed by the present invention is, when purifying a target gas from a mixed gas containing a target component using pressure swing adsorption, preventing effects of impurity components that reduce the purification capacity of an adsorbent while recovering high-purity target gas with good efficiency. This method repeatedly carries out, for each adsorption unit, a cycle that includes an adsorption step wherein the mixed gas is introduced into adsorption units, in a state where the adsorption units are at relatively high pressure, by pressure swing adsorption carried out using a plurality of adsorption units filled with the adsorbent, which selectively adsorbs impurity components, the adsorbent is made to adsorb the impurity components in the mixed gas, and a gas in which the target component is enriched is exhausted from the adsorption units and a pressure reduction step wherein pressure is reduced in the adsorption units and gas is exhausted from the adsorption units. Each adsorption unit includes first and second adsorption tanks (10A - 10D, 20A - 20D) connected in series. In the pressure reduction step, switching between a state in which the first and second adsorption tanks are linked and a state where the same are not linked is carried out by an on-off valve (16) provided between the first and second adsorption tanks.
PH12016501880A 2014-03-28 2016-09-23 Purification method and purification device for target gas PH12016501880B1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2014068970 2014-03-28
PCT/JP2015/058189 WO2015146766A1 (en) 2014-03-28 2015-03-19 Purification method and purification device for target gas

Publications (2)

Publication Number Publication Date
PH12016501880A1 true PH12016501880A1 (en) 2017-01-09
PH12016501880B1 PH12016501880B1 (en) 2017-01-09

Family

ID=54195287

Family Applications (1)

Application Number Title Priority Date Filing Date
PH12016501880A PH12016501880B1 (en) 2014-03-28 2016-09-23 Purification method and purification device for target gas

Country Status (5)

Country Link
JP (1) JP6502921B2 (en)
KR (1) KR102317284B1 (en)
PH (1) PH12016501880B1 (en)
TW (1) TWI669270B (en)
WO (1) WO2015146766A1 (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP6585545B2 (en) * 2016-05-20 2019-10-02 株式会社神戸製鋼所 Hydrogen gas production method and hydrogen gas production apparatus
JP6611264B2 (en) * 2017-03-24 2019-11-27 大陽日酸株式会社 Gas purification method and apparatus
TWI771584B (en) * 2019-05-13 2022-07-21 純萃材料股份有限公司 Adsorption apparatus and adsorption method

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4264340A (en) * 1979-02-28 1981-04-28 Air Products And Chemicals, Inc. Vacuum swing adsorption for air fractionation
JPS58168876A (en) 1982-03-31 1983-10-05 日本酸素株式会社 Method of recovering hydrogen from coke oven gas
JPS605419U (en) * 1983-06-20 1985-01-16 新日本製鐵株式会社 Pressure swing adsorption/desorption device
DE3543468A1 (en) * 1985-12-09 1987-06-11 Linde Ag PRESSURE EXCHANGE ADDING METHOD
DE3716898A1 (en) 1987-05-20 1988-12-15 Bergwerksverband Gmbh METHOD AND DEVICE FOR HELIUM ENHANCEMENT
JPH06126120A (en) * 1992-10-13 1994-05-10 Nippon Steel Corp Method for increasing co concentration in cracking gas
WO2002051523A1 (en) * 2000-12-26 2002-07-04 Sumitomo Seika Chemicals Co., Ltd. Method and device for separating object gas
JP4180534B2 (en) * 2004-02-24 2008-11-12 本田技研工業株式会社 Fuel gas production apparatus and operation method thereof
JP4481112B2 (en) * 2004-08-26 2010-06-16 大陽日酸株式会社 Pressure fluctuation adsorption type gas separation method and apparatus

Also Published As

Publication number Publication date
WO2015146766A1 (en) 2015-10-01
JPWO2015146766A1 (en) 2017-04-13
KR20160137622A (en) 2016-11-30
TW201605722A (en) 2016-02-16
KR102317284B1 (en) 2021-10-25
JP6502921B2 (en) 2019-04-17
PH12016501880B1 (en) 2017-01-09
TWI669270B (en) 2019-08-21

Similar Documents

Publication Publication Date Title
MX2018011639A (en) Processes using improved rho adsorbent compositions.
EA201391250A1 (en) METHODS OF REMOVING POLLUTING IMPURITIES FROM A FLOW OF HYDROCARBONS IN A CYCLIC ADSORPTION PROCESS AND ASSOCIATED DEVICES AND SYSTEMS
MX2013004914A (en) Kinetic fractionators, and cycling processes for fractionation of gas mixtures.
EA201391257A1 (en) METHODS OF REMOVING POLLUTING IMPURITIES FROM A FLOW OF HYDROCARBONS IN A CYCLIC ADSORPTION PROCESS AND ASSOCIATED DEVICES AND SYSTEMS
MX371091B (en) Sorbents for removal of mercury.
MY188714A (en) Heater arrangement for tepsa system
WO2014137907A3 (en) Activated carbon sorbent including nitrogen and methods of using the same
WO2006076402A3 (en) Methods and apparatus for improved control of psa flow variations
WO2012024135A3 (en) Process for purifying natural gas and regenerating one or more adsorbers
MX2018003546A (en) Adsorbent regeneration method in a combined pressure and temperature swing adsorption process.
PH12016501880A1 (en) Purification method and purification device for target gas
PH12015501485A1 (en) Gas purification apparatus
MX2018011640A (en) Rho adsorbent compositions, methods of making and using them.
PH12019500651A1 (en) Method for purifying hydrogen or helium, and device for purifying hydrogen or helium
WO2016003484A3 (en) A rapid temperature swing adsorption (rtsa) method using structured adsorbent for co2 capture from low pressure and low co2 concentration sources
MX2019009509A (en) Multi-bed rapid cycle kinetic psa.
PH12016502584A1 (en) Gas concentration method
WO2013106046A3 (en) Purification of trans-1,3,3,3-tetrafluoropropene
MY161178A (en) Process for purifying a gas in a temperature swing adsorption unit
EP3495032A3 (en) Method of drying a hydrogen gas mixture produced by an electrochemical hydrogen compressor
EA201370228A1 (en) LOW ENERGY CYCLIC METHOD PSA
MY160935A (en) Vertical baffle in horizontal adsorber vessels
PH12019500649A1 (en) Method for purifying hydrogen or helium gas, and apparatus for purifying hydrogen or helium gas
MY182513A (en) Process for purification of an organic composition
WO2017095268A4 (en) Separation of multi-component gas mixtures by a pressure swing adsorption method