MX9805188A - Cloracion selectiva de un 1-(2-fluoro-fenil)-1,2,4-triazol. - Google Patents
Cloracion selectiva de un 1-(2-fluoro-fenil)-1,2,4-triazol.Info
- Publication number
- MX9805188A MX9805188A MX9805188A MX9805188A MX9805188A MX 9805188 A MX9805188 A MX 9805188A MX 9805188 A MX9805188 A MX 9805188A MX 9805188 A MX9805188 A MX 9805188A MX 9805188 A MX9805188 A MX 9805188A
- Authority
- MX
- Mexico
- Prior art keywords
- fluorophenyl
- triazole
- dihydro
- oxo
- selective chlorination
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D249/00—Heterocyclic compounds containing five-membered rings having three nitrogen atoms as the only ring hetero atoms
- C07D249/02—Heterocyclic compounds containing five-membered rings having three nitrogen atoms as the only ring hetero atoms not condensed with other rings
- C07D249/08—1,2,4-Triazoles; Hydrogenated 1,2,4-triazoles
- C07D249/10—1,2,4-Triazoles; Hydrogenated 1,2,4-triazoles with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D249/12—Oxygen or sulfur atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Plural Heterocyclic Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
Abstract
Se describe un procedimiento en el que se clora la posicion 4 del grupo 1-(2-flurofenilo) unido a 4-5-dihidro-3-metil-5-oxo-1H-1,2,4-triazol, intermediario en la ruta para preparar el herbicida alfa-2-dicloro-5-[4-difluorometil)-4,5-dihidro-3-m etil-5-oxo-1H-1,2,4-triazol-1-il]-4-fluorobencenop ropanoato de etilo, en buen rendimiento. El procedimiento supone la adicion de gas cloro en tres etapas independientes eliminando el subproducto cloruro de hidrogeno al final de cada una de las etapas de adicion de cloro.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US932095P | 1995-12-29 | 1995-12-29 |
Publications (1)
Publication Number | Publication Date |
---|---|
MX9805188A true MX9805188A (es) | 1998-10-31 |
Family
ID=21736931
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MX9805188A MX9805188A (es) | 1995-12-29 | 1998-06-25 | Cloracion selectiva de un 1-(2-fluoro-fenil)-1,2,4-triazol. |
Country Status (18)
Country | Link |
---|---|
US (1) | US5965742A (es) |
EP (1) | EP0889882B1 (es) |
JP (1) | JP3802566B2 (es) |
KR (1) | KR100454802B1 (es) |
CN (1) | CN1067383C (es) |
AT (1) | ATE271549T1 (es) |
AU (1) | AU710982B2 (es) |
BR (1) | BR9612366A (es) |
CA (1) | CA2241632C (es) |
CZ (1) | CZ292185B6 (es) |
DE (1) | DE69632966T2 (es) |
ES (1) | ES2224185T3 (es) |
HK (1) | HK1017678A1 (es) |
HU (1) | HU225546B1 (es) |
MX (1) | MX9805188A (es) |
PL (1) | PL186048B1 (es) |
RU (1) | RU2167870C2 (es) |
WO (1) | WO1997024337A1 (es) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103965124A (zh) * | 2014-04-29 | 2014-08-06 | 安徽苏启化工有限公司 | 一种三唑啉酮合成方法 |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN85106905A (zh) * | 1985-08-08 | 1987-02-04 | Fmc公司 | 含有1-芳基-δ2-1,2,4,-三唑啉-5-酮类的除草剂及其制备方法 |
WO1988009617A1 (en) * | 1987-06-12 | 1988-12-15 | Fmc Corporation | 1-(4-chloro-2-fluoro-5-methoxyphenyl)-3-methyl-4-difluoromethyl-delta2-1,2,4-triazolin-5-one as herbicidal agent |
US5256793A (en) * | 1992-05-13 | 1993-10-26 | Fmc Corporation | Triazolinone ring formation in tert-butanol |
US5468868A (en) * | 1993-12-16 | 1995-11-21 | Fmc Corporation | Process for the selective chlorination of 4,5-dihydro-1-phenyl-1H-1,2,4-triazol-5-one |
US5438149A (en) * | 1994-05-27 | 1995-08-01 | Fmc Corporation | Difluoromethylation of a phenyl triazolinone |
US5449784A (en) * | 1994-06-22 | 1995-09-12 | Fmc Corporation | Method of preparing aryl triazolinones with trialkyl orthoacetates |
-
1996
- 1996-11-20 CN CN96198753A patent/CN1067383C/zh not_active Expired - Fee Related
- 1996-11-20 US US09/091,867 patent/US5965742A/en not_active Expired - Fee Related
- 1996-11-20 WO PCT/US1996/018600 patent/WO1997024337A1/en active IP Right Grant
- 1996-11-20 AU AU10562/97A patent/AU710982B2/en not_active Ceased
- 1996-11-20 KR KR10-1998-0704897A patent/KR100454802B1/ko not_active IP Right Cessation
- 1996-11-20 CZ CZ19981646A patent/CZ292185B6/cs not_active IP Right Cessation
- 1996-11-20 JP JP52432097A patent/JP3802566B2/ja not_active Expired - Fee Related
- 1996-11-20 ES ES96941410T patent/ES2224185T3/es not_active Expired - Lifetime
- 1996-11-20 HU HU9902053A patent/HU225546B1/hu not_active IP Right Cessation
- 1996-11-20 RU RU98114503/04A patent/RU2167870C2/ru not_active IP Right Cessation
- 1996-11-20 EP EP96941410A patent/EP0889882B1/en not_active Expired - Lifetime
- 1996-11-20 BR BR9612366A patent/BR9612366A/pt not_active IP Right Cessation
- 1996-11-20 PL PL96327601A patent/PL186048B1/pl not_active IP Right Cessation
- 1996-11-20 AT AT96941410T patent/ATE271549T1/de not_active IP Right Cessation
- 1996-11-20 DE DE69632966T patent/DE69632966T2/de not_active Expired - Fee Related
- 1996-11-20 CA CA002241632A patent/CA2241632C/en not_active Expired - Fee Related
-
1998
- 1998-06-25 MX MX9805188A patent/MX9805188A/es unknown
-
1999
- 1999-06-24 HK HK99102718A patent/HK1017678A1/xx not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
PL327601A1 (en) | 1998-12-21 |
JP3802566B2 (ja) | 2006-07-26 |
CZ292185B6 (cs) | 2003-08-13 |
HUP9902053A2 (hu) | 1999-11-29 |
DE69632966T2 (de) | 2005-08-25 |
KR100454802B1 (ko) | 2004-12-31 |
EP0889882B1 (en) | 2004-07-21 |
KR19990076773A (ko) | 1999-10-15 |
US5965742A (en) | 1999-10-12 |
CA2241632C (en) | 2005-10-18 |
CN1203591A (zh) | 1998-12-30 |
BR9612366A (pt) | 1999-07-13 |
HUP9902053A3 (en) | 2000-01-28 |
EP0889882A4 (en) | 2000-01-26 |
EP0889882A1 (en) | 1999-01-13 |
HK1017678A1 (en) | 1999-11-26 |
ES2224185T3 (es) | 2005-03-01 |
CA2241632A1 (en) | 1997-07-10 |
DE69632966D1 (de) | 2004-08-26 |
ATE271549T1 (de) | 2004-08-15 |
AU1056297A (en) | 1997-07-28 |
CZ164698A3 (cs) | 1998-09-16 |
HU225546B1 (en) | 2007-03-28 |
PL186048B1 (pl) | 2003-09-30 |
CN1067383C (zh) | 2001-06-20 |
AU710982B2 (en) | 1999-10-07 |
JP2000502701A (ja) | 2000-03-07 |
RU2167870C2 (ru) | 2001-05-27 |
WO1997024337A1 (en) | 1997-07-10 |
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