NO134294B - - Google Patents
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- Publication number
- NO134294B NO134294B NO593/71A NO59371A NO134294B NO 134294 B NO134294 B NO 134294B NO 593/71 A NO593/71 A NO 593/71A NO 59371 A NO59371 A NO 59371A NO 134294 B NO134294 B NO 134294B
- Authority
- NO
- Norway
- Prior art keywords
- lime
- zone
- pipe
- reaction
- mixture
- Prior art date
Links
- 235000008733 Citrus aurantifolia Nutrition 0.000 claims description 32
- 235000011941 Tilia x europaea Nutrition 0.000 claims description 32
- 239000004571 lime Substances 0.000 claims description 32
- 239000007788 liquid Substances 0.000 claims description 32
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 30
- 239000000203 mixture Substances 0.000 claims description 28
- 238000006243 chemical reaction Methods 0.000 claims description 26
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 22
- 238000000034 method Methods 0.000 claims description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 14
- 239000000376 reactant Substances 0.000 claims description 10
- 239000003054 catalyst Substances 0.000 claims description 9
- 239000011541 reaction mixture Substances 0.000 claims description 8
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims description 7
- 239000000920 calcium hydroxide Substances 0.000 claims description 7
- 229910001861 calcium hydroxide Inorganic materials 0.000 claims description 7
- 235000011116 calcium hydroxide Nutrition 0.000 claims description 7
- 239000000463 material Substances 0.000 claims description 7
- 239000000377 silicon dioxide Substances 0.000 claims description 7
- 235000012239 silicon dioxide Nutrition 0.000 claims description 7
- 239000002250 absorbent Substances 0.000 claims description 5
- 230000002745 absorbent Effects 0.000 claims description 5
- 238000009833 condensation Methods 0.000 claims description 5
- 230000005494 condensation Effects 0.000 claims description 5
- 125000004432 carbon atom Chemical group C* 0.000 claims description 4
- 238000010924 continuous production Methods 0.000 claims description 3
- 239000007787 solid Substances 0.000 claims description 3
- 229910001860 alkaline earth metal hydroxide Inorganic materials 0.000 claims description 2
- 238000001816 cooling Methods 0.000 claims description 2
- 238000006073 displacement reaction Methods 0.000 claims description 2
- 125000002485 formyl group Chemical class [H]C(*)=O 0.000 claims description 2
- 238000010438 heat treatment Methods 0.000 claims description 2
- 239000011949 solid catalyst Substances 0.000 claims description 2
- 239000012876 carrier material Substances 0.000 description 14
- 150000001299 aldehydes Chemical class 0.000 description 9
- HGINCPLSRVDWNT-UHFFFAOYSA-N Acrolein Chemical compound C=CC=O HGINCPLSRVDWNT-UHFFFAOYSA-N 0.000 description 8
- 238000009826 distribution Methods 0.000 description 7
- 238000004821 distillation Methods 0.000 description 6
- 229910002012 Aerosil® Inorganic materials 0.000 description 5
- 239000007795 chemical reaction product Substances 0.000 description 5
- STNJBCKSHOAVAJ-UHFFFAOYSA-N Methacrolein Chemical compound CC(=C)C=O STNJBCKSHOAVAJ-UHFFFAOYSA-N 0.000 description 4
- 238000009835 boiling Methods 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 150000001412 amines Chemical class 0.000 description 3
- 239000003153 chemical reaction reagent Substances 0.000 description 3
- 150000002500 ions Chemical class 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- HSCUZOQCNBPBST-UHFFFAOYSA-N 2-methoxy-2-methylpropanal Chemical compound COC(C)(C)C=O HSCUZOQCNBPBST-UHFFFAOYSA-N 0.000 description 2
- CERVLVANLTVGSM-UHFFFAOYSA-N 2-methoxybutanal Chemical compound CCC(OC)C=O CERVLVANLTVGSM-UHFFFAOYSA-N 0.000 description 2
- -1 amine salt Chemical class 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000006482 condensation reaction Methods 0.000 description 2
- 230000001419 dependent effect Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- GMLDCZYTIPCVMO-UHFFFAOYSA-N 2-methylidenebutanal Chemical compound CCC(=C)C=O GMLDCZYTIPCVMO-UHFFFAOYSA-N 0.000 description 1
- MMHMXZCCWWPBJL-UHFFFAOYSA-N 4-methoxy-2-methylbutanal Chemical compound COCCC(C)C=O MMHMXZCCWWPBJL-UHFFFAOYSA-N 0.000 description 1
- 229910002016 Aerosil® 200 Inorganic materials 0.000 description 1
- 229910002019 Aerosil® 380 Inorganic materials 0.000 description 1
- 101100277337 Arabidopsis thaliana DDM1 gene Proteins 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 150000001335 aliphatic alkanes Chemical class 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 229910000288 alkali metal carbonate Inorganic materials 0.000 description 1
- 150000008041 alkali metal carbonates Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 239000012295 chemical reaction liquid Substances 0.000 description 1
- 101150113676 chr1 gene Proteins 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- MLUCVPSAIODCQM-NSCUHMNNSA-N crotonaldehyde Chemical compound C\C=C\C=O MLUCVPSAIODCQM-NSCUHMNNSA-N 0.000 description 1
- MLUCVPSAIODCQM-UHFFFAOYSA-N crotonaldehyde Natural products CC=CC=O MLUCVPSAIODCQM-UHFFFAOYSA-N 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 150000001983 dialkylethers Chemical class 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000010828 elution Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 239000012263 liquid product Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000012429 reaction media Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 239000000741 silica gel Substances 0.000 description 1
- 229910002027 silica gel Inorganic materials 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 150000003512 tertiary amines Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
- C07C45/67—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton
- C07C45/68—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms
- C07C45/70—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms by reaction with functional groups containing oxygen only in singly bound form
- C07C45/71—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms by reaction with functional groups containing oxygen only in singly bound form being hydroxy groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7015829A FR2088940A5 (cs) | 1970-04-30 | 1970-04-30 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| NO134294B true NO134294B (cs) | 1976-06-08 |
| NO134294C NO134294C (cs) | 1976-09-15 |
Family
ID=9054898
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO593/71A NO134294C (cs) | 1970-04-30 | 1971-02-18 |
Country Status (15)
| Country | Link |
|---|---|
| US (1) | US3795643A (cs) |
| JP (1) | JPS5010844B1 (cs) |
| AT (1) | AT306690B (cs) |
| BE (1) | BE766489A (cs) |
| CA (1) | CA941385A (cs) |
| CH (1) | CH539010A (cs) |
| CS (1) | CS158692B2 (cs) |
| ES (1) | ES390607A1 (cs) |
| FR (1) | FR2088940A5 (cs) |
| GB (1) | GB1289264A (cs) |
| NL (1) | NL7102482A (cs) |
| NO (1) | NO134294C (cs) |
| PL (1) | PL81603B1 (cs) |
| RO (1) | RO61777A (cs) |
| SE (1) | SE364253B (cs) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4499308A (en) * | 1983-12-05 | 1985-02-12 | The Standard Oil Company | Catalytic reaction of acrolein and methacrolein with alcohols and glycols |
-
1970
- 1970-04-30 FR FR7015829A patent/FR2088940A5/fr not_active Expired
-
1971
- 1971-02-09 CS CS93771*#A patent/CS158692B2/cs unknown
- 1971-02-18 NO NO593/71A patent/NO134294C/no unknown
- 1971-02-25 NL NL7102482A patent/NL7102482A/xx not_active Application Discontinuation
- 1971-03-15 JP JP46014345A patent/JPS5010844B1/ja active Pending
- 1971-03-23 SE SE03781/71A patent/SE364253B/xx unknown
- 1971-03-25 US US00128016A patent/US3795643A/en not_active Expired - Lifetime
- 1971-03-30 CA CA109,126A patent/CA941385A/en not_active Expired
- 1971-04-19 GB GB1289264D patent/GB1289264A/en not_active Expired
- 1971-04-21 AT AT339271A patent/AT306690B/de not_active IP Right Cessation
- 1971-04-26 ES ES390607A patent/ES390607A1/es not_active Expired
- 1971-04-28 PL PL1971147803A patent/PL81603B1/pl unknown
- 1971-04-29 BE BE766489A patent/BE766489A/xx unknown
- 1971-04-29 CH CH634971A patent/CH539010A/fr not_active IP Right Cessation
- 1971-04-30 RO RO66768A patent/RO61777A/ro unknown
Also Published As
| Publication number | Publication date |
|---|---|
| US3795643A (en) | 1974-03-05 |
| JPS5010844B1 (cs) | 1975-04-24 |
| SE364253B (cs) | 1974-02-18 |
| BE766489A (fr) | 1971-10-29 |
| PL81603B1 (cs) | 1975-08-30 |
| NL7102482A (cs) | 1971-11-02 |
| NO134294C (cs) | 1976-09-15 |
| CH539010A (fr) | 1973-07-15 |
| DE2106174A1 (de) | 1972-06-15 |
| AT306690B (de) | 1973-04-25 |
| FR2088940A5 (cs) | 1972-01-07 |
| CS158692B2 (cs) | 1974-11-25 |
| CA941385A (en) | 1974-02-05 |
| GB1289264A (cs) | 1972-09-13 |
| RO61777A (cs) | 1977-05-15 |
| ES390607A1 (es) | 1974-04-01 |
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