MX345248B - Reactor y proceso para preparar sulfuro de hidrogeno. - Google Patents

Reactor y proceso para preparar sulfuro de hidrogeno.

Info

Publication number
MX345248B
MX345248B MX2014015659A MX2014015659A MX345248B MX 345248 B MX345248 B MX 345248B MX 2014015659 A MX2014015659 A MX 2014015659A MX 2014015659 A MX2014015659 A MX 2014015659A MX 345248 B MX345248 B MX 345248B
Authority
MX
Mexico
Prior art keywords
reactor
hydrogen sulphide
preparing hydrogen
hydrogen
relates
Prior art date
Application number
MX2014015659A
Other languages
English (en)
Other versions
MX2014015659A (es
Inventor
Finkeldei Caspar-Heinrich
Körfer Martin
Kee Cheung Chiu
Maassen Ralf
Wenner Stefan
Original Assignee
Evonik Degussa Gmbh *
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Evonik Degussa Gmbh * filed Critical Evonik Degussa Gmbh *
Publication of MX2014015659A publication Critical patent/MX2014015659A/es
Publication of MX345248B publication Critical patent/MX345248B/es

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J10/00Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
    • B01J10/005Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor carried out at high temperatures in the presence of a molten material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/006Baffles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • B01J19/2415Tubular reactors
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/001Feed or outlet devices as such, e.g. feeding tubes
    • B01J4/002Nozzle-type elements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J7/00Apparatus for generating gases
    • B01J7/02Apparatus for generating gases by wet methods
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B01J8/067Heating or cooling the reactor
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00Sulfur; Compounds thereof
    • C01B17/16Hydrogen sulfides
    • C01B17/161Preparation from elemental sulfur
    • C01B17/162Preparation from elemental sulfur from elemental sulfur and hydrogen
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00Sulfur; Compounds thereof
    • C01B17/20Methods for preparing sulfides or polysulfides, in general
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00164Controlling or regulating processes controlling the flow
    • B01J2219/00166Controlling or regulating processes controlling the flow controlling the residence time inside the reactor vessel
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761Details of the reactor
    • B01J2219/00763Baffles
    • B01J2219/00765Baffles attached to the reactor wall
    • B01J2219/00768Baffles attached to the reactor wall vertical
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761Details of the reactor
    • B01J2219/00763Baffles
    • B01J2219/00765Baffles attached to the reactor wall
    • B01J2219/00777Baffles attached to the reactor wall horizontal
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24Stationary reactors without moving elements inside

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Hydrogen, Water And Hydrids (AREA)
  • Catalysts (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

La presente invención se refiere a un reactor y a un proceso para la síntesis de sulfuro de hidrógeno a partir de azufre elemental y de hidrógeno a presión elevada y temperatura elevada. La invención se refiere además al uso del reactor para la preparación de sulfuro de hidrógeno en un alto rendimiento y con un bajo contenido de H2SX.
MX2014015659A 2012-06-22 2013-05-31 Reactor y proceso para preparar sulfuro de hidrogeno. MX345248B (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP12173253.1A EP2676928A1 (de) 2012-06-22 2012-06-22 Reaktor und Verfahren zur Herstellung von Schwefelwasserstoff
PCT/EP2013/061230 WO2013189715A1 (en) 2012-06-22 2013-05-31 Reactor and process for preparing hydrogen sulphide

Publications (2)

Publication Number Publication Date
MX2014015659A MX2014015659A (es) 2015-04-09
MX345248B true MX345248B (es) 2017-01-23

Family

ID=48537990

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2014015659A MX345248B (es) 2012-06-22 2013-05-31 Reactor y proceso para preparar sulfuro de hidrogeno.

Country Status (12)

Country Link
US (1) US9649615B2 (es)
EP (2) EP2676928A1 (es)
JP (1) JP6157610B2 (es)
KR (1) KR102022148B1 (es)
CN (1) CN104603048B (es)
BR (1) BR112014031936B1 (es)
ES (1) ES2583808T3 (es)
MX (1) MX345248B (es)
MY (1) MY166862A (es)
RU (1) RU2623766C2 (es)
SG (1) SG11201408551PA (es)
WO (1) WO2013189715A1 (es)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2676927A1 (de) * 2012-06-22 2013-12-25 Evonik Industries AG Reaktor und Verfahren zur Herstellung von Schwefelwasserstoff
EP2676926A1 (de) * 2012-06-22 2013-12-25 Evonik Industries AG Reaktor und Verfahren zur Herstellung von Schwefelwasserstoff
CA3009451A1 (en) * 2015-12-27 2017-07-06 Metoxs Pte, Ltd. System for generating h2s in an alkaline medium and method of using the same
CN112770834B (zh) * 2018-09-05 2023-07-21 巴斯夫欧洲公司 进行气/液两相高压反应的方法
CN112221435A (zh) * 2020-09-27 2021-01-15 山东新和成氨基酸有限公司 一种连续制备硫化氢的反应器及方法
KR102692857B1 (ko) * 2022-01-24 2024-08-07 주식회사 레이크테크놀로지 황화수소 반응기
KR102707194B1 (ko) * 2022-02-28 2024-09-20 주식회사 레이크테크놀로지 황화리튬 제조 장치
KR102707201B1 (ko) * 2022-02-28 2024-09-20 주식회사 레이크테크놀로지 황화리튬 제조 장치
KR102707192B1 (ko) * 2022-02-28 2024-09-20 주식회사 레이크테크놀로지 황화리튬 제조 장치

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2863725A (en) 1953-04-24 1958-12-09 Hooker Chemical Corp Process for making sulfur free hydrogen sulfide
US2876070A (en) 1955-03-28 1959-03-03 Chemetron Corp Method for producing hydrogen sulfide by synthesis
US2876071A (en) * 1955-05-31 1959-03-03 Chemetron Corp Method for producing hydrogen sulfide by synthesis
FR1593276A (es) * 1967-12-19 1970-05-25
SU649648A1 (ru) * 1975-07-28 1979-02-28 Н. Г. Вилесов, В. И. Калько, Б. Я. Скрипко, А. Д. Биба, В. Е. Ткаченко и В. Г. Болыиунов Способ получени сероводорода
SU833479A1 (ru) * 1979-10-29 1981-05-30 Институт Газа Академии Наук Усср Способ получени восстановительногогАзА, СОдЕРжАщЕгО СЕРОВОдОРОд и ОКиСьуглЕРОдА
WO1998023708A1 (en) * 1996-11-25 1998-06-04 Ashland Inc. H2s production from a molten metal reactor
DE10245164B4 (de) * 2002-09-26 2014-11-13 Evonik Degussa Gmbh Verfahren zur Umwandlung von Polysulfanen
FR2885138B1 (fr) * 2005-04-29 2007-06-15 Inst Rech Pour Le Dev I R D Et Procede de production d'acide sulfhydrique et son application, notamment a la depollution d'effluents contenant des metaux lourds
DE102006019590A1 (de) * 2006-04-27 2007-10-31 Degussa Gmbh Reaktionsbehälter für die Herstellung von Schwefelwasserstoff
US7833509B2 (en) * 2007-01-16 2010-11-16 Basf Se Method and device for the continuous production of hydrogen sulfide
CA2674554C (en) * 2007-01-16 2016-09-20 Basf Se Process and apparatus for continuously preparing hydrogen sulfide
WO2008087110A1 (de) 2007-01-16 2008-07-24 Basf Se Reaktor und verfahren zur herstellung von schwefelwasserstoff
DE102008040544A1 (de) 2008-07-18 2010-01-21 Evonik Degussa Gmbh Reaktionsbehälter und Verfahren zur Verwendung

Also Published As

Publication number Publication date
WO2013189715A1 (en) 2013-12-27
KR102022148B1 (ko) 2019-09-17
JP6157610B2 (ja) 2017-07-05
ES2583808T3 (es) 2016-09-22
US9649615B2 (en) 2017-05-16
BR112014031936B1 (pt) 2021-02-02
MX2014015659A (es) 2015-04-09
KR20150027226A (ko) 2015-03-11
EP2864245A1 (en) 2015-04-29
CN104603048A (zh) 2015-05-06
RU2015101750A (ru) 2016-08-10
RU2623766C2 (ru) 2017-06-29
EP2676928A1 (de) 2013-12-25
JP2015520112A (ja) 2015-07-16
BR112014031936A2 (pt) 2017-06-27
US20150151271A1 (en) 2015-06-04
SG11201408551PA (en) 2015-01-29
EP2864245B1 (en) 2016-04-20
CN104603048B (zh) 2016-10-05
MY166862A (en) 2018-07-24

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