MX2020004740A - Reactor sólido-gas-líquido (sgl) para la lixiviación de minerales polimetálicos y/o concentrados base plomo, cobre, zinc, fierro y/o sus mezclas. - Google Patents

Reactor sólido-gas-líquido (sgl) para la lixiviación de minerales polimetálicos y/o concentrados base plomo, cobre, zinc, fierro y/o sus mezclas.

Info

Publication number
MX2020004740A
MX2020004740A MX2020004740A MX2020004740A MX2020004740A MX 2020004740 A MX2020004740 A MX 2020004740A MX 2020004740 A MX2020004740 A MX 2020004740A MX 2020004740 A MX2020004740 A MX 2020004740A MX 2020004740 A MX2020004740 A MX 2020004740A
Authority
MX
Mexico
Prior art keywords
reactor
gas
leaching
zinc
mixtures
Prior art date
Application number
MX2020004740A
Other languages
English (en)
Inventor
Pérez Ricardo Benavides
Guzmán Isaías Almaguer
Vázquez David Ezequiel Vázquez
Original Assignee
Penoles Tecnologia S A De C V
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Penoles Tecnologia S A De C V filed Critical Penoles Tecnologia S A De C V
Publication of MX2020004740A publication Critical patent/MX2020004740A/es

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/86Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis co-operating with deflectors or baffles fixed to the receptacle
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05Stirrers
    • B01F27/11Stirrers characterised by the configuration of the stirrers
    • B01F27/19Stirrers with two or more mixing elements mounted in sequence on the same axis
    • B01F27/191Stirrers with two or more mixing elements mounted in sequence on the same axis with similar elements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/91Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with propellers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/70Mixers specially adapted for working at sub- or super-atmospheric pressure, e.g. combined with de-foaming
    • B01F33/71Mixers specially adapted for working at sub- or super-atmospheric pressure, e.g. combined with de-foaming working at super-atmospheric pressure, e.g. in pressurised vessels
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/40Mounting or supporting mixing devices or receptacles; Clamping or holding arrangements therefor
    • B01F35/41Mounting or supporting stirrer shafts or stirrer units on receptacles
    • B01F35/412Mounting or supporting stirrer shafts or stirrer units on receptacles by supporting both extremities of the shaft
    • B01F35/4121Mounting or supporting stirrer shafts or stirrer units on receptacles by supporting both extremities of the shaft at the top and at the bottom of the receptacle, e.g. for performing a conical orbital movement about a vertical axis
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/90Heating or cooling systems
    • B01F35/92Heating or cooling systems for heating the outside of the receptacle, e.g. heated jackets or burners
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/006Baffles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B15/00Obtaining copper
    • C22B15/0063Hydrometallurgy
    • C22B15/0065Leaching or slurrying
    • C22B15/0067Leaching or slurrying with acids or salts thereof
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B19/00Obtaining zinc or zinc oxide
    • C22B19/20Obtaining zinc otherwise than by distilling
    • C22B19/22Obtaining zinc otherwise than by distilling with leaching with acids
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/02Apparatus therefor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00054Controlling or regulating the heat exchange system
    • B01J2219/00056Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00067Liquid level measurement
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/0009Coils
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761Details of the reactor
    • B01J2219/00763Baffles
    • B01J2219/00765Baffles attached to the reactor wall
    • B01J2219/00768Baffles attached to the reactor wall vertical
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761Details of the reactor
    • B01J2219/00763Baffles
    • B01J2219/00779Baffles attached to the stirring means
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Metallurgy (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • Environmental & Geological Engineering (AREA)
  • Geology (AREA)
  • Geochemistry & Mineralogy (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

La presente invención se refiere a un reactor vertical a baja presión de tanque agitado para la lixiviación de minerales polimetálicos y concentrados base plomo, cobre, zinc, fierro y/o sus mezclas, en un sistema de suspensión de tres fases, sólido-gas-líquido. El reactor vertical a baja presión de tanque agitado consiste de: un recipiente vertical de forma cilíndrica con tres o cuatro deflectores en una distribución equidistante en los 360°; un sistema de agitación compuesto de dos impulsores acoplados sobre una flecha agitadora, que provee la adecuada reacción e interacción de las especies metálicas de interés; un espacio del volumen del reactor que corresponde a entre el 20% al 35% del total del volumen del recipiente, ubicado en la parte superior del reactor y que actúa como una cámara de gas que provee de una alimentación continua de oxígeno; y un sistema de serpentines colocado sobre la superficie exterior o interior del reactor para asegurar rendimientos de transferencia de calor eficientes y una cinética controlada.
MX2020004740A 2017-11-06 2017-11-06 Reactor sólido-gas-líquido (sgl) para la lixiviación de minerales polimetálicos y/o concentrados base plomo, cobre, zinc, fierro y/o sus mezclas. MX2020004740A (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/MX2017/000125 WO2019088815A1 (es) 2017-11-06 2017-11-06 Reactor sólido-gas-líquido (sgl) para la lixiviación de minerales polimetálicos y/o concentrados base plomo, cobre, zinc y/o sus mezclas

Publications (1)

Publication Number Publication Date
MX2020004740A true MX2020004740A (es) 2022-02-25

Family

ID=66332221

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2020004740A MX2020004740A (es) 2017-11-06 2017-11-06 Reactor sólido-gas-líquido (sgl) para la lixiviación de minerales polimetálicos y/o concentrados base plomo, cobre, zinc, fierro y/o sus mezclas.

Country Status (5)

Country Link
US (1) US11110411B2 (es)
CA (1) CA3077013C (es)
MX (1) MX2020004740A (es)
PE (1) PE20201140A1 (es)
WO (1) WO2019088815A1 (es)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111921229B (zh) * 2020-10-14 2020-12-25 南昌市第三中学 萃取装置
CN115341093B (zh) * 2022-07-21 2023-10-24 永州市瑞祥锌材料有限公司 一种基于锌元素浸出装置
CN115572822A (zh) * 2022-10-08 2023-01-06 赣州西克节能自动化设备有限公司 一种原矿浸出工艺易监测控制的反应装置

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US3130015A (en) * 1958-10-31 1964-04-21 Mid Century Corp High pressure reactor
US3149888A (en) * 1962-11-14 1964-09-22 Nettco Corp Foot bearing construction for mixers
DE3516027A1 (de) 1985-05-04 1986-11-06 Huels Chemische Werke Ag Ruehrsystem und verfahren zum begasen von fluessigkeiten
FI86601C (fi) 1987-10-21 1992-09-25 Outokumpu Oy Saett att aostadkomma dubbelcirkulationsfloede och apparatur daertill.
US5240327A (en) * 1987-10-21 1993-08-31 Outokumpu Oy Method for creating double loop flow
US5211924A (en) * 1988-02-29 1993-05-18 Amoco Corporation Method and apparatus for increasing conversion efficiency and reducing power costs for oxidation of an aromatic alkyl to an aromatic carboxylic acid
FI110760B (fi) * 2000-07-21 2003-03-31 Outokumpu Oy Sekoitinlaitteisto ja menetelmä kaasun sekoittamiseksi suljetussa reaktorissa
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US20090134173A1 (en) * 2007-11-26 2009-05-28 Paul Mueller Company Baffle System for a Vessel
RS55556B1 (sr) * 2010-07-30 2017-05-31 Total Res & Technology Feluy Upotreba sistema za pipremanje suspenzije katalizatora
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FI124934B (fi) 2013-01-30 2015-03-31 Outotec Oyj Sekoitussäiliöreaktori

Also Published As

Publication number Publication date
CA3077013A1 (en) 2019-05-09
US20200254405A1 (en) 2020-08-13
PE20201140A1 (es) 2020-10-26
CA3077013C (en) 2021-08-17
WO2019088815A1 (es) 2019-05-09
US11110411B2 (en) 2021-09-07

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