MX367470B - Proceso para la preparacion de 1-cloro-3,3,3-trifluoropropeno utilizando un catalizador de transferencia de fase. - Google Patents
Proceso para la preparacion de 1-cloro-3,3,3-trifluoropropeno utilizando un catalizador de transferencia de fase.Info
- Publication number
- MX367470B MX367470B MX2015009941A MX2015009941A MX367470B MX 367470 B MX367470 B MX 367470B MX 2015009941 A MX2015009941 A MX 2015009941A MX 2015009941 A MX2015009941 A MX 2015009941A MX 367470 B MX367470 B MX 367470B
- Authority
- MX
- Mexico
- Prior art keywords
- chloro
- transfer catalyst
- trifluoropropene
- preparation
- phase transfer
- Prior art date
Links
- LDTMPQQAWUMPKS-OWOJBTEDSA-N (e)-1-chloro-3,3,3-trifluoroprop-1-ene Chemical compound FC(F)(F)\C=C\Cl LDTMPQQAWUMPKS-OWOJBTEDSA-N 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- 239000003444 phase transfer catalyst Substances 0.000 title abstract 2
- VVWFZKBKXPXGBH-UHFFFAOYSA-N 1,1,1,3,3-pentachloropropane Chemical compound ClC(Cl)CC(Cl)(Cl)Cl VVWFZKBKXPXGBH-UHFFFAOYSA-N 0.000 abstract 2
- 238000006243 chemical reaction Methods 0.000 abstract 2
- 239000000376 reactant Substances 0.000 abstract 2
- XPIGFCKQOOBTLK-UHFFFAOYSA-N 1,1,3,3-tetrachloroprop-1-ene Chemical compound ClC(Cl)C=C(Cl)Cl XPIGFCKQOOBTLK-UHFFFAOYSA-N 0.000 abstract 1
- GVVUPGXFVJLPDE-UHFFFAOYSA-N 1,3,3,3-tetrachloroprop-1-ene Chemical compound ClC=CC(Cl)(Cl)Cl GVVUPGXFVJLPDE-UHFFFAOYSA-N 0.000 abstract 1
- 238000003682 fluorination reaction Methods 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
- C07C17/202—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction
- C07C17/204—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction the other compound being a halogen
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
- C07C17/202—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction
- C07C17/206—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction the other compound being HX
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
- C07C17/21—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms with simultaneous increase of the number of halogen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/25—Preparation of halogenated hydrocarbons by splitting-off hydrogen halides from halogenated hydrocarbons
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
Abstract
Se describe un proceso en el que la fluoración de un reactivo orgánico que comprende el 1,1,1,3,3-pentacloropropano (240fa) con HF anhidro se lleva a cabo en la presencia de una cantidad eficaz de un catalizador de transferencia de fase, que facilita la reacción entre estos componentes de reacción incompatibles para producir 1-cloro-3, 3, 3-trifluoro-propeno (1233zd) . Otros materiales reactivos orgánicos incluyen el 1,1,3,3-tetra--cloro-pr openo (HCO-1230za), 1,3, 3,3-tetra-cloro-propeno (HCO-1230zd), y diversas mezclas con o sin 240fa.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201361760321P | 2013-02-04 | 2013-02-04 | |
US14/168,065 US8907146B2 (en) | 2013-02-04 | 2014-01-30 | Process for the preparation of 1-chloro-3,3,3-trifluoropropene using a phase transfer catalyst |
PCT/US2014/014360 WO2014121171A1 (en) | 2013-02-04 | 2014-02-03 | Process for the preparation of 1-chloro-3,3,3-trifluoropropene using a phase transfer catalyst |
Publications (2)
Publication Number | Publication Date |
---|---|
MX2015009941A MX2015009941A (es) | 2015-09-29 |
MX367470B true MX367470B (es) | 2019-08-23 |
Family
ID=51259781
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MX2015009941A MX367470B (es) | 2013-02-04 | 2014-02-03 | Proceso para la preparacion de 1-cloro-3,3,3-trifluoropropeno utilizando un catalizador de transferencia de fase. |
Country Status (7)
Country | Link |
---|---|
US (1) | US8907146B2 (es) |
EP (1) | EP2951140B1 (es) |
JP (2) | JP2016510338A (es) |
CN (1) | CN105026347B (es) |
ES (1) | ES2660601T3 (es) |
MX (1) | MX367470B (es) |
WO (1) | WO2014121171A1 (es) |
Families Citing this family (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US9156752B2 (en) * | 2011-01-04 | 2015-10-13 | Honeywell International Inc. | High purity E-1-chloro-3,3,3-trifluoropropene and methods of making the same |
US9222177B2 (en) | 2013-03-13 | 2015-12-29 | Honeywell International Inc. | Azeotropic compositions of 1,3,3,3-tetrachloroprop-1-ene and hydrogen fluoride |
US9255045B2 (en) | 2014-01-13 | 2016-02-09 | Arkema France | E-1-chloro-3,3,3-trifluoropropene production process from 1,1,3,3-tetrachloropropene |
FR3036398B1 (fr) | 2015-05-22 | 2019-05-03 | Arkema France | Compositions a base de 1,1,3,3-tetrachloropropene |
US10000431B1 (en) * | 2018-01-30 | 2018-06-19 | Honeywell International Inc. | Process for the production of 1-chloro-3,3,3-trifluoropropene (HCFO-1233zd) |
FR3081158B1 (fr) | 2018-05-16 | 2020-07-31 | Arkema France | Procede de production du 1-chloro-3,3,3-trifluoropropene. |
FR3083232B1 (fr) * | 2018-06-27 | 2021-11-12 | Arkema France | Procede de production du 1-chloro-3,3,3-trifluoropropene |
FR3086287B1 (fr) | 2018-09-26 | 2020-09-18 | Arkema France | Stabilisation du 1-chloro-3,3,3-trifluoropropene |
US10875819B2 (en) * | 2019-03-04 | 2020-12-29 | Honeywell International Inc. | Processes for producing trifluoroiodomethane using metal trifluoroacetates |
CN113600236B (zh) * | 2021-08-05 | 2022-05-17 | 肯特催化材料股份有限公司 | 一种相转移催化剂及其制备方法及应用 |
Family Cites Families (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4140719A (en) | 1977-10-31 | 1979-02-20 | Merck & Co., Inc. | Solid-liquid phase transfer catalysis improved method of preparing 2,4-difluoroaniline |
IT1106051B (it) * | 1977-10-31 | 1985-11-11 | Merck & Co Inc | Procedimento per preparare 2/4-di fluoroanilina |
US5710352A (en) | 1996-09-19 | 1998-01-20 | Alliedsignal Inc. | Vapor phase process for making 1,1,1,3,3-pentafluoropropane and 1-chloro-3,3,3-trifluoropropene |
JP3804289B2 (ja) | 1998-09-22 | 2006-08-02 | ダイキン工業株式会社 | 1,1,1,3,3−ペンタフルオロプロパン及び/又は1−クロロ−3,3,3−トリフルオロプロペンの製造方法 |
US6844475B1 (en) * | 2003-08-08 | 2005-01-18 | Honeywell International Business Machines | Low temperature production of 1-chloro-3,3,3-trifluoropropene (HCFC-1233zd) |
CN1218935C (zh) * | 2003-08-15 | 2005-09-14 | 中国科学院动物研究所 | 取代苯甲酰脲类昆虫生长调节剂的合成方法 |
JP4875626B2 (ja) * | 2004-11-17 | 2012-02-15 | ピラマル クリティカル ケアー インコーポレイテッド | セボフルランの調製のための方法 |
GB0806389D0 (en) * | 2008-04-09 | 2008-05-14 | Ineos Fluor Holdings Ltd | Process |
CN102164881B (zh) * | 2008-09-25 | 2015-05-27 | 中央硝子株式会社 | 1,3,3,3-四氟丙烯的制造方法 |
US8075797B2 (en) | 2009-01-29 | 2011-12-13 | Honeywell International Inc. | Azeotrope-like compositions of pentafluoropropane, chlorotrifluoropropene, and hydrogen fluoride |
US9045386B2 (en) * | 2010-02-18 | 2015-06-02 | Honeywell International Inc. | Integrated process and methods of producing (E)-1-chloro-3,3,3-trifluoropropene |
US8373010B2 (en) | 2010-09-03 | 2013-02-12 | Honeywell International Inc. | Methods to produce 3,3,3-trifluoropropene |
US8889924B2 (en) | 2012-02-14 | 2014-11-18 | Honeywell International Inc. | Process for the production of 1,3,3,3-tetrafluoropropene |
-
2014
- 2014-01-30 US US14/168,065 patent/US8907146B2/en active Active
- 2014-02-03 EP EP14746002.6A patent/EP2951140B1/en active Active
- 2014-02-03 MX MX2015009941A patent/MX367470B/es active IP Right Grant
- 2014-02-03 ES ES14746002.6T patent/ES2660601T3/es active Active
- 2014-02-03 WO PCT/US2014/014360 patent/WO2014121171A1/en active Application Filing
- 2014-02-03 JP JP2015556193A patent/JP2016510338A/ja active Pending
- 2014-02-03 CN CN201480007303.4A patent/CN105026347B/zh active Active
-
2018
- 2018-07-20 JP JP2018136493A patent/JP6571248B2/ja active Active
Also Published As
Publication number | Publication date |
---|---|
CN105026347B (zh) | 2018-10-09 |
JP2016510338A (ja) | 2016-04-07 |
EP2951140B1 (en) | 2018-01-10 |
EP2951140A1 (en) | 2015-12-09 |
US8907146B2 (en) | 2014-12-09 |
EP2951140A4 (en) | 2016-09-28 |
US20140221704A1 (en) | 2014-08-07 |
MX2015009941A (es) | 2015-09-29 |
ES2660601T3 (es) | 2018-03-23 |
JP2018184442A (ja) | 2018-11-22 |
CN105026347A (zh) | 2015-11-04 |
JP6571248B2 (ja) | 2019-09-04 |
WO2014121171A1 (en) | 2014-08-07 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
MX2015009941A (es) | Proceso para preparacion de 1-cloro-3,3,3-trifluoropropeno utilizando un catalizador de transferencia de fase. | |
WO2012148695A3 (en) | INTEGRATED PROCESS TO CO-PRODUCE 1,1,1,3,3-PENTAFLUOROPROPANE, TRANS-1-CHLORO-3,3,3-TRIFLUOROPROPENE and TRANS-1,3,3,3-TETRAFLUOROPROPENE | |
MX341276B (es) | Procedimiento para la fabricacion de 2,3,3,3-tetrafluoropropeno mediante fluoracion en fase gaseosa de pentacloropropano. | |
ES2645268T3 (es) | Proceso para la preparación de 2,3,3,3 tetrafluoropropeno | |
MX2013002467A (es) | Proceso integrado para co-producir trans-1-cloro-3,3,3-trifluoropr openo, trans-1,3,3,3-tetrafluoropropeno y 1,1,1,3,3-pentafluoropro pano. | |
MX347872B (es) | Proceso para la preparacion de 2,3,3,3-tetrafluoropropeno. | |
PL2563750T3 (pl) | SPOSÓB WYTWARZANIA 2-CHLORO-3,3,3-TRIFLUOROPROPENU (HCFO 1233xf) PRZEZ FLUOROWANIE PENTACHLOROPROPANU W FAZIE CIEKŁEJ | |
MX343619B (es) | Proceso para la fabricacion de 2-cloro-1,1,1,2-tetrafluoropropano por fluoracion en fase liquida de 2-cloro-3,3,3-trifluoropropeno. | |
WO2012154227A3 (en) | Integrated process to co-produce trans-1-chloro-3,3,3-trifluoropropene, trans-1,3,3,3-tetrafluoropropene, and 1,1,1,3,3-pentafluoropropane | |
MX2014009265A (es) | Proceso mejorado para la fabricacion de 2, 3, 3, 3 - tetrafluoropropeno. | |
WO2011126679A3 (en) | Catalyst life improvement in the vapor phase fluorination of chlorocarbons | |
WO2009125199A3 (en) | Process for the preparation of 2, 3, 3, 3-tetrafluoropropene | |
SG10201509239XA (en) | Compositions comprising 2,3,3,3-tetrafluoropropene, 1,1,2,3-tetrachloropropene, 2-chloro-3,3,3-trifluoropropene, or 2-chloro-1,1,1,2-tetrafluoropropane | |
MX2016004735A (es) | Proceso para producir 1-cloro-3,3,3-trifluropropeno en un liquido ionico. | |
MX2009008662A (es) | Metodo para la produccion de 2,3,3,3-tetrafluoropropeno. | |
MX356631B (es) | Proceso para la fabricación de 2-cloro-3,3,3-trifluoropropeno (hcfo 1233xf) por fluoración en fase líquida de pentacloropropano. | |
MX344552B (es) | Proceso para producir 2, 3, 3, 3 - tetrafluoropropeno. | |
MX2014005243A (es) | Proceso para producir 2,3,3,3-tetrafluoropropeno. | |
MX2018001489A (es) | Isomerizacion catalitica de z-1,1,14,4,4,-hexafluoro-2-buteno a e-1,1,1,4,4,4-hexafluoro-2-buteno. | |
EP2737006A4 (en) | FOAMS AND FLAME-RESISTANT ARTICLES OF FOAMING WITH 1-CHLORO-3,3,3-TRIFLUORPROPENE (1233ZD) | |
WO2014151448A3 (en) | An improved integrated process to produce 2,3,3,3-tetrafluoropropene | |
AR088658A1 (es) | Proceso para producir 2,3,3,3-tetrafluoropropeno | |
MX345769B (es) | Proceso para la fabricación de 2-cloro-3,3,3-trifluoropropeno por fluoración en fase gas de pentacloropropano. | |
MX2016009118A (es) | Procedimiento de produccion de e-1-cloro-3,3,3-trifluoropropeno a partir de 1,1,3,3-tetracloropropeno. | |
MX2015010962A (es) | Proceso para producir 2,3,3,3-tetrafluoropropeno. |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
FG | Grant or registration |