NO975499L - Form III krystallinsk (R-(R*,R*)-2(4-fluorfenyl)-<beta>-<delta>-dihydroksy-(1-metyl-etyl)-3-fenyl-4-(fenylamino)karbonyl)-1H-pyrrol-1-heptansyre-hemi-kalsiumsalt - Google Patents
Form III krystallinsk (R-(R*,R*)-2(4-fluorfenyl)-<beta>-<delta>-dihydroksy-(1-metyl-etyl)-3-fenyl-4-(fenylamino)karbonyl)-1H-pyrrol-1-heptansyre-hemi-kalsiumsaltInfo
- Publication number
- NO975499L NO975499L NO975499A NO975499A NO975499L NO 975499 L NO975499 L NO 975499L NO 975499 A NO975499 A NO 975499A NO 975499 A NO975499 A NO 975499A NO 975499 L NO975499 L NO 975499L
- Authority
- NO
- Norway
- Prior art keywords
- phenylamino
- fluorophenyl
- pyrrole
- dihydroxy
- carbonyl
- Prior art date
Links
- -1 (4-Fluorophenyl) - Chemical class 0.000 title abstract 2
- 159000000007 calcium salts Chemical class 0.000 title 1
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 title 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 2
- 125000004642 (C1-C12) alkoxy group Chemical group 0.000 abstract 1
- 125000006273 (C1-C3) alkyl group Chemical group 0.000 abstract 1
- 125000006559 (C1-C3) alkylamino group Chemical group 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 125000000217 alkyl group Chemical group 0.000 abstract 1
- 229910021529 ammonia Inorganic materials 0.000 abstract 1
- SXZIXHOMFPUIRK-UHFFFAOYSA-N diphenylmethanimine Chemical compound C=1C=CC=CC=1C(=N)C1=CC=CC=C1 SXZIXHOMFPUIRK-UHFFFAOYSA-N 0.000 abstract 1
- 150000002148 esters Chemical class 0.000 abstract 1
- 239000007789 gas Substances 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 125000004430 oxygen atom Chemical group O* 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C253/00—Preparation of carboxylic acid nitriles
- C07C253/30—Preparation of carboxylic acid nitriles by reactions not involving the formation of cyano groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C255/00—Carboxylic acid nitriles
- C07C255/01—Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms
- C07C255/32—Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms having cyano groups bound to acyclic carbon atoms of a carbon skeleton containing at least one six-membered aromatic ring
- C07C255/41—Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms having cyano groups bound to acyclic carbon atoms of a carbon skeleton containing at least one six-membered aromatic ring the carbon skeleton being further substituted by carboxyl groups, other than cyano groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Fremgangsmåte for fremstilling av flytende 2-cyan-3,3-diarylakrylsyreestere med den generelle formel l \ / c=c. /CN /=( COOR3 V > (I) hvori R1 og R2 betyr hydrogen, C^C^-alkylgrupper, C,-C12-alkoksygrupper eller di- (C^C^alkyOaminogrupper, og R3 en C4-C18-alkylgruppe, som kan være avbrutt med oksygenatomer i eierfunksjon, ved omsetning av et benzofenonimin med den generelle formel II C=NH (II) med en cyaneddikester med den generelle formel r /CN COOR3 (in) karakterisert ved at man foretar omsetningen ved 20 til 60°C, og at man herunder løpende fjerner den frigjorte ammoniakk fra reaksjonsblandingen ved hjelp av en gass-strøm eller ved redusering av trykket til 900-100 mbar.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19519894A DE19519894A1 (de) | 1995-05-31 | 1995-05-31 | Verfahren zur Herstellung von 2-Cyan-3,3-diarylacrylsäureestern |
| PCT/EP1996/002238 WO1996038409A1 (de) | 1995-05-31 | 1996-05-24 | Verfahren zur herstellung von 2-cyan-3,3-diarylacrylsäureestern |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| NO975499D0 NO975499D0 (no) | 1997-11-28 |
| NO975499L true NO975499L (no) | 1997-11-28 |
Family
ID=7763277
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO975499A NO975499L (no) | 1995-05-31 | 1997-11-28 | Form III krystallinsk (R-(R*,R*)-2(4-fluorfenyl)-<beta>-<delta>-dihydroksy-(1-metyl-etyl)-3-fenyl-4-(fenylamino)karbonyl)-1H-pyrrol-1-heptansyre-hemi-kalsiumsalt |
Country Status (16)
| Country | Link |
|---|---|
| US (1) | US5917080A (no) |
| EP (1) | EP0828708A1 (no) |
| JP (1) | JP3773534B2 (no) |
| KR (1) | KR19990014781A (no) |
| CN (1) | CN1071312C (no) |
| AU (1) | AU6000096A (no) |
| BG (1) | BG102059A (no) |
| BR (1) | BR9608495A (no) |
| CA (1) | CA2218813A1 (no) |
| DE (1) | DE19519894A1 (no) |
| NO (1) | NO975499L (no) |
| NZ (1) | NZ309758A (no) |
| PL (1) | PL323590A1 (no) |
| TR (1) | TR199701451T1 (no) |
| TW (1) | TW419453B (no) |
| WO (1) | WO1996038409A1 (no) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19850624A1 (de) * | 1998-11-03 | 2000-05-04 | Basf Ag | Verfahren zur Herstellung von Cyanessigsäureestern |
| DE10161864A1 (de) * | 2001-12-14 | 2003-07-03 | Basf Ag | Stabilisatorzusammensetzung III |
| US7763994B2 (en) | 2005-01-25 | 2010-07-27 | Panasonic Corporation | Power source system |
| US8641957B2 (en) * | 2006-07-05 | 2014-02-04 | GM Global Technology Operations LLC | Molding cosmetic composite panels with visible fibers from ultraviolent light resistant epoxy compositions |
| WO2008089920A1 (en) * | 2007-01-26 | 2008-07-31 | Dsm Ip Assets B.V. | Process for the manufacture of substituted 2-cyano cinnamic esters |
| DE102007011069A1 (de) * | 2007-03-07 | 2008-09-11 | Bayer Materialscience Ag | Polycarbonatzusammensetzung enthaltend UV-Absorber |
| US9670144B2 (en) | 2013-05-02 | 2017-06-06 | Galaxy Surfactants, Ltd. | Process for the preparation of 2-cyano-3,3-diarylacrylates |
| CN109608360B (zh) * | 2018-11-13 | 2021-09-03 | 中国天辰工程有限公司 | 一种制备1-氨基-2-氰基环戊烯的方法 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3215724A (en) * | 1961-09-18 | 1965-11-02 | Gen Aniline & Film Corp | alpha-cyano-beta, beta-diphenyl acrylic acid esters |
| EP0430023A1 (en) * | 1989-11-29 | 1991-06-05 | BASF Corporation | Process for the preparation of substituted phenylcinnamates |
| DE4314035B4 (de) * | 1993-04-29 | 2004-07-01 | Symrise Gmbh & Co. Kg | Verfahren zur Herstellung von substituierten 2-Cyanzimtsäureestern |
| DE4442138A1 (de) * | 1994-11-26 | 1996-05-30 | Basf Ag | Verfahren zur Herstellung von Benzophenonimin |
-
1995
- 1995-05-31 DE DE19519894A patent/DE19519894A1/de not_active Withdrawn
-
1996
- 1996-05-24 CA CA002218813A patent/CA2218813A1/en not_active Abandoned
- 1996-05-24 PL PL96323590A patent/PL323590A1/xx unknown
- 1996-05-24 AU AU60000/96A patent/AU6000096A/en not_active Abandoned
- 1996-05-24 US US08/952,667 patent/US5917080A/en not_active Expired - Lifetime
- 1996-05-24 NZ NZ309758A patent/NZ309758A/en unknown
- 1996-05-24 JP JP53616396A patent/JP3773534B2/ja not_active Expired - Lifetime
- 1996-05-24 WO PCT/EP1996/002238 patent/WO1996038409A1/de not_active Ceased
- 1996-05-24 KR KR1019970708124A patent/KR19990014781A/ko not_active Withdrawn
- 1996-05-24 EP EP96917418A patent/EP0828708A1/de not_active Withdrawn
- 1996-05-24 BR BR9608495A patent/BR9608495A/pt not_active Application Discontinuation
- 1996-05-24 CN CN96194236A patent/CN1071312C/zh not_active Expired - Lifetime
- 1996-05-24 TR TR97/01451T patent/TR199701451T1/xx unknown
- 1996-05-31 TW TW085106506A patent/TW419453B/zh active
-
1997
- 1997-11-20 BG BG102059A patent/BG102059A/xx unknown
- 1997-11-28 NO NO975499A patent/NO975499L/no unknown
Also Published As
| Publication number | Publication date |
|---|---|
| NZ309758A (en) | 1999-04-29 |
| WO1996038409A1 (de) | 1996-12-05 |
| KR19990014781A (ko) | 1999-02-25 |
| TW419453B (en) | 2001-01-21 |
| NO975499D0 (no) | 1997-11-28 |
| TR199701451T1 (xx) | 1998-03-21 |
| CA2218813A1 (en) | 1996-12-05 |
| DE19519894A1 (de) | 1996-12-05 |
| BG102059A (en) | 1998-09-30 |
| CN1185780A (zh) | 1998-06-24 |
| BR9608495A (pt) | 1999-07-06 |
| JPH11505858A (ja) | 1999-05-25 |
| PL323590A1 (en) | 1998-04-14 |
| US5917080A (en) | 1999-06-29 |
| CN1071312C (zh) | 2001-09-19 |
| AU6000096A (en) | 1996-12-18 |
| MX9708836A (es) | 1998-03-31 |
| EP0828708A1 (de) | 1998-03-18 |
| JP3773534B2 (ja) | 2006-05-10 |
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