NO315902B1 - Fremgangsmåte for fremstilling av et sensitivisert emulsjonssprengstoff - Google Patents
Fremgangsmåte for fremstilling av et sensitivisert emulsjonssprengstoff Download PDFInfo
- Publication number
- NO315902B1 NO315902B1 NO20016374A NO20016374A NO315902B1 NO 315902 B1 NO315902 B1 NO 315902B1 NO 20016374 A NO20016374 A NO 20016374A NO 20016374 A NO20016374 A NO 20016374A NO 315902 B1 NO315902 B1 NO 315902B1
- Authority
- NO
- Norway
- Prior art keywords
- emulsion
- gas
- urea
- solution
- gassing
- Prior art date
Links
- 239000000839 emulsion Substances 0.000 title claims abstract description 136
- 239000002360 explosive Substances 0.000 title claims abstract description 42
- 238000000034 method Methods 0.000 title claims abstract description 38
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims abstract description 102
- 239000004202 carbamide Substances 0.000 claims abstract description 53
- IOVCWXUNBOPUCH-UHFFFAOYSA-M Nitrite anion Chemical compound [O-]N=O IOVCWXUNBOPUCH-UHFFFAOYSA-M 0.000 claims abstract description 11
- 150000007524 organic acids Chemical class 0.000 claims abstract description 10
- 125000004432 carbon atom Chemical group C* 0.000 claims abstract description 4
- 239000003153 chemical reaction reagent Substances 0.000 claims description 49
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 48
- 230000001050 lubricating effect Effects 0.000 claims description 38
- 230000003647 oxidation Effects 0.000 claims description 28
- 238000007254 oxidation reaction Methods 0.000 claims description 28
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 claims description 9
- 239000000446 fuel Substances 0.000 claims description 7
- 230000001235 sensitizing effect Effects 0.000 claims description 7
- 235000002906 tartaric acid Nutrition 0.000 claims description 7
- 239000011975 tartaric acid Substances 0.000 claims description 7
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 6
- 238000004519 manufacturing process Methods 0.000 claims description 5
- 150000003839 salts Chemical class 0.000 claims description 5
- MWUXSHHQAYIFBG-UHFFFAOYSA-N nitrogen oxide Inorganic materials O=[N] MWUXSHHQAYIFBG-UHFFFAOYSA-N 0.000 abstract description 99
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 31
- 239000000126 substance Substances 0.000 abstract description 7
- 231100000331 toxic Toxicity 0.000 abstract description 5
- 230000002588 toxic effect Effects 0.000 abstract description 5
- 238000005461 lubrication Methods 0.000 abstract description 4
- 239000007789 gas Substances 0.000 description 148
- 239000000243 solution Substances 0.000 description 49
- 239000000203 mixture Substances 0.000 description 22
- 239000007762 w/o emulsion Substances 0.000 description 14
- LPXPTNMVRIOKMN-UHFFFAOYSA-M sodium nitrite Chemical compound [Na+].[O-]N=O LPXPTNMVRIOKMN-UHFFFAOYSA-M 0.000 description 10
- PXRKCOCTEMYUEG-UHFFFAOYSA-N 5-aminoisoindole-1,3-dione Chemical compound NC1=CC=C2C(=O)NC(=O)C2=C1 PXRKCOCTEMYUEG-UHFFFAOYSA-N 0.000 description 9
- 230000015572 biosynthetic process Effects 0.000 description 9
- PAWQVTBBRAZDMG-UHFFFAOYSA-N 2-(3-bromo-2-fluorophenyl)acetic acid Chemical compound OC(=O)CC1=CC=CC(Br)=C1F PAWQVTBBRAZDMG-UHFFFAOYSA-N 0.000 description 8
- 238000002309 gasification Methods 0.000 description 8
- 238000002156 mixing Methods 0.000 description 7
- 238000005422 blasting Methods 0.000 description 6
- 239000012530 fluid Substances 0.000 description 6
- UMGDCJDMYOKAJW-UHFFFAOYSA-N thiourea Chemical compound NC(N)=S UMGDCJDMYOKAJW-UHFFFAOYSA-N 0.000 description 6
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Natural products CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 5
- 235000010288 sodium nitrite Nutrition 0.000 description 5
- 239000003795 chemical substances by application Substances 0.000 description 4
- 239000012266 salt solution Substances 0.000 description 4
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- 239000003995 emulsifying agent Substances 0.000 description 3
- NIFIFKQPDTWWGU-UHFFFAOYSA-N pyrite Chemical compound [Fe+2].[S-][S-] NIFIFKQPDTWWGU-UHFFFAOYSA-N 0.000 description 3
- 229910052683 pyrite Inorganic materials 0.000 description 3
- 239000011028 pyrite Substances 0.000 description 3
- ZORQXIQZAOLNGE-UHFFFAOYSA-N 1,1-difluorocyclohexane Chemical compound FC1(F)CCCCC1 ZORQXIQZAOLNGE-UHFFFAOYSA-N 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 206010070834 Sensitisation Diseases 0.000 description 2
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- ZCCIPPOKBCJFDN-UHFFFAOYSA-N calcium nitrate Chemical compound [Ca+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O ZCCIPPOKBCJFDN-UHFFFAOYSA-N 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000007800 oxidant agent Substances 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 238000005086 pumping Methods 0.000 description 2
- 230000008313 sensitization Effects 0.000 description 2
- VWDWKYIASSYTQR-UHFFFAOYSA-N sodium nitrate Chemical compound [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000001593 sorbitan monooleate Substances 0.000 description 2
- 229940035049 sorbitan monooleate Drugs 0.000 description 2
- 235000011069 sorbitan monooleate Nutrition 0.000 description 2
- 230000003068 static effect Effects 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 238000005979 thermal decomposition reaction Methods 0.000 description 2
- 239000002341 toxic gas Substances 0.000 description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 241000219146 Gossypium Species 0.000 description 1
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 description 1
- 229920005372 Plexiglas® Polymers 0.000 description 1
- ZMZDMBWJUHKJPS-UHFFFAOYSA-M Thiocyanate anion Chemical compound [S-]C#N ZMZDMBWJUHKJPS-UHFFFAOYSA-M 0.000 description 1
- 125000000218 acetic acid group Chemical group C(C)(=O)* 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000003638 chemical reducing agent Substances 0.000 description 1
- -1 citric acid Chemical class 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- XLJMAIOERFSOGZ-UHFFFAOYSA-M cyanate Chemical compound [O-]C#N XLJMAIOERFSOGZ-UHFFFAOYSA-M 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 239000002316 fumigant Substances 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- XMBWDFGMSWQBCA-UHFFFAOYSA-N hydrogen iodide Chemical compound I XMBWDFGMSWQBCA-UHFFFAOYSA-N 0.000 description 1
- ZMZDMBWJUHKJPS-UHFFFAOYSA-N hydrogen thiocyanate Natural products SC#N ZMZDMBWJUHKJPS-UHFFFAOYSA-N 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 229910001959 inorganic nitrate Inorganic materials 0.000 description 1
- 150000004694 iodide salts Chemical class 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 239000004005 microsphere Substances 0.000 description 1
- 150000002823 nitrates Chemical class 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- GQPLMRYTRLFLPF-UHFFFAOYSA-N nitrous oxide Inorganic materials [O-][N+]#N GQPLMRYTRLFLPF-UHFFFAOYSA-N 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 230000008092 positive effect Effects 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 239000011435 rock Substances 0.000 description 1
- 239000004317 sodium nitrate Substances 0.000 description 1
- 235000010344 sodium nitrate Nutrition 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 150000003567 thiocyanates Chemical class 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
- 231100000925 very toxic Toxicity 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B47/00—Compositions in which the components are separately stored until the moment of burning or explosion, e.g. "Sprengel"-type explosives; Suspensions of solid component in a normally non-explosive liquid phase, including a thickened aqueous phase
- C06B47/14—Compositions in which the components are separately stored until the moment of burning or explosion, e.g. "Sprengel"-type explosives; Suspensions of solid component in a normally non-explosive liquid phase, including a thickened aqueous phase comprising a solid component and an aqueous phase
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B47/00—Compositions in which the components are separately stored until the moment of burning or explosion, e.g. "Sprengel"-type explosives; Suspensions of solid component in a normally non-explosive liquid phase, including a thickened aqueous phase
- C06B47/14—Compositions in which the components are separately stored until the moment of burning or explosion, e.g. "Sprengel"-type explosives; Suspensions of solid component in a normally non-explosive liquid phase, including a thickened aqueous phase comprising a solid component and an aqueous phase
- C06B47/145—Water in oil emulsion type explosives in which a carbonaceous fuel forms the continuous phase
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B23/00—Compositions characterised by non-explosive or non-thermic constituents
- C06B23/002—Sensitisers or density reducing agents, foam stabilisers, crystal habit modifiers
- C06B23/004—Chemical sensitisers
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F42—AMMUNITION; BLASTING
- F42D—BLASTING
- F42D1/00—Blasting methods or apparatus, e.g. loading or tamping
- F42D1/08—Tamping methods; Methods for loading boreholes with explosives; Apparatus therefor
- F42D1/10—Feeding explosives in granular or slurry form; Feeding explosives by pneumatic or hydraulic pressure
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- General Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Lubricants (AREA)
- Medicinal Preparation (AREA)
- Air Bags (AREA)
- Colloid Chemistry (AREA)
- Manufacturing Of Micro-Capsules (AREA)
- Cosmetics (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Priority Applications (15)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NO20016374A NO315902B1 (no) | 2001-12-27 | 2001-12-27 | Fremgangsmåte for fremstilling av et sensitivisert emulsjonssprengstoff |
| ES02783866T ES2292828T3 (es) | 2001-12-27 | 2002-12-20 | Un metodo para preparar un explosivo de emulsion sensibilizada. |
| PT02783866T PT1458660E (pt) | 2001-12-27 | 2002-12-20 | Um método para preparar um explosivo de emulsão sensível |
| PCT/NO2002/000494 WO2003055830A1 (en) | 2001-12-27 | 2002-12-20 | A method for preparing a sensitised emulsion explosive |
| RU2004119560/02A RU2316529C2 (ru) | 2001-12-27 | 2002-12-20 | Способ получения сенсибилизированного эмульсионного взрывчатого вещества |
| KR10-2004-7010187A KR20040077691A (ko) | 2001-12-27 | 2002-12-20 | 증감 유제형 화약 제조방법 |
| AU2002347688A AU2002347688B2 (en) | 2001-12-27 | 2002-12-20 | A method for preparing a sensitised emulsion explosive |
| BRPI0215355-6A BR0215355B1 (pt) | 2001-12-27 | 2002-12-20 | método para preparar um explosivo em emulsão sensibilizado sem a formação de óxidos de nitrigênio tóxicos. |
| DE60222174T DE60222174T2 (de) | 2001-12-27 | 2002-12-20 | Verfahren zur herstellung eines sensibilisierten emulsionssprengstoffs |
| EP02783866A EP1458660B1 (de) | 2001-12-27 | 2002-12-20 | Verfahren zur herstellung eines sensibilisierten emulsionssprengstoffs |
| JP2003556366A JP4138661B2 (ja) | 2001-12-27 | 2002-12-20 | 敏感化されたエマルジョン爆発物の調製方法 |
| CA002469783A CA2469783C (en) | 2001-12-27 | 2002-12-20 | A method for preparing a sensitised emulsion explosive |
| AT02783866T ATE371635T1 (de) | 2001-12-27 | 2002-12-20 | Verfahren zur herstellung eines sensibilisierten emulsionssprengstoffs |
| ZA2004/05073A ZA200405073B (en) | 2001-12-27 | 2004-06-25 | A method for preparing a sensitised emulsion explosive |
| CO04066834A CO5590949A2 (es) | 2001-12-27 | 2004-07-14 | Un metodo para la preparacion de una emulsion explosiva sensibilizada |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NO20016374A NO315902B1 (no) | 2001-12-27 | 2001-12-27 | Fremgangsmåte for fremstilling av et sensitivisert emulsjonssprengstoff |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| NO20016374D0 NO20016374D0 (no) | 2001-12-27 |
| NO20016374L NO20016374L (no) | 2003-06-30 |
| NO315902B1 true NO315902B1 (no) | 2003-11-10 |
Family
ID=19913192
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO20016374A NO315902B1 (no) | 2001-12-27 | 2001-12-27 | Fremgangsmåte for fremstilling av et sensitivisert emulsjonssprengstoff |
Country Status (15)
| Country | Link |
|---|---|
| EP (1) | EP1458660B1 (de) |
| JP (1) | JP4138661B2 (de) |
| KR (1) | KR20040077691A (de) |
| AT (1) | ATE371635T1 (de) |
| AU (1) | AU2002347688B2 (de) |
| BR (1) | BR0215355B1 (de) |
| CA (1) | CA2469783C (de) |
| CO (1) | CO5590949A2 (de) |
| DE (1) | DE60222174T2 (de) |
| ES (1) | ES2292828T3 (de) |
| NO (1) | NO315902B1 (de) |
| PT (1) | PT1458660E (de) |
| RU (1) | RU2316529C2 (de) |
| WO (1) | WO2003055830A1 (de) |
| ZA (1) | ZA200405073B (de) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102004010130B4 (de) * | 2004-03-02 | 2015-03-05 | Maxam Deutschland Gmbh | Verfahren zur Herstellung sowie Verfahren zum Verbringen eines hochviskosen Emulsionssprengstoffs |
| CN102070380A (zh) * | 2010-12-06 | 2011-05-25 | 陕西华秦新能源科技有限责任公司 | 一种炸药用的发泡剂 |
| CN103946184B (zh) | 2011-11-17 | 2019-09-24 | 戴诺诺贝尔亚太股份有限公司 | 炸药组合物 |
| WO2013131139A1 (en) * | 2012-03-09 | 2013-09-12 | Dyno Nobel Asia Pacific Pty Limited | Modified blasting agent |
| BR112015018669B1 (pt) | 2013-02-07 | 2021-04-06 | Dyno Nobel Inc. | Método de variação da energia explosiva de explosivos em um furo para explosão, sistema de entrega de explosivos e método de entrega de explosivos |
| RU2544680C1 (ru) * | 2013-08-19 | 2015-03-20 | Товарищество с ограниченной ответственностью "Индастриал Эксплозив" | Эмульсионное водоустойчивое взрывчатое вещество и эмульсионный состав для водоустойчивых взрывчатых веществ |
| WO2017035594A1 (en) * | 2015-09-01 | 2017-03-09 | The University Of Sydney | Blasting agent |
| SG11202006602WA (en) | 2018-02-20 | 2020-08-28 | Dyno Nobel Inc | Inhibited emulsions for use in blasting in reactive ground or under high temperature conditions |
| US20200216369A1 (en) * | 2019-01-04 | 2020-07-09 | Dyno Nobel Asia Pacific Pty Limited | Explosive compositions with reduced fume |
| CN111747804B (zh) * | 2020-06-22 | 2021-03-16 | 铜陵雷鸣双狮化工有限责任公司 | 一种乳化炸药及其生产工艺 |
| KR20230101310A (ko) * | 2021-12-29 | 2023-07-06 | 주식회사 한화 | 저비중 에멀젼 폭약 조성물 |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2187490B (en) * | 1986-03-05 | 1989-12-06 | Aeci Ltd | Charging of explosives into boreholes |
| ZA962552B (en) * | 1995-04-05 | 1996-10-07 | Aeci Explosives Ltd | Explosive |
-
2001
- 2001-12-27 NO NO20016374A patent/NO315902B1/no not_active IP Right Cessation
-
2002
- 2002-12-20 CA CA002469783A patent/CA2469783C/en not_active Expired - Fee Related
- 2002-12-20 PT PT02783866T patent/PT1458660E/pt unknown
- 2002-12-20 AU AU2002347688A patent/AU2002347688B2/en not_active Ceased
- 2002-12-20 WO PCT/NO2002/000494 patent/WO2003055830A1/en active IP Right Grant
- 2002-12-20 JP JP2003556366A patent/JP4138661B2/ja not_active Expired - Fee Related
- 2002-12-20 BR BRPI0215355-6A patent/BR0215355B1/pt not_active IP Right Cessation
- 2002-12-20 AT AT02783866T patent/ATE371635T1/de not_active IP Right Cessation
- 2002-12-20 DE DE60222174T patent/DE60222174T2/de not_active Expired - Lifetime
- 2002-12-20 KR KR10-2004-7010187A patent/KR20040077691A/ko active IP Right Grant
- 2002-12-20 ES ES02783866T patent/ES2292828T3/es not_active Expired - Lifetime
- 2002-12-20 RU RU2004119560/02A patent/RU2316529C2/ru active
- 2002-12-20 EP EP02783866A patent/EP1458660B1/de not_active Expired - Lifetime
-
2004
- 2004-06-25 ZA ZA2004/05073A patent/ZA200405073B/en unknown
- 2004-07-14 CO CO04066834A patent/CO5590949A2/es not_active Application Discontinuation
Also Published As
| Publication number | Publication date |
|---|---|
| BR0215355A (pt) | 2004-12-14 |
| ZA200405073B (en) | 2005-08-31 |
| RU2316529C2 (ru) | 2008-02-10 |
| NO20016374D0 (no) | 2001-12-27 |
| NO20016374L (no) | 2003-06-30 |
| JP4138661B2 (ja) | 2008-08-27 |
| ATE371635T1 (de) | 2007-09-15 |
| EP1458660A1 (de) | 2004-09-22 |
| CA2469783C (en) | 2008-02-12 |
| RU2004119560A (ru) | 2006-01-10 |
| KR20040077691A (ko) | 2004-09-06 |
| CA2469783A1 (en) | 2003-07-10 |
| BR0215355B1 (pt) | 2011-10-04 |
| EP1458660B1 (de) | 2007-08-29 |
| CO5590949A2 (es) | 2005-12-30 |
| PT1458660E (pt) | 2007-12-06 |
| JP2005512937A (ja) | 2005-05-12 |
| AU2002347688A1 (en) | 2003-07-15 |
| ES2292828T3 (es) | 2008-03-16 |
| DE60222174T2 (de) | 2008-06-12 |
| WO2003055830A1 (en) | 2003-07-10 |
| AU2002347688B2 (en) | 2007-06-07 |
| DE60222174D1 (de) | 2007-10-11 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MK1K | Patent expired |