NO115554B - - Google Patents
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- Publication number
- NO115554B NO115554B NO155723A NO15572364A NO115554B NO 115554 B NO115554 B NO 115554B NO 155723 A NO155723 A NO 155723A NO 15572364 A NO15572364 A NO 15572364A NO 115554 B NO115554 B NO 115554B
- Authority
- NO
- Norway
- Prior art keywords
- polymers
- weight
- polymerization
- monomer
- polymer
- Prior art date
Links
- 229920000642 polymer Polymers 0.000 claims description 38
- 239000000178 monomer Substances 0.000 claims description 28
- 238000000034 method Methods 0.000 claims description 26
- 238000006116 polymerization reaction Methods 0.000 claims description 22
- DKGAVHZHDRPRBM-UHFFFAOYSA-N Tert-Butanol Chemical compound CC(C)(C)O DKGAVHZHDRPRBM-UHFFFAOYSA-N 0.000 claims description 11
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 claims description 9
- 239000000203 mixture Substances 0.000 claims description 8
- 238000004519 manufacturing process Methods 0.000 claims description 6
- 239000011541 reaction mixture Substances 0.000 claims description 6
- 229920003169 water-soluble polymer Polymers 0.000 claims description 6
- 150000003926 acrylamides Chemical class 0.000 claims description 3
- ZQXSFZAMFNRZOQ-UHFFFAOYSA-N 2-methylpropan-2-ol;hydrate Chemical compound O.CC(C)(C)O ZQXSFZAMFNRZOQ-UHFFFAOYSA-N 0.000 claims description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 2
- 125000000217 alkyl group Chemical group 0.000 claims description 2
- 239000001257 hydrogen Substances 0.000 claims description 2
- 229910052739 hydrogen Inorganic materials 0.000 claims description 2
- 239000002244 precipitate Substances 0.000 claims description 2
- 239000002904 solvent Substances 0.000 description 13
- 239000003999 initiator Substances 0.000 description 11
- 239000000047 product Substances 0.000 description 10
- 239000000243 solution Substances 0.000 description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 239000012190 activator Substances 0.000 description 5
- 238000005259 measurement Methods 0.000 description 5
- -1 vinyl sodium carboxylates Chemical class 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical group C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 4
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 4
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 4
- 229920002554 vinyl polymer Polymers 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- 239000000499 gel Substances 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- USHAGKDGDHPEEY-UHFFFAOYSA-L potassium persulfate Chemical compound [K+].[K+].[O-]S(=O)(=O)OOS([O-])(=O)=O USHAGKDGDHPEEY-UHFFFAOYSA-L 0.000 description 3
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 3
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 2
- 239000004159 Potassium persulphate Substances 0.000 description 2
- ROOXNKNUYICQNP-UHFFFAOYSA-N ammonium persulfate Chemical compound [NH4+].[NH4+].[O-]S(=O)(=O)OOS([O-])(=O)=O ROOXNKNUYICQNP-UHFFFAOYSA-N 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 229920001577 copolymer Polymers 0.000 description 2
- 238000004090 dissolution Methods 0.000 description 2
- 239000007863 gel particle Substances 0.000 description 2
- 239000012442 inert solvent Substances 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 239000003505 polymerization initiator Substances 0.000 description 2
- 235000011164 potassium chloride Nutrition 0.000 description 2
- 239000001103 potassium chloride Substances 0.000 description 2
- 235000019394 potassium persulphate Nutrition 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- PQUXFUBNSYCQAL-UHFFFAOYSA-N 1-(2,3-difluorophenyl)ethanone Chemical compound CC(=O)C1=CC=CC(F)=C1F PQUXFUBNSYCQAL-UHFFFAOYSA-N 0.000 description 1
- WDRZVZVXHZNSFG-UHFFFAOYSA-N 1-ethenylpyridin-1-ium Chemical class C=C[N+]1=CC=CC=C1 WDRZVZVXHZNSFG-UHFFFAOYSA-N 0.000 description 1
- OZAIFHULBGXAKX-UHFFFAOYSA-N 2-(2-cyanopropan-2-yldiazenyl)-2-methylpropanenitrile Chemical compound N#CC(C)(C)N=NC(C)(C)C#N OZAIFHULBGXAKX-UHFFFAOYSA-N 0.000 description 1
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- YQUDMNIUBTXLSX-UHFFFAOYSA-N 2-ethenyl-5-ethylpyridine Chemical compound CCC1=CC=C(C=C)N=C1 YQUDMNIUBTXLSX-UHFFFAOYSA-N 0.000 description 1
- KGIGUEBEKRSTEW-UHFFFAOYSA-N 2-vinylpyridine Chemical compound C=CC1=CC=CC=N1 KGIGUEBEKRSTEW-UHFFFAOYSA-N 0.000 description 1
- KFDVPJUYSDEJTH-UHFFFAOYSA-N 4-ethenylpyridine Chemical compound C=CC1=CC=NC=C1 KFDVPJUYSDEJTH-UHFFFAOYSA-N 0.000 description 1
- XKIGDOOFWYHZDA-UHFFFAOYSA-M 5-ethenyl-1,2-dimethylpyridin-1-ium;methyl sulfate Chemical compound COS([O-])(=O)=O.CC1=CC=C(C=C)C=[N+]1C XKIGDOOFWYHZDA-UHFFFAOYSA-M 0.000 description 1
- VJOWMORERYNYON-UHFFFAOYSA-N 5-ethenyl-2-methylpyridine Chemical compound CC1=CC=C(C=C)C=N1 VJOWMORERYNYON-UHFFFAOYSA-N 0.000 description 1
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 description 1
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 1
- DWAQJAXMDSEUJJ-UHFFFAOYSA-M Sodium bisulfite Chemical compound [Na+].OS([O-])=O DWAQJAXMDSEUJJ-UHFFFAOYSA-M 0.000 description 1
- 229940048053 acrylate Drugs 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 229910001870 ammonium persulfate Inorganic materials 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 125000002843 carboxylic acid group Chemical group 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 229920006037 cross link polymer Polymers 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 239000011243 crosslinked material Substances 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 238000006073 displacement reaction Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- QDXBVEACAWKSFL-UHFFFAOYSA-N ethenethiol Chemical class SC=C QDXBVEACAWKSFL-UHFFFAOYSA-N 0.000 description 1
- 238000009950 felting Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 229920006158 high molecular weight polymer Polymers 0.000 description 1
- 239000012456 homogeneous solution Substances 0.000 description 1
- 229920001519 homopolymer Polymers 0.000 description 1
- 230000006698 induction Effects 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- FQPSGWSUVKBHSU-UHFFFAOYSA-N methacrylamide Chemical compound CC(=C)C(N)=O FQPSGWSUVKBHSU-UHFFFAOYSA-N 0.000 description 1
- JZMJDSHXVKJFKW-UHFFFAOYSA-M methyl sulfate(1-) Chemical compound COS([O-])(=O)=O JZMJDSHXVKJFKW-UHFFFAOYSA-M 0.000 description 1
- 230000000379 polymerizing effect Effects 0.000 description 1
- 150000003242 quaternary ammonium salts Chemical class 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 150000003839 salts Chemical group 0.000 description 1
- 229940047670 sodium acrylate Drugs 0.000 description 1
- 235000010267 sodium hydrogen sulphite Nutrition 0.000 description 1
- 239000004289 sodium hydrogen sulphite Substances 0.000 description 1
- SONHXMAHPHADTF-UHFFFAOYSA-M sodium;2-methylprop-2-enoate Chemical compound [Na+].CC(=C)C([O-])=O SONHXMAHPHADTF-UHFFFAOYSA-M 0.000 description 1
- BWYYYTVSBPRQCN-UHFFFAOYSA-M sodium;ethenesulfonate Chemical compound [Na+].[O-]S(=O)(=O)C=C BWYYYTVSBPRQCN-UHFFFAOYSA-M 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F20/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride, ester, amide, imide or nitrile thereof
- C08F20/02—Monocarboxylic acids having less than ten carbon atoms, Derivatives thereof
- C08F20/52—Amides or imides
- C08F20/54—Amides, e.g. N,N-dimethylacrylamide or N-isopropylacrylamide
- C08F20/56—Acrylamide; Methacrylamide
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Polymerisation Methods In General (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US358069A US3336269A (en) | 1964-04-07 | 1964-04-07 | Preparation of acrylamide-type water-soluble polymers |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| NO115554B true NO115554B (xx) | 1968-10-21 |
Family
ID=23408163
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO155723A NO115554B (xx) | 1964-04-07 | 1964-11-25 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US3336269A (xx) |
| JP (1) | JPS5230544B1 (xx) |
| DE (1) | DE1301079C2 (xx) |
| FI (1) | FI44062B (xx) |
| GB (1) | GB1083198A (xx) |
| NL (1) | NL142171B (xx) |
| NO (1) | NO115554B (xx) |
| SE (1) | SE333061B (xx) |
Families Citing this family (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3509113A (en) * | 1967-08-14 | 1970-04-28 | Hercules Inc | Preparation of acrylamide-type water-soluble polymers |
| US3779917A (en) * | 1971-11-26 | 1973-12-18 | Marathon Oil Co | Oil recovery with vinyl sulfonic acid-acrylamide copolymers |
| US3868260A (en) * | 1972-04-13 | 1975-02-25 | Warner Lambert Co | Denture adhesive preparation |
| US3868340A (en) * | 1972-04-13 | 1975-02-25 | Warner Lambert Co | Denture adhesive preparation |
| JPS5146154B2 (xx) * | 1972-05-11 | 1976-12-07 | ||
| US3926870A (en) * | 1973-10-15 | 1975-12-16 | Warner Lambert Co | Denture adhesive preparation containing an anionic protein material |
| US3878135A (en) * | 1973-10-15 | 1975-04-15 | Warner Lambert Co | Denture adhesive preparation containing an anionic protein material |
| JPS5246276B2 (xx) * | 1974-01-16 | 1977-11-22 | ||
| US4077930A (en) * | 1974-07-16 | 1978-03-07 | Calgon Corporation | Self-inverting emulsions of dialkyldiallyl ammonium chloride polymers and copolymers |
| DE2545007B2 (de) * | 1975-10-08 | 1977-08-11 | Wolff Walsrode Ag, 3030 Walsrode | Lineares, hochmolekulares acrylamid-homopolymerisat und seine verwendung als hilfsmittel zur verbesserung der retention, entwaesserung und aufbereitung |
| US4147681A (en) * | 1976-02-24 | 1979-04-03 | Calgon Corporation | Stable, self-inverting water-in-oil emulsions |
| JPS52127989A (en) * | 1976-04-19 | 1977-10-27 | Mitsubishi Rayon Co Ltd | Aerobic compositions |
| US4267103A (en) * | 1978-12-07 | 1981-05-12 | The B. F. Goodrich Company | Solvent polymerization of carboxyl containing monomers |
| US4355073A (en) * | 1979-06-26 | 1982-10-19 | Scott Bader Company Limited | Adhesive coatings of prepasted wall coverings |
| US4396513A (en) * | 1981-09-08 | 1983-08-02 | Betz Laboratories, Inc. | Use of very high charge cationic polymers in biological sludge dewatering |
| US5080809A (en) * | 1983-01-28 | 1992-01-14 | Phillips Petroleum Company | Polymers useful in the recovery and processing of natural resources |
| US5186257A (en) * | 1983-01-28 | 1993-02-16 | Phillips Petroleum Company | Polymers useful in the recovery and processing of natural resources |
| US4544722A (en) * | 1983-09-09 | 1985-10-01 | Nalco Chemical Company | Water-soluble terpolymers of 2-acrylamido-2-methylpropane-sulfonic acid, sodium salt (AMPS), n-vinylpyrrolidone and acrylonitrile |
| DE3427220A1 (de) * | 1984-07-24 | 1986-01-30 | Cassella Ag, 6000 Frankfurt | Verfahren zur herstellung von copolymeren |
| US4988568A (en) * | 1988-03-30 | 1991-01-29 | Nippon Zeon Co., Ltd. | Hydrophilic fine gel particles and process for production thereof |
| AU1692392A (en) * | 1991-04-01 | 1992-11-02 | Isp Investments Inc. | Precipitation polymerization process |
| JPH0635678U (ja) * | 1992-10-19 | 1994-05-13 | ジャトコ株式会社 | 多板クラッチ |
| FR2756830B1 (fr) * | 1996-12-09 | 1999-02-26 | Atochem Elf Sa | Polymeres hydrophiles fluores |
| US6016872A (en) * | 1997-03-17 | 2000-01-25 | Forta Corporation | Method for removing debris from a well-bore |
| FR2779436B1 (fr) * | 1998-06-03 | 2000-07-07 | Atochem Elf Sa | Polymeres hydrophiles fluores |
| US6258275B1 (en) * | 1999-10-01 | 2001-07-10 | Ecole Polytechnique Federale De Lausanne | Affinity macroligands |
| RU2537401C1 (ru) * | 2013-08-20 | 2015-01-10 | Федеральное государственное бюджетное учреждение Национальный исследовательский центр "Курчатовский институт" | Способ получения геля (со)полимеров акриловой кислоты и акриламида |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE468665A (xx) * | 1945-10-16 | |||
| BE476083A (xx) * | 1946-07-22 | |||
| US2764578A (en) * | 1952-04-18 | 1956-09-25 | Du Pont | Vinyloxyalkyl quaternary ammonium copolymers |
| GB757770A (en) * | 1953-08-22 | 1956-09-26 | Basf Ag | Improvements in the production of water-soluble polymers |
| US3008851A (en) * | 1955-03-21 | 1961-11-14 | Rohm & Haas | Novel quaternary ammonium compounds and methods of producing them |
| US3040012A (en) * | 1957-04-07 | 1962-06-19 | Ciba Ltd | New polymerization process of basic compounds |
| US2972535A (en) * | 1957-09-03 | 1961-02-21 | Eastman Kodak Co | Quaternary salts of c-vinylpyridine polymers with compounds containing a haloacetyl group |
| DE1495645C3 (de) * | 1961-05-26 | 1974-11-07 | Bayer Ag, 5090 Leverkusen | Verfahren zur Herstellung stabiler, wäßriger Emulsionen bzw. Dispersionen von Äthylen-Mischpolymerisaten |
| US3235490A (en) * | 1962-07-12 | 1966-02-15 | Kerr Mc Gee Oil Ind Inc | Process for flocculating and settling solids suspended in an aqueous medium and composition for use therein |
| US3254138A (en) * | 1963-09-12 | 1966-05-31 | Eastman Kodak Co | Graft copolymers of acrylonitrile onto a homopolymeric polyamide having n-alkyl substitution |
-
1964
- 1964-04-07 US US358069A patent/US3336269A/en not_active Expired - Lifetime
- 1964-11-25 NO NO155723A patent/NO115554B/no unknown
- 1964-11-30 GB GB48652/64A patent/GB1083198A/en not_active Expired
- 1964-12-11 FI FI2626/64A patent/FI44062B/fi active
-
1965
- 1965-01-19 DE DE1965H0054905 patent/DE1301079C2/de not_active Expired
- 1965-02-24 JP JP40010234A patent/JPS5230544B1/ja active Pending
- 1965-04-07 SE SE04543/65A patent/SE333061B/xx unknown
- 1965-04-07 NL NL656504429A patent/NL142171B/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| FI44062B (xx) | 1971-04-30 |
| SE333061B (xx) | 1971-03-01 |
| GB1083198A (en) | 1967-09-13 |
| NL6504429A (xx) | 1965-10-08 |
| DE1301079B (de) | 1969-08-14 |
| NL142171B (nl) | 1974-05-15 |
| DE1301079C2 (de) | 1975-07-10 |
| JPS5230544B1 (xx) | 1977-08-09 |
| US3336269A (en) | 1967-08-15 |
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