MX2016011621A - Metodo para producir mentonas a partir de isopulegol en la fase gaseosa. - Google Patents

Metodo para producir mentonas a partir de isopulegol en la fase gaseosa.

Info

Publication number
MX2016011621A
MX2016011621A MX2016011621A MX2016011621A MX2016011621A MX 2016011621 A MX2016011621 A MX 2016011621A MX 2016011621 A MX2016011621 A MX 2016011621A MX 2016011621 A MX2016011621 A MX 2016011621A MX 2016011621 A MX2016011621 A MX 2016011621A
Authority
MX
Mexico
Prior art keywords
gas phase
isopulegol
menthones
producing
products
Prior art date
Application number
MX2016011621A
Other languages
English (en)
Inventor
Rüdenauer Stefan
Keller Andreas
Schneider Daniel
HICKMANN Volker
Dehn Martine
Renz Stephanie
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of MX2016011621A publication Critical patent/MX2016011621A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/51—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition
    • C07C45/511—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition involving transformation of singly bound oxygen functional groups to >C = O groups
    • C07C45/512—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition involving transformation of singly bound oxygen functional groups to >C = O groups the singly bound functional group being a free hydroxyl group
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/35—Ketones, e.g. benzophenone
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/889—Manganese, technetium or rhenium
    • B01J23/8892—Manganese
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/29—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation of hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/29—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation of hydroxy groups
    • C07C45/298—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation of hydroxy groups with manganese derivatives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/385—Saturated compounds containing a keto group being part of a ring
    • C07C49/403—Saturated compounds containing a keto group being part of a ring of a six-membered ring
    • C07C49/407—Menthones
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/10—General cosmetic use
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • Animal Behavior & Ethology (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Emergency Medicine (AREA)
  • Oral & Maxillofacial Surgery (AREA)
  • Dermatology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Cosmetics (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Seasonings (AREA)
  • Medicinal Preparation (AREA)

Abstract

La presente invención se refiere a un procedimiento para hacer reaccionar isopulegol para obtener mentona en la fase gaseosa, mediante el uso de un catalizador de cobre, y al uso de los productos de reacción así preparados como aditivos en productos alimenticios, productos cosméticos, productos farmacéuticos, formulaciones de tabaco, productos para la casa, y productos para el cuidado de la ropa.
MX2016011621A 2014-03-07 2015-03-06 Metodo para producir mentonas a partir de isopulegol en la fase gaseosa. MX2016011621A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP14158373.2A EP2915797A1 (de) 2014-03-07 2014-03-07 Verfahren zur Herstellung von Menthonen aus Isopulegol in der Gasphase
PCT/EP2015/054693 WO2015132370A1 (de) 2014-03-07 2015-03-06 Verfahren zur herstellung von menthonen aus isopulegol in der gasphase

Publications (1)

Publication Number Publication Date
MX2016011621A true MX2016011621A (es) 2016-12-14

Family

ID=50231068

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2016011621A MX2016011621A (es) 2014-03-07 2015-03-06 Metodo para producir mentonas a partir de isopulegol en la fase gaseosa.

Country Status (7)

Country Link
US (1) US9856199B2 (es)
EP (3) EP2915797A1 (es)
JP (1) JP6580605B2 (es)
CN (1) CN106061933B (es)
ES (2) ES2750313T3 (es)
MX (1) MX2016011621A (es)
WO (1) WO2015132370A1 (es)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3221286B1 (en) 2014-11-18 2019-03-13 Basf Se Process for the preparation of 1-(2,6,6-trimethylcyclohexyl)-alkan-3-ols
EP3483151A1 (de) 2015-03-05 2019-05-15 Basf Se Tetrahydropyranylester als riechstoffe
MX2017014148A (es) 2015-05-04 2018-03-15 Basf Se Proceso para la preparacion de melonal.
ES2899823T3 (es) 2015-07-10 2022-03-14 Basf Se Procedimiento para la hidroformilación de butadienos sustituidos en posición 2 y para la producción de sus derivados, especialmente de Ambrox
MX2018000606A (es) 2015-07-15 2018-05-28 Basf Se Proceso para preparar un arilpropeno.
WO2017009462A1 (en) 2015-07-15 2017-01-19 Basf Se Process for preparing an arylpropene
EP3170828A1 (de) 2015-11-23 2017-05-24 Basf Se Verfahren zur herstellung von verbindungen mit 16-oxabicyclo[10.3.1]pentadecengerüst und deren folgeprodukten
EP3386919B1 (en) 2015-12-08 2021-10-20 Basf Se A tin-containing zeolitic material having a bea framework structure
US10954538B2 (en) 2016-02-19 2021-03-23 Basf Se Enzymatic cyclization of homofarnesylic acid
CN107602357B (zh) * 2017-09-28 2020-06-02 万华化学集团股份有限公司 一种制备薄荷酮的方法
CN109704944B (zh) * 2018-12-25 2022-01-07 万华化学集团股份有限公司 一种由香茅醛制备薄荷酮的方法及用于该方法的催化剂体系
CN110922316B (zh) * 2019-12-04 2022-11-08 万华化学集团股份有限公司 一种由r-香茅醛制备l-薄荷酮的方法
CN112250556B (zh) * 2020-10-23 2022-04-22 万华化学集团股份有限公司 一种薄荷酮的制备方法
CN114570376B (zh) * 2022-03-07 2024-01-26 安徽海华科技集团有限公司 一种合成薄荷酮用的催化剂及合成薄荷酮的方法

Family Cites Families (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2785188A (en) 1952-02-04 1957-03-12 Union Oil Co Method for preparing 3, 3'-5, 5'-tetraalkyl-4, 4'-diphenoquinones
US2885444A (en) 1958-03-05 1959-05-05 Dow Chemical Co Oxidation of 2, 4-di-tertiary-alkyl-phenols with oxygen
US3247262A (en) 1961-11-17 1966-04-19 Dow Chemical Co Process for making polyphenols
US4097461A (en) 1976-12-03 1978-06-27 Ici Americas Inc. Oxidative coupling of alkylphenols or 1-naphthols catalyzed by metal complexes of diketo compounds
US4134919A (en) 1977-06-14 1979-01-16 Takasago Perfumery Co., Ltd. Process for producing menthone
US4380676A (en) 1980-02-29 1983-04-19 Ciba-Geigy Corporation Process for the production of 2,2'-dihydroxy-biphenyls
DE4236111A1 (de) 1992-10-26 1994-04-28 Henkel Kgaa Verfahren zur Herstellung von L-Menthon
GB0229770D0 (en) 2002-12-20 2003-01-29 Sasol Technology Uk Ltd Olefinic metathesis in the presence of phenolic compounds
US8575086B2 (en) * 2005-01-18 2013-11-05 Takasago International Corporation Flavor and fragrance compositions
JP5025955B2 (ja) * 2005-01-18 2012-09-12 高砂香料工業株式会社 香料組成物
JP5065608B2 (ja) * 2006-03-16 2012-11-07 高砂香料工業株式会社 ミント組成物
RU2009104151A (ru) * 2006-08-02 2010-09-10 Вм. Ригли Дж. Компани (Us) Способ приготовления состава и состав (варианты) для ухода за полостью рта
EP2181084B1 (de) 2007-07-23 2015-07-01 Basf Se Verfahren zur herstellung von menthol durch hydrierung von isopulegol
CN102010297B (zh) * 2010-11-23 2013-06-12 广东省食品工业研究所 一种手性合成左旋薄荷醇的方法
US20130281696A1 (en) 2012-04-20 2013-10-24 Basf Se Process for preparing branched alcohols
US9061960B2 (en) 2012-05-30 2015-06-23 Basf Se Method for working up mixtures
US20130331607A1 (en) 2012-06-11 2013-12-12 Basf Se Process for preparing formic acid
DE102012212437A1 (de) 2012-07-16 2014-01-16 Basf Se Verfahren zur Herstellung von Acrylsäure aus Ethylenoxid und Kohlenmonoxid
DE102012212424A1 (de) 2012-07-16 2014-01-16 Basf Se Verfahren zur Herstellung von Acrylsäure durch eine mit wenigstens einer molekularen Wirkverbindung katalysierte Thermolyse von Poly-3-hydroxypropionat
US9085526B2 (en) 2012-07-17 2015-07-21 Basf Se Process for preparing carboxylic acid esters
US8853400B2 (en) 2012-07-23 2014-10-07 Basf Se Process for the homogeneously catalyzed amination of alcohols with ammonia in the presence of a complex catalyst which comprises no anionic ligands
EP2706054A1 (de) * 2012-09-10 2014-03-12 Basf Se Verfahren zur Herstellung von Menthon aus Isopulegol
US20160304415A1 (en) 2013-12-11 2016-10-20 Basf Se Work-up of a reaction mixture (rm) comprising cyclododecatriene and an active catalyst system

Also Published As

Publication number Publication date
CN106061933B (zh) 2019-07-09
EP2915797A1 (de) 2015-09-09
EP3114104A1 (de) 2017-01-11
ES2750313T3 (es) 2020-03-25
WO2015132370A1 (de) 2015-09-11
JP6580605B2 (ja) 2019-09-25
EP3114104B1 (de) 2019-07-17
US20170066705A1 (en) 2017-03-09
EP3539942C0 (de) 2023-09-13
JP2017514886A (ja) 2017-06-08
EP3539942B1 (de) 2023-09-13
ES2965627T3 (es) 2024-04-16
EP3539942A1 (de) 2019-09-18
US9856199B2 (en) 2018-01-02
CN106061933A (zh) 2016-10-26

Similar Documents

Publication Publication Date Title
MX2016011621A (es) Metodo para producir mentonas a partir de isopulegol en la fase gaseosa.
ZA201504665B (en) Processes and apparatus for producing nanocellulose, and compositions and products produced therefrom
PH12014502010A1 (en) Bispecific antibodies against human tweak and human il17 and uses thereof
MX2019000609A (es) Proceso para preparacion de microcapsulas.
MX2015003077A (es) Metodo para preparar mentona a partir de isopulegol.
EA201291095A1 (ru) Способ получения пероральной лекарственной формы, содержащей финголимод
MX2013008046A (es) Hidrogeles a base de esteres de acido poliisobutenosuccinico.
NZ758332A (en) Clean label stabilized buckwheat starch
MX369662B (es) Granulos de harina de microalgas y proceso de preparacion de estos.
MX2014004055A (es) Proceso para la preparacion de metoximelonal.
MX2017009358A (es) Proceso para la preparacion de microcapsulas libres de melamina-formaldehido.
GEP201706708B (en) Isoxazolidine derivatives
MX2017008090A (es) Nuevos compuestos, su procedimiento de sintesis y su uso en medicina, asi como en cosmetica.
MX2018015269A (es) Derivados de tailanstatina a, metodos de tratamiento y metodos de sintesis de los mismos.
IN2014MU00495A (es)
MX363686B (es) Capsulas de aceite de cafe.
MX2015011881A (es) Proceso para la preparacion de 3,7-dimetilnonan-1-ol.
PH12017501147A1 (en) Total synthesis of trioxacarcin dc-45-a2 and preparation of trioxacarcin analogs
CY1118614T1 (el) Νεα παραγωγα (αζα)βενζυδρυλαιθερα, διεργασια παρασκευης τους και χρηση τους ως προσδετες h4-υποδοχεα για θεραπευτικες εφαρμογες
IN2013CH05865A (es)
IN2015DN02660A (es)
PH12017550027A1 (en) Sugar-dipeptide conjugates as flavor molecules
PH12017550033A1 (en) Sugar-dipeptide conjugates as flavor molecules
CN302231873S (zh) 家庭网关(e5172)
GR1008653B (el) Μεθοδος δια την παρασκευη πιπεροναλης