MD242Z - Method for producing hydrophilic PbS nanocrystals - Google Patents

Method for producing hydrophilic PbS nanocrystals

Info

Publication number
MD242Z
MD242Z MDS20100019A MDS20100019A MD242Z MD 242 Z MD242 Z MD 242Z MD S20100019 A MDS20100019 A MD S20100019A MD S20100019 A MDS20100019 A MD S20100019A MD 242 Z MD242 Z MD 242Z
Authority
MD
Moldova
Prior art keywords
pbs nanocrystals
boiling
producing
producing hydrophilic
nanocrystals
Prior art date
Application number
MDS20100019A
Other languages
Romanian (ro)
Russian (ru)
Inventor
Анатолие ГАВРИЛУЦА
Корнелиу ГЕРМАН
Анатол МИТИОГЛУ
Рената ЛАСКОВА
Генадие НОВИЦКИЙ
Михаил РЕВЕНКО
Леонид КУЛЮК
Original Assignee
Институт Прикладной Физики Академии Наук Молдовы
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Институт Прикладной Физики Академии Наук Молдовы filed Critical Институт Прикладной Физики Академии Наук Молдовы
Priority to MDS20100019A priority Critical patent/MD242Z/en
Publication of MD242Y publication Critical patent/MD242Y/en
Publication of MD242Z publication Critical patent/MD242Z/en

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  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)

Abstract

The invention relates to methods for producing PbS nanocrystals, in particular to a method for producing hydrophilic PbS nanocrystals.The method, according to the invention, includes the homogenization of PbS nanocrystals, stabilized by oleic acid, in a nonpolar solvent, the boiling point of which is below the water boiling point in a ratio of 25 mg/ml, treatment of the obtained solution with 0.05...1.0 N solution of lithium or sodium, or potassium, or rubidium hydroxide, heating of the obtained mixture at the temperature of 50...60°C up to its staining in an intense black and brown colour, the gradual increase of temperature to the boiling of nonpolar solvent and maintenance of boiling up to its complete evaporation.
MDS20100019A 2010-01-26 2010-01-26 Method for producing hydrophilic PbS nanocrystals MD242Z (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
MDS20100019A MD242Z (en) 2010-01-26 2010-01-26 Method for producing hydrophilic PbS nanocrystals

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
MDS20100019A MD242Z (en) 2010-01-26 2010-01-26 Method for producing hydrophilic PbS nanocrystals

Publications (2)

Publication Number Publication Date
MD242Y MD242Y (en) 2010-07-30
MD242Z true MD242Z (en) 2011-03-31

Family

ID=45815112

Family Applications (1)

Application Number Title Priority Date Filing Date
MDS20100019A MD242Z (en) 2010-01-26 2010-01-26 Method for producing hydrophilic PbS nanocrystals

Country Status (1)

Country Link
MD (1) MD242Z (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109850937B (en) * 2019-01-25 2022-03-25 深圳扑浪创新科技有限公司 Preparation method of lead sulfide quantum dot fluorescent powder

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GB2420343A (en) * 2004-11-18 2006-05-24 Dambarudhar Mohanta Coupled lead sulphide (PbS) quantum dots dispersed in a rubber matrix
MD2982G2 (en) * 2005-08-10 2006-10-31 Институт Прикладной Физики Академии Наук Молдовы Process for obtaining semiconductor nanostructures
CN1907863A (en) * 2006-08-24 2007-02-07 同济大学 Method of preparing sulfide nano material of lead with calixarene adjusting solvent thermal system
CN1944270A (en) * 2006-10-13 2007-04-11 中国科学院上海硅酸盐研究所 Method for preparing sulfure family compound nano tube of lead by cysteine biological molecule assisted self assembling
CN101049960A (en) * 2007-03-29 2007-10-10 浙江大学 Method for fabricating Nano rod of lead sulfide
MD3320G2 (en) * 2006-03-24 2007-12-31 Институт Прикладной Физики Академии Наук Молдовы Process for obtaining zinc oxide nanostructures
MD3404G2 (en) * 2006-11-30 2008-04-30 Институт Прикладной Физики Академии Наук Молдовы Process for obtaining nanostructured zinc gallate
MD3652F1 (en) * 2007-04-20 2008-07-31 Institutul De Fizica Aplicata Al Academiei De Stiinte A Moldovei Photoluminescent nanocomposite on base of oxidic semiconductor and organic polymer (variants)
MD3535G2 (en) * 2007-03-21 2008-10-31 Государственный Университет Молд0 Process for nanodispersed titanium dioxide obtaining
RU2341472C1 (en) * 2007-03-02 2008-12-20 Государственное образовательное учреждение высшего профессионального образования "Санкт-Петербургский государственный технологический институт (технический университет)" Glass with nanocrystals of lead selenide for saturable absorbers
MD3888F1 (en) * 2007-11-12 2009-04-30 Universitatea De Stat Din Moldova Process for obtaining a photoluminescent nanocomposite from CdS and organic polymers
MD3934B1 (en) * 2008-09-08 2009-06-30 Institutul De Inginerie Electronica Si Tehnologii Industriale Al Academiei De Stiinte A Moldovei Process for obtaining the substrate of BaF2 with perfect surface
CN101605717A (en) * 2007-01-05 2009-12-16 大光横滨电池工业私人有限公司 Produce the method for nano lead oxides
KR20100011506A (en) * 2008-07-25 2010-02-03 아주대학교산학협력단 Lead sulfide nanorod crystals and method for controlling shape of the nanocrystals
  • 2010

Patent Citations (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU1640123A1 (en) * 1988-05-17 1991-04-07 Казанский научно-исследовательский, технологический и проектный институт химико-фотографической промышленности Производственного объединения "Тасма" Method of separating red lead from sewage containing gelatine
RU2236033C2 (en) * 2002-10-10 2004-09-10 Государственное унитарное предприятие "НПО "ОРИОН" Method of preparing light-sensitive lead sulfide layers
GB2420343A (en) * 2004-11-18 2006-05-24 Dambarudhar Mohanta Coupled lead sulphide (PbS) quantum dots dispersed in a rubber matrix
MD2982G2 (en) * 2005-08-10 2006-10-31 Институт Прикладной Физики Академии Наук Молдовы Process for obtaining semiconductor nanostructures
MD3320G2 (en) * 2006-03-24 2007-12-31 Институт Прикладной Физики Академии Наук Молдовы Process for obtaining zinc oxide nanostructures
CN1907863A (en) * 2006-08-24 2007-02-07 同济大学 Method of preparing sulfide nano material of lead with calixarene adjusting solvent thermal system
CN1944270A (en) * 2006-10-13 2007-04-11 中国科学院上海硅酸盐研究所 Method for preparing sulfure family compound nano tube of lead by cysteine biological molecule assisted self assembling
MD3404G2 (en) * 2006-11-30 2008-04-30 Институт Прикладной Физики Академии Наук Молдовы Process for obtaining nanostructured zinc gallate
CN101605717A (en) * 2007-01-05 2009-12-16 大光横滨电池工业私人有限公司 Produce the method for nano lead oxides
RU2341472C1 (en) * 2007-03-02 2008-12-20 Государственное образовательное учреждение высшего профессионального образования "Санкт-Петербургский государственный технологический институт (технический университет)" Glass with nanocrystals of lead selenide for saturable absorbers
MD3535G2 (en) * 2007-03-21 2008-10-31 Государственный Университет Молд0 Process for nanodispersed titanium dioxide obtaining
CN101049960A (en) * 2007-03-29 2007-10-10 浙江大学 Method for fabricating Nano rod of lead sulfide
MD3652F1 (en) * 2007-04-20 2008-07-31 Institutul De Fizica Aplicata Al Academiei De Stiinte A Moldovei Photoluminescent nanocomposite on base of oxidic semiconductor and organic polymer (variants)
MD3888F1 (en) * 2007-11-12 2009-04-30 Universitatea De Stat Din Moldova Process for obtaining a photoluminescent nanocomposite from CdS and organic polymers
KR20100011506A (en) * 2008-07-25 2010-02-03 아주대학교산학협력단 Lead sulfide nanorod crystals and method for controlling shape of the nanocrystals
MD3934B1 (en) * 2008-09-08 2009-06-30 Institutul De Inginerie Electronica Si Tehnologii Industriale Al Academiei De Stiinte A Moldovei Process for obtaining the substrate of BaF2 with perfect surface

Non-Patent Citations (8)

* Cited by examiner, † Cited by third party
Title
Bakueva L., Gorelikov I., Musikhin S., Zhao X.S., Sargent E.H., Kumacheva E. Adv. Mater., V. 16(11), 2004, p. 926-929. *
Bakueva, L., Gorelikov, I., Musikhin, S., Zhao, X.S., Sargent, E.H., Kumacheva, E. Adv. Mater., V. 16(11), 2004, pp. 926-929. *
Chen S., Liu W. Materials Chemistry and Physics, V. 98(1), 2006, p. 183-189 *
Gokarna A., Jun K-W., Khanna P.K., Baeg J-O.,. Seok A.I Bull. Korean Chem Soc., V26(11), 2005, p.1804 *
Lascova R., Gavriluţa A., Mitioglu A., Gherman C., Noviţchi Gh. Materialele Conferinţei Fizicienilor din Moldova, CFM-2009, 26-28 noiembrie 2009, p. 76 *
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Patel, A.A., Wu, F., Zhang, J.Z., Torres-Martines, C.L., Mehra, R.K., Yang, Y., Risbud, S.H. J. hys. Chem. B, 2000, V. 104, 11598-11605. *
Zhao, X., Gorelikov, I., Musikhin, S., Cauchi, S., Sukhovatkin, V., Sargent, E.H., Kumacheva, E. Langmiur, V. 21, 2005, pp. 1086-1090. *

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Publication number Publication date
MD242Y (en) 2010-07-30

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KA4Y Short-term patent lapsed due to non-payment of fees (with right of restoration)