MD4178C1 - Procedeu de obţinere a 2-nitro-4,5-difenilimidazolului - Google Patents
Procedeu de obţinere a 2-nitro-4,5-difenilimidazolului Download PDFInfo
- Publication number
- MD4178C1 MD4178C1 MDA20120023A MD20120023A MD4178C1 MD 4178 C1 MD4178 C1 MD 4178C1 MD A20120023 A MDA20120023 A MD A20120023A MD 20120023 A MD20120023 A MD 20120023A MD 4178 C1 MD4178 C1 MD 4178C1
- Authority
- MD
- Moldova
- Prior art keywords
- diphenylimidazole
- nitro
- producing
- compounds
- coordinative
- Prior art date
Links
- STGHAEAHYGLKLG-UHFFFAOYSA-N 2-nitro-4,5-diphenyl-1h-imidazole Chemical compound N1C([N+](=O)[O-])=NC(C=2C=CC=CC=2)=C1C1=CC=CC=C1 STGHAEAHYGLKLG-UHFFFAOYSA-N 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 2
- 150000001875 compounds Chemical class 0.000 abstract 4
- CPHGOBGXZQKCKI-UHFFFAOYSA-N 4,5-diphenyl-1h-imidazole Chemical compound N1C=NC(C=2C=CC=CC=2)=C1C1=CC=CC=C1 CPHGOBGXZQKCKI-UHFFFAOYSA-N 0.000 abstract 1
- 229910002651 NO3 Inorganic materials 0.000 abstract 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 abstract 1
- PTFCDOFLOPIGGS-UHFFFAOYSA-N Zinc dication Chemical compound [Zn+2] PTFCDOFLOPIGGS-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 239000012736 aqueous medium Substances 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- XLJKHNWPARRRJB-UHFFFAOYSA-N cobalt(2+) Chemical compound [Co+2] XLJKHNWPARRRJB-UHFFFAOYSA-N 0.000 abstract 1
- 238000007324 demetalation reaction Methods 0.000 abstract 1
- 125000000623 heterocyclic group Chemical group 0.000 abstract 1
- 229910052500 inorganic mineral Inorganic materials 0.000 abstract 1
- 230000003993 interaction Effects 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 239000011707 mineral Substances 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 238000006386 neutralization reaction Methods 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| MDA20120023A MD4178C1 (ro) | 2012-02-27 | 2012-02-27 | Procedeu de obţinere a 2-nitro-4,5-difenilimidazolului |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| MDA20120023A MD4178C1 (ro) | 2012-02-27 | 2012-02-27 | Procedeu de obţinere a 2-nitro-4,5-difenilimidazolului |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| MD4178B1 MD4178B1 (en) | 2012-07-31 |
| MD4178C1 true MD4178C1 (ro) | 2013-02-28 |
Family
ID=46582440
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MDA20120023A MD4178C1 (ro) | 2012-02-27 | 2012-02-27 | Procedeu de obţinere a 2-nitro-4,5-difenilimidazolului |
Country Status (1)
| Country | Link |
|---|---|
| MD (1) | MD4178C1 (mo) |
Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB700211A (en) * | 1950-07-21 | 1953-11-25 | Ciba Ltd | Manufacture of azo dyestuffs |
| US4199592A (en) * | 1978-08-29 | 1980-04-22 | E. I. Du Pont De Nemours And Company | Antiinflammatory 4,5-diaryl-2-nitroimidazoles |
| US4241060A (en) * | 1977-08-19 | 1980-12-23 | Hoffmann-La Roche Inc. | Nitroimidazoles and compositions thereof |
| US5008398A (en) * | 1988-10-15 | 1991-04-16 | Basf Aktiengesellschaft | Preparation of p-nitrophenyl-imidazoles |
| EP0510036A1 (en) * | 1990-01-12 | 1992-10-28 | Rhone Poulenc Rorer Sa | 2-SUBSTITUTED 4,5-DIPHENYLIMIDAZOLES. |
| WO1994019310A1 (en) * | 1993-02-26 | 1994-09-01 | Instituto Nacional De Engenharia E Tecnologia Industrial | New process for the nitration of aromatic compounds in mild, non-corrosive conditions |
| RU2021249C1 (ru) * | 1990-10-16 | 1994-10-15 | Индивидуально-частное предприятие "Ост-Вест" | Способ получения ароматических 1,2-дикетонов |
| CN1736976A (zh) * | 2005-08-30 | 2006-02-22 | 南京大学 | 硝酸铝在芳环硝化中的应用 |
| WO2008070336A2 (en) * | 2006-10-27 | 2008-06-12 | Natural Pharmacia International, Inc. | Hypoxia-selective, weakly basic 2-nitroimidazole delivery agents and methods of use thereof |
| US20100004460A1 (en) * | 2007-01-23 | 2010-01-07 | Pola Pharma Inc | Method for producing 2-nitroimidazole derivative |
| MD4150B1 (en) * | 2011-10-11 | 2012-02-29 | Inst De Chimie Al Academiei De Stiinte A Moldovei | Process for producing coordinative compounds of Co(II), Ni(II) and Zn(II) with 2-nitro-4,5-diphenylimidazole starting from 4,5-diphenylimidazole and nitrates of said metals |
-
2012
- 2012-02-27 MD MDA20120023A patent/MD4178C1/ro not_active IP Right Cessation
Patent Citations (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB700211A (en) * | 1950-07-21 | 1953-11-25 | Ciba Ltd | Manufacture of azo dyestuffs |
| US4241060A (en) * | 1977-08-19 | 1980-12-23 | Hoffmann-La Roche Inc. | Nitroimidazoles and compositions thereof |
| US4199592A (en) * | 1978-08-29 | 1980-04-22 | E. I. Du Pont De Nemours And Company | Antiinflammatory 4,5-diaryl-2-nitroimidazoles |
| US5008398A (en) * | 1988-10-15 | 1991-04-16 | Basf Aktiengesellschaft | Preparation of p-nitrophenyl-imidazoles |
| EP0510036A1 (en) * | 1990-01-12 | 1992-10-28 | Rhone Poulenc Rorer Sa | 2-SUBSTITUTED 4,5-DIPHENYLIMIDAZOLES. |
| RU2021249C1 (ru) * | 1990-10-16 | 1994-10-15 | Индивидуально-частное предприятие "Ост-Вест" | Способ получения ароматических 1,2-дикетонов |
| WO1994019310A1 (en) * | 1993-02-26 | 1994-09-01 | Instituto Nacional De Engenharia E Tecnologia Industrial | New process for the nitration of aromatic compounds in mild, non-corrosive conditions |
| CN1736976A (zh) * | 2005-08-30 | 2006-02-22 | 南京大学 | 硝酸铝在芳环硝化中的应用 |
| WO2008070336A2 (en) * | 2006-10-27 | 2008-06-12 | Natural Pharmacia International, Inc. | Hypoxia-selective, weakly basic 2-nitroimidazole delivery agents and methods of use thereof |
| US7842278B2 (en) * | 2006-10-27 | 2010-11-30 | Natural Pharmacia International, Inc. | Hypoxia-selective, weakly basic 2-nitroimidazole delivery agents and methods of use thereof |
| US20100004460A1 (en) * | 2007-01-23 | 2010-01-07 | Pola Pharma Inc | Method for producing 2-nitroimidazole derivative |
| MD4150B1 (en) * | 2011-10-11 | 2012-02-29 | Inst De Chimie Al Academiei De Stiinte A Moldovei | Process for producing coordinative compounds of Co(II), Ni(II) and Zn(II) with 2-nitro-4,5-diphenylimidazole starting from 4,5-diphenylimidazole and nitrates of said metals |
Non-Patent Citations (9)
| Title |
|---|
| Bergan T. Antibacterial activity and pharmacokinetics of nitroimidazoles. A review. Scand. J. Infect. Dis., 1985, vol. 17 (Suppl. 46), p. 64-71 * |
| Charlson R.H., Brown T.L. Inorg. Chem., vol. 5, no. 2, 1966, p. 268 * |
| Cornelius A., Laszlo P., "Clay supported copper(II) and iron(III) nitrates: novel multipurpose reagents for organic synthesis". Synthesis, October, p. 909-918 (1985) * |
| Es T. van and Backerberg O.G. Substitution of 4,5-diphenyl-oxazoles and some related compounds. J. Chem. Soc., 1963, p. 1363-1370 * |
| Palamaru M.N., Iordan A.R., Cecal A. Chimie bioanorganică şi metalele vieţii, BIT, Iaşi, 1997, 395 p. * |
| Sathururu R and Biehl Ed, "Facile, high-yield, regioselective synthesis of ortho-nitroderivatives of hydroxy heterocycles using cerium (IV) ammonium nitrate", ARCHIVOC, The Archive for Organic Chemistry, 2004 (xiv) 89-95. Published on the web 23 Sep 2004, (regăsit în Internet la 2011.12.20, url: http://quod.lib.umich.edu/cgi/p/pod/dod-idx?c=ark;idno=5550190.0005.e09 ) * |
| Yagovkin A.Yu. and Bakibaev A.A. Formation of a 2-Nitro Derivative in the Oxidation of 4,5-Diphenylimidazole to Benzyl using Nitric Acid. Chemistry of Heterocyclic Compounds, 1995, vol.31, No. 12, p. 1696-1697 * |
| Новиков С.С. и др. Химия Гетероциклических Соединений, 1970, № 4, с. 503 * |
| Эйхгорн Г. Неорганическая химия, Мир, Москва, 1978, том 1, том 2 * |
Also Published As
| Publication number | Publication date |
|---|---|
| MD4178B1 (en) | 2012-07-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG4A | Patent for invention issued | ||
| KA4A | Patent for invention lapsed due to non-payment of fees (with right of restoration) | ||
| MM4A | Patent for invention definitely lapsed due to non-payment of fees |