NO20015042L - Fremgangsmåter for fremstilling av optisk aktive aminosyrederivater - Google Patents

Fremgangsmåter for fremstilling av optisk aktive aminosyrederivater

Info

Publication number
NO20015042L
NO20015042L NO20015042A NO20015042A NO20015042L NO 20015042 L NO20015042 L NO 20015042L NO 20015042 A NO20015042 A NO 20015042A NO 20015042 A NO20015042 A NO 20015042A NO 20015042 L NO20015042 L NO 20015042L
Authority
NO
Norway
Prior art keywords
optically active
derivative
amino acid
nitrated
benzenesulfonyl
Prior art date
Application number
NO20015042A
Other languages
English (en)
Other versions
NO20015042D0 (no
Inventor
Masanobu Sugawara
Akio Fujii
Kazumi Okuro
Yasuhiro Saka
Nobuo Nagashima
Kenji Inoue
Toshihiro Takeda
Koichi Kinoshita
Tadashi Moroshima
Yoshihide Fuse
Yasuyoshi Ueda
Original Assignee
Kaneka Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kaneka Corp filed Critical Kaneka Corp
Publication of NO20015042D0 publication Critical patent/NO20015042D0/no
Publication of NO20015042L publication Critical patent/NO20015042L/no

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D203/00—Heterocyclic compounds containing three-membered rings with one nitrogen atom as the only ring hetero atom
    • C07D203/04—Heterocyclic compounds containing three-membered rings with one nitrogen atom as the only ring hetero atom not condensed with other rings
    • C07D203/06—Heterocyclic compounds containing three-membered rings with one nitrogen atom as the only ring hetero atom not condensed with other rings having no double bonds between ring members or between ring members and non-ring members
    • C07D203/08—Heterocyclic compounds containing three-membered rings with one nitrogen atom as the only ring hetero atom not condensed with other rings having no double bonds between ring members or between ring members and non-ring members with only hydrogen atoms, hydrocarbon or substituted hydrocarbon radicals, directly attached to the ring nitrogen atom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/04—Formation of amino groups in compounds containing carboxyl groups
    • C07C227/10—Formation of amino groups in compounds containing carboxyl groups with simultaneously increasing the number of carbon atoms in the carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/30—Preparation of optical isomers
    • C07C227/32—Preparation of optical isomers by stereospecific synthesis
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/38—Separation; Purification; Stabilisation; Use of additives
    • C07C227/40—Separation; Purification
    • C07C227/42—Crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C229/30—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and unsaturated
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/36—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D203/00—Heterocyclic compounds containing three-membered rings with one nitrogen atom as the only ring hetero atom
    • C07D203/04—Heterocyclic compounds containing three-membered rings with one nitrogen atom as the only ring hetero atom not condensed with other rings
    • C07D203/06—Heterocyclic compounds containing three-membered rings with one nitrogen atom as the only ring hetero atom not condensed with other rings having no double bonds between ring members or between ring members and non-ring members
    • C07D203/16—Heterocyclic compounds containing three-membered rings with one nitrogen atom as the only ring hetero atom not condensed with other rings having no double bonds between ring members or between ring members and non-ring members with acylated ring nitrogen atoms
    • C07D203/20—Heterocyclic compounds containing three-membered rings with one nitrogen atom as the only ring hetero atom not condensed with other rings having no double bonds between ring members or between ring members and non-ring members with acylated ring nitrogen atoms by carbonic acid, or by sulfur or nitrogen analogues thereof, e.g. carbamates
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D203/00—Heterocyclic compounds containing three-membered rings with one nitrogen atom as the only ring hetero atom
    • C07D203/04—Heterocyclic compounds containing three-membered rings with one nitrogen atom as the only ring hetero atom not condensed with other rings
    • C07D203/06—Heterocyclic compounds containing three-membered rings with one nitrogen atom as the only ring hetero atom not condensed with other rings having no double bonds between ring members or between ring members and non-ring members
    • C07D203/22—Heterocyclic compounds containing three-membered rings with one nitrogen atom as the only ring hetero atom not condensed with other rings having no double bonds between ring members or between ring members and non-ring members with hetero atoms directly attached to the ring nitrogen atom
    • C07D203/24—Sulfur atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/07—Optical isomers

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Et optisk aktivt aminosyrederivat fremstilles ved enten å underkaste et optisk aktivt 3-haloalaninderivat (1) for N- beskyttelse, etterfulgt av cyklisering eller cyklisering etterfulgt av en N-beskyttelse for å fremstille et optisk aktivt aziridinkarboksylsyrederivat (3), hvis iminogruppe er beskyttet med 2- og/eller 4-nitrert benzensulfonyl og behandle dette derivat (3) med et organometallreagens eller ved å underkaste et optisk aktivt 3-haloalaninderivat for N- beskyttelse for å oppnå et optisk aktivt 3-haloalaninderivat (4), hvis aminogruppe er beskyttet med 2- og/eller 4-nitrert benzensulfonyl, og behandle dette derivat (4) med et organometallreagens. I henhold til en slik fremgangsmåte, kan naturlige og ikke-naturlige optisk aktive aminosyrer fremstilles fra billige råmaterialer ved hjelp av en enkel og lett operasjon. I nevnte derivater er X halogen, R1 og R2 er hver hydrogen eller lignende, * representerer et asymmetrisk karbonatom og P1 er 2- og/eller 4-nitrert benzensulfonyl.
NO20015042A 2000-02-17 2001-10-16 Fremgangsmåter for fremstilling av optisk aktive aminosyrederivater NO20015042L (no)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2000039415 2000-02-17
JP2000334391 2000-11-01
PCT/JP2001/001132 WO2001060795A1 (fr) 2000-02-17 2001-02-16 Procedes pour preparer des derives d'aminoacides a activite optique

Publications (2)

Publication Number Publication Date
NO20015042D0 NO20015042D0 (no) 2001-10-16
NO20015042L true NO20015042L (no) 2001-12-14

Family

ID=26585550

Family Applications (1)

Application Number Title Priority Date Filing Date
NO20015042A NO20015042L (no) 2000-02-17 2001-10-16 Fremgangsmåter for fremstilling av optisk aktive aminosyrederivater

Country Status (10)

Country Link
US (2) US6720449B2 (no)
EP (1) EP1179530A4 (no)
KR (1) KR20020006703A (no)
AU (1) AU3232701A (no)
CA (1) CA2369678A1 (no)
CZ (1) CZ20014121A3 (no)
HU (1) HUP0201353A3 (no)
NO (1) NO20015042L (no)
PL (1) PL350362A1 (no)
WO (1) WO2001060795A1 (no)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TW373123B (en) 1996-07-26 1999-11-01 Merck Patent Gmbh Combination of optical elements, means to produce substantially linear polarized light, optical retardation film and liquid crystal display device
AU2001286230A1 (en) * 2000-09-14 2002-03-26 Kaneka Corporation Process for the removal of nitrobenzenesulfonyl
CN108752253B (zh) * 2018-06-27 2020-11-24 深圳市茵诺圣生物科技有限公司 一种多元氮杂环状非天然手性氨基酸及其合成方法
CN114942295B (zh) * 2022-04-28 2023-12-22 上海市食品药品检验研究院 一种化妆品中总亚硝胺的提取方法及检测方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB847205A (en) 1957-10-25 1960-09-07 Hoffmann La Roche A process for the manufacture of ethylenimine derivatives and novel ethylenimine derivatives
JPS5414669B2 (no) 1973-09-03 1979-06-08
JPS6039357B2 (ja) 1981-03-09 1985-09-05 三井東圧化学株式会社 アジリジン−２−カルボン酸塩の製造法
EP0078853B1 (en) 1981-05-18 1985-11-13 MITSUI TOATSU CHEMICALS, Inc. Process for preparing beta-chloroalanine
EP0191462A1 (en) * 1985-02-13 1986-08-20 Research Association For Utilization Of Light Oil Purification of aziridine-2-carboxylic acid salts
JPH07138281A (ja) 1993-11-12 1995-05-30 Takeda Chem Ind Ltd 呈味関連物質のリチウム塩およびその用途
JP3551735B2 (ja) 1997-12-05 2004-08-11 住友化学工業株式会社 光学活性アゼチジン−２−カルボン酸の製造方法

Also Published As

Publication number Publication date
EP1179530A4 (en) 2005-07-27
CZ20014121A3 (cs) 2002-10-16
HUP0201353A3 (en) 2003-01-28
US20050143586A1 (en) 2005-06-30
KR20020006703A (ko) 2002-01-24
NO20015042D0 (no) 2001-10-16
US20030032814A1 (en) 2003-02-13
US7109352B2 (en) 2006-09-19
US6720449B2 (en) 2004-04-13
PL350362A1 (en) 2002-12-02
WO2001060795A1 (fr) 2001-08-23
EP1179530A1 (en) 2002-02-13
HUP0201353A2 (en) 2002-08-28
AU3232701A (en) 2001-08-27
CA2369678A1 (en) 2001-08-23

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