NL146150B - Werkwijze voor de bereiding van 2-butyl-n,n'-difenyl-malonzuur-monohydrazide en de calcium-, magnesium- en aluminiumzouten daarvan. - Google Patents
Werkwijze voor de bereiding van 2-butyl-n,n'-difenyl-malonzuur-monohydrazide en de calcium-, magnesium- en aluminiumzouten daarvan.Info
- Publication number
- NL146150B NL146150B NL7115546A NL7115546A NL146150B NL 146150 B NL146150 B NL 146150B NL 7115546 A NL7115546 A NL 7115546A NL 7115546 A NL7115546 A NL 7115546A NL 146150 B NL146150 B NL 146150B
- Authority
- NL
- Netherlands
- Prior art keywords
- salt
- alkali metal
- water
- monohydrazide
- metal salt
- Prior art date
Links
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 title abstract 5
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 title abstract 5
- 239000011575 calcium Substances 0.000 title abstract 5
- 229910052791 calcium Inorganic materials 0.000 title abstract 5
- 239000011777 magnesium Substances 0.000 title abstract 5
- 229910052749 magnesium Inorganic materials 0.000 title abstract 5
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 title 1
- FLWFHHFTIRLFPV-UHFFFAOYSA-N bumadizone Chemical compound C=1C=CC=CC=1N(C(=O)C(C(O)=O)CCCC)NC1=CC=CC=C1 FLWFHHFTIRLFPV-UHFFFAOYSA-N 0.000 title 1
- 229910052783 alkali metal Inorganic materials 0.000 abstract 8
- 150000003839 salts Chemical class 0.000 abstract 8
- -1 alkali metal salt Chemical class 0.000 abstract 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 6
- 239000003960 organic solvent Substances 0.000 abstract 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 3
- 159000000013 aluminium salts Chemical class 0.000 abstract 3
- 229910000329 aluminium sulfate Inorganic materials 0.000 abstract 3
- 230000007935 neutral effect Effects 0.000 abstract 3
- 229910052757 nitrogen Inorganic materials 0.000 abstract 3
- USPWKWBDZOARPV-UHFFFAOYSA-N pyrazolidine Chemical compound C1CNNC1 USPWKWBDZOARPV-UHFFFAOYSA-N 0.000 abstract 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract 2
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 abstract 2
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 abstract 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 abstract 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 abstract 2
- 150000008044 alkali metal hydroxides Chemical class 0.000 abstract 2
- 150000001340 alkali metals Chemical class 0.000 abstract 2
- 150000007522 mineralic acids Chemical class 0.000 abstract 2
- 150000007524 organic acids Chemical class 0.000 abstract 2
- 230000020477 pH reduction Effects 0.000 abstract 2
- 239000012266 salt solution Substances 0.000 abstract 2
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 abstract 1
- 239000012670 alkaline solution Substances 0.000 abstract 1
- 239000004411 aluminium Substances 0.000 abstract 1
- 229910052782 aluminium Inorganic materials 0.000 abstract 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 abstract 1
- BNIILDVGGAEEIG-UHFFFAOYSA-L disodium hydrogen phosphate Chemical compound [Na+].[Na+].OP([O-])([O-])=O BNIILDVGGAEEIG-UHFFFAOYSA-L 0.000 abstract 1
- 238000000605 extraction Methods 0.000 abstract 1
- 150000008282 halocarbons Chemical class 0.000 abstract 1
- 230000003301 hydrolyzing effect Effects 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 229910052751 metal Inorganic materials 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 239000012074 organic phase Substances 0.000 abstract 1
- VYMDGNCVAMGZFE-UHFFFAOYSA-N phenylbutazonum Chemical compound O=C1C(CCCC)C(=O)N(C=2C=CC=CC=2)N1C1=CC=CC=C1 VYMDGNCVAMGZFE-UHFFFAOYSA-N 0.000 abstract 1
- 239000001103 potassium chloride Substances 0.000 abstract 1
- 235000011164 potassium chloride Nutrition 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
- 238000010992 reflux Methods 0.000 abstract 1
- 239000001632 sodium acetate Substances 0.000 abstract 1
- 235000017281 sodium acetate Nutrition 0.000 abstract 1
- 239000011780 sodium chloride Substances 0.000 abstract 1
- 229910052938 sodium sulfate Inorganic materials 0.000 abstract 1
- 235000011152 sodium sulphate Nutrition 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C241/00—Preparation of compounds containing chains of nitrogen atoms singly-bound to each other, e.g. hydrazines, triazanes
- C07C241/04—Preparation of hydrazides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19702055845 DE2055845C3 (de) | 1970-11-13 | 1970-11-13 | Verfahren zur Herstellung von 2-Butyl-N.N'-diphenyl-malono-monohydrazid und seinen Calcium-, Magnesium- und Aluminiumsalzen |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| NL7115546A NL7115546A (enrdf_load_stackoverflow) | 1972-05-16 |
| NL146150B true NL146150B (nl) | 1975-06-16 |
Family
ID=5787984
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NL7115546A NL146150B (nl) | 1970-11-13 | 1971-11-12 | Werkwijze voor de bereiding van 2-butyl-n,n'-difenyl-malonzuur-monohydrazide en de calcium-, magnesium- en aluminiumzouten daarvan. |
Country Status (8)
| Country | Link |
|---|---|
| JP (1) | JPS5235653B1 (enrdf_load_stackoverflow) |
| BE (1) | BE775200A (enrdf_load_stackoverflow) |
| CA (1) | CA925875A (enrdf_load_stackoverflow) |
| CH (1) | CH563349A5 (enrdf_load_stackoverflow) |
| DE (1) | DE2055845C3 (enrdf_load_stackoverflow) |
| FR (1) | FR2114512A5 (enrdf_load_stackoverflow) |
| GB (1) | GB1355370A (enrdf_load_stackoverflow) |
| NL (1) | NL146150B (enrdf_load_stackoverflow) |
-
1970
- 1970-11-13 DE DE19702055845 patent/DE2055845C3/de not_active Expired
-
1971
- 1971-11-09 CH CH1629671A patent/CH563349A5/xx not_active IP Right Cessation
- 1971-11-10 CA CA127323A patent/CA925875A/en not_active Expired
- 1971-11-10 BE BE775200A patent/BE775200A/xx not_active IP Right Cessation
- 1971-11-10 GB GB5223171A patent/GB1355370A/en not_active Expired
- 1971-11-10 FR FR7140236A patent/FR2114512A5/fr not_active Expired
- 1971-11-12 NL NL7115546A patent/NL146150B/xx not_active IP Right Cessation
- 1971-11-12 JP JP46090504A patent/JPS5235653B1/ja active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5235653B1 (enrdf_load_stackoverflow) | 1977-09-10 |
| DE2055845B2 (de) | 1974-04-04 |
| DE2055845C3 (de) | 1974-11-07 |
| CH563349A5 (enrdf_load_stackoverflow) | 1975-06-30 |
| FR2114512A5 (enrdf_load_stackoverflow) | 1972-06-30 |
| GB1355370A (en) | 1974-06-05 |
| DE2055845A1 (de) | 1972-05-25 |
| BE775200A (fr) | 1972-05-10 |
| CA925875A (en) | 1973-05-08 |
| NL7115546A (enrdf_load_stackoverflow) | 1972-05-16 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| V1 | Lapsed because of non-payment of the annual fee | ||
| NL80 | Abbreviated name of patent owner mentioned of already nullified patent |
Owner name: BYK GULDEN |