MX2019010517A - Metodo de sintesis multirreactor de cristales de zeolita de granulometria controlada. - Google Patents

Metodo de sintesis multirreactor de cristales de zeolita de granulometria controlada.

Info

Publication number
MX2019010517A
MX2019010517A MX2019010517A MX2019010517A MX2019010517A MX 2019010517 A MX2019010517 A MX 2019010517A MX 2019010517 A MX2019010517 A MX 2019010517A MX 2019010517 A MX2019010517 A MX 2019010517A MX 2019010517 A MX2019010517 A MX 2019010517A
Authority
MX
Mexico
Prior art keywords
particle size
crystals
zeolite
controlled particle
reactors
Prior art date
Application number
MX2019010517A
Other languages
English (en)
Inventor
Lutz Cécile
Nicolas Serge
Original Assignee
Arkema France
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Arkema France filed Critical Arkema France
Publication of MX2019010517A publication Critical patent/MX2019010517A/es

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1812—Tubular reactors
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/20—Faujasite type, e.g. type X or Y
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/26—Mordenite type
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/36—Pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00027—Process aspects
    • B01J2219/00029—Batch processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00027—Process aspects
    • B01J2219/00033—Continuous processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00279—Features relating to reactor vessels
    • B01J2219/00306—Reactor vessels in a multiple arrangement
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00583—Features relative to the processes being carried out
    • B01J2219/0059—Sequential processes
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/51—Particles with a specific particle size distribution
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)

Abstract

La presente invención se refiere a un método de preparación de cristales de zeolita que tienen una distribución granulométrica multimodal, y cuyos tamaños están comprendidos entre 0.02 µm y 20 µm, comprendiendo el método la alimentación de cada uno de al menos dos reactores con un gel de síntesis adecuado para formar cristales de zeolita, la modalidad de una reacción de cristalización, en paralelo, en cada uno de los al menos dos reactores, y la mezcla de los medios de reacción de los al menos dos reactores tras el inicio de al menos una de las reacciones de cristalización.
MX2019010517A 2017-03-17 2018-03-12 Metodo de sintesis multirreactor de cristales de zeolita de granulometria controlada. MX2019010517A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1752199A FR3063995A1 (fr) 2017-03-17 2017-03-17 Procede de synthese multi-reacteur de cristaux de zeolithe a granulometrie controlee
PCT/FR2018/050571 WO2018167417A1 (fr) 2017-03-17 2018-03-12 Procédé de synthèse multi-réacteur de cristaux de zéolithe à granulométrie contrôlée

Publications (1)

Publication Number Publication Date
MX2019010517A true MX2019010517A (es) 2019-10-17

Family

ID=59253651

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2019010517A MX2019010517A (es) 2017-03-17 2018-03-12 Metodo de sintesis multirreactor de cristales de zeolita de granulometria controlada.

Country Status (11)

Country Link
US (1) US11377361B2 (es)
EP (1) EP3596012A1 (es)
JP (1) JP6961010B2 (es)
KR (1) KR102291888B1 (es)
CN (1) CN110446684B (es)
EA (1) EA037046B1 (es)
FR (1) FR3063995A1 (es)
MX (1) MX2019010517A (es)
TW (1) TWI676598B (es)
WO (1) WO2018167417A1 (es)
ZA (1) ZA201905758B (es)

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1357762A (fr) 1963-02-27 1964-04-10 Pernod & Ricard Perfectionnements aux procédés de préparation de jus de fruits et de légumes et notamment de jus de raisin
ZA851734B (en) * 1984-03-23 1986-10-29 Mobil Oil Corp A continuous process for manufacturing crystalline zeolites
NO304355B1 (no) * 1997-02-20 1998-12-07 Sinvent As Multi-autoklav for metodisk, automatisert syntese av zeolitter og andre forbindelser
JP3257509B2 (ja) * 1997-11-27 2002-02-18 東ソー株式会社 低シリカフォージャサイト型ゼオライトおよびその製造方法
US5989518A (en) * 1998-12-29 1999-11-23 Uop Llc Process for synthesizing and controlling the particle size and particle size distribution of a molecular sieve
JP2002020116A (ja) * 2000-06-30 2002-01-23 Taiyo Machinery Co Ltd 人工ゼオライトの製造方法と該方法に用いる製造装置
GB0523707D0 (en) 2005-11-22 2005-12-28 Nitech Solutions Ltd Improved apparatus and method for temperature controlled processes
FR2925478B1 (fr) * 2007-12-20 2009-12-18 Ceca Sa Zeolite de type lsx a granulometrie controlee
CN105358483B (zh) * 2013-07-09 2019-06-04 三菱化学株式会社 沸石的制造方法
CN105682795B (zh) * 2013-10-24 2020-11-17 格雷斯公司 用于合成磷酸硅铝-34分子筛的方法

Also Published As

Publication number Publication date
US20200048102A1 (en) 2020-02-13
FR3063995A1 (fr) 2018-09-21
EP3596012A1 (fr) 2020-01-22
EA201992198A1 (ru) 2020-02-07
EA037046B1 (ru) 2021-01-29
CN110446684A (zh) 2019-11-12
KR102291888B1 (ko) 2021-08-19
JP2020509987A (ja) 2020-04-02
TW201838919A (zh) 2018-11-01
TWI676598B (zh) 2019-11-11
KR20190118200A (ko) 2019-10-17
CN110446684B (zh) 2023-04-04
US11377361B2 (en) 2022-07-05
WO2018167417A1 (fr) 2018-09-20
JP6961010B2 (ja) 2021-11-05
ZA201905758B (en) 2021-02-24

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