MX9709461A - Proceso para la preparacion de 3-(metiltio)propanal y 2-hidroxi-4-(metiltio)butanonitrilo. - Google Patents

Proceso para la preparacion de 3-(metiltio)propanal y 2-hidroxi-4-(metiltio)butanonitrilo.

Info

Publication number
MX9709461A
MX9709461A MX9709461A MX9709461A MX9709461A MX 9709461 A MX9709461 A MX 9709461A MX 9709461 A MX9709461 A MX 9709461A MX 9709461 A MX9709461 A MX 9709461A MX 9709461 A MX9709461 A MX 9709461A
Authority
MX
Mexico
Prior art keywords
methylthio
butanenitrile
propanal
hydroxy
preparation
Prior art date
Application number
MX9709461A
Other languages
English (en)
Other versions
MXPA97009461A (es
Inventor
Thomas F Blackburn
Paul F Pellegrin
Allen H Kranz
Original Assignee
Novus Int Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US08/476,356 external-priority patent/US5663409A/en
Application filed by Novus Int Inc filed Critical Novus Int Inc
Publication of MXPA97009461A publication Critical patent/MXPA97009461A/es
Publication of MX9709461A publication Critical patent/MX9709461A/es

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/14Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides
    • C07C319/20Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides by reactions not involving the formation of sulfide groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/14Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides
    • C07C319/18Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides by addition of thiols to unsaturated compounds

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Pyridine Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

La presente invencion describe un proceso catalítico para la preparacion de 3-(metiltio) propanal y 2-hidroxi-4-(metiltio)butanonitrilo, usando catalizadores de adicion novedosos. Los catalizadores de adicion novedosos incluyen: triisopropanlamina, nicotinamida, imidazol, bencimidazol, 2-fluoropiridina, picolina, pirazina, trialquilaminas que tienen desde tres a dieciocho átomos de carbono en cadauno de los substituyentes de alquilo unidos al átomo de nitrogeno, y aminas terciarias que tienen la formula (I), en donde A es arilo, R1 y R2 son alquilo, y x, a, b y c son enteros tales que 0 <- x <- 3, a<- a <- 3, 0 <- b <- 2, 0 <- c <- 2, siempre que a + b + c = 3.
MX9709461A 1995-06-07 1996-06-04 Proceso para la preparacion de 3-(metiltio)propanal y 2-hidroxi-4-(metiltio)butanonitrilo. MX9709461A (es)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US08/476,356 US5663409A (en) 1995-06-07 1995-06-07 Process for the preparation of 3-(methylthio) propanal and 2-hydroxy-4-(methylthio) butanenitrile
US08476356 1995-06-07
US08581249 1995-12-29
US08/581,249 US5705675A (en) 1995-06-07 1995-12-29 Processes for the preparation of 3-(methylthio)propanal and 2-hydroxy-4-(methylthio)butanenitrile
PCT/US1996/009060 WO1996040631A1 (en) 1995-06-07 1996-06-04 Processes for the preparation of 3-(methylthio)propanal and 2-hydroxy-4-(methylthio)butanenitrile

Publications (2)

Publication Number Publication Date
MXPA97009461A MXPA97009461A (es) 1998-02-01
MX9709461A true MX9709461A (es) 1998-02-28

Family

ID=27045156

Family Applications (1)

Application Number Title Priority Date Filing Date
MX9709461A MX9709461A (es) 1995-06-07 1996-06-04 Proceso para la preparacion de 3-(metiltio)propanal y 2-hidroxi-4-(metiltio)butanonitrilo.

Country Status (11)

Country Link
EP (1) EP0830341B1 (es)
JP (1) JPH11511119A (es)
CN (2) CN1092184C (es)
AR (1) AR002174A1 (es)
AU (1) AU714151B2 (es)
DE (1) DE69615022T2 (es)
ES (1) ES2160819T3 (es)
MX (1) MX9709461A (es)
PL (1) PL323722A1 (es)
PT (1) PT830341E (es)
WO (1) WO1996040631A1 (es)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102004038053A1 (de) * 2004-08-05 2006-04-27 Degussa Ag Verfahren zur Herstellung von 3-(Methylthio)propanal
DE102005003990A1 (de) * 2005-01-28 2006-08-03 Degussa Ag Herstellung von 3-(Alkylthio)propanal
PL2321270T3 (pl) 2008-08-19 2016-09-30 Ulepszony sposób addycji tiolanów do alfa, beta-nienasyconych związków karbonylowych lub sulfonylowych
JP2010111642A (ja) * 2008-11-07 2010-05-20 Sumitomo Chemical Co Ltd メチオニンの製造方法
FR2938535B1 (fr) 2008-11-20 2012-08-17 Arkema France Procede de fabrication de methylmercaptopropionaldehyde et de methionine a partir de matieres renouvelables
JP5182198B2 (ja) 2009-04-06 2013-04-10 住友化学株式会社 3−メチルチオプロパナールの製造方法
AU2010317842A1 (en) 2009-11-16 2012-07-12 Mellitech [1,5]-diazocin derivatives
JP5402864B2 (ja) * 2010-07-20 2014-01-29 住友化学株式会社 3−メチルチオプロパナールの製造方法
FR2966456B1 (fr) * 2010-10-26 2013-03-15 Adisseo France Sas Procede d'obtention d'acroleine par deshydratation catalytique de glycerol ou de glycerine
BR112013018092B1 (pt) 2011-02-23 2021-04-27 Evonik Operations Gmbh Método para produção de 2-hidróxi-4-(metiltio) butano nitrila a partir de 3- (metiltio) propanal e cianeto de hidrogênio, e uso de um produto de reação, que contém mmp-cianidrina
CN103380109B (zh) 2011-02-23 2015-05-20 赢创德固赛有限公司 存储稳定的2-羟基-4-(甲硫基)丁酸腈
EP2679579A1 (de) * 2012-06-27 2014-01-01 Evonik Industries AG Integriertes Verfahren zur Herstellung von Acrolein und 3-Methylmercaptopropionaldehyd
CN105136942A (zh) * 2015-08-27 2015-12-09 天津春发生物科技集团有限公司 一种2,3-二甲基吡嗪的分析检测方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2542768A (en) * 1945-10-24 1951-02-20 Du Pont Hydroxy-methylmercaptobutyronitrile
FR976673A (fr) * 1948-10-11 1951-03-21 M Le Ministre De L Ind Et Du C Procédé de préparation de produits beta-thioalcoylés
US2745745A (en) * 1952-10-30 1956-05-15 Monsanto Chemicals Poultry feed
JPS5755742B2 (es) * 1972-05-16 1982-11-26
JPS4924046A (es) * 1972-06-24 1974-03-04
DE2320544C2 (de) * 1973-04-21 1975-06-05 Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler, 6000 Frankfurt Verfahren zur Herstellung von 3-Methylmercaptopropionaldehyd
FR2314917A1 (fr) * 1975-06-20 1977-01-14 Rhone Poulenc Ind Procede de fabrication de l'aldehyde beta-methylthiopropionique

Also Published As

Publication number Publication date
AU5987396A (en) 1996-12-30
ES2160819T3 (es) 2001-11-16
DE69615022T2 (de) 2002-03-21
CN1510030A (zh) 2004-07-07
EP0830341A1 (en) 1998-03-25
AU714151B2 (en) 1999-12-23
EP0830341B1 (en) 2001-09-05
PL323722A1 (en) 1998-04-14
AR002174A1 (es) 1998-01-07
JPH11511119A (ja) 1999-09-28
CN1189818A (zh) 1998-08-05
PT830341E (pt) 2001-12-28
CN1092184C (zh) 2002-10-09
DE69615022D1 (de) 2001-10-11
WO1996040631A1 (en) 1996-12-19

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