MA65125A1 - Méthode de préparation de phosphate d'ammonium-manganèse-fer, et phosphate de lithium-manganèse-fer et utilisation associée - Google Patents

Méthode de préparation de phosphate d'ammonium-manganèse-fer, et phosphate de lithium-manganèse-fer et utilisation associée

Info

Publication number
MA65125A1
MA65125A1 MA65125A MA65125A MA65125A1 MA 65125 A1 MA65125 A1 MA 65125A1 MA 65125 A MA65125 A MA 65125A MA 65125 A MA65125 A MA 65125A MA 65125 A1 MA65125 A1 MA 65125A1
Authority
MA
Morocco
Prior art keywords
manganese
iron phosphate
solution
ammonium
mixed
Prior art date
Application number
MA65125A
Other languages
English (en)
Inventor
Haijun YU
Yinghao XIE
Xuemei Zhang
Changdong LI
Aixia LI
Original Assignee
Guangdong Brunp Recycling Technology Co., Ltd.
Hunan Brunp Recycling Technology Co., Ltd.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from CN202210741388.5A external-priority patent/CN115043387B/zh
Application filed by Guangdong Brunp Recycling Technology Co., Ltd., Hunan Brunp Recycling Technology Co., Ltd. filed Critical Guangdong Brunp Recycling Technology Co., Ltd.
Publication of MA65125A1 publication Critical patent/MA65125A1/fr

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00Phosphorus; Compounds thereof
    • C01B25/16Oxyacids of phosphorus; Salts thereof
    • C01B25/26Phosphates
    • C01B25/45Phosphates containing plural metal, or metal and ammonium
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00Phosphorus; Compounds thereof
    • C01B25/16Oxyacids of phosphorus; Salts thereof
    • C01B25/26Phosphates
    • C01B25/45Phosphates containing plural metal, or metal and ammonium
    • C01B25/451Phosphates containing plural metal, or metal and ammonium containing metal and ammonium
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00Secondary cells; Manufacture thereof
    • H01M10/05Accumulators with non-aqueous electrolyte
    • H01M10/052Li-accumulators
    • H01M10/0525Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/58Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/5825Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/01Particle morphology depicted by an image
    • C01P2004/03Particle morphology depicted by an image obtained by SEM
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/61Micrometer sized, i.e. from 1-100 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/40Electric properties
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Battery Electrode And Active Subsutance (AREA)

Abstract

L'invention concerne une méthode de préparation de phosphate d'ammonium-manganèse-fer, et du phosphate de lithium-manganèse-fer et une utilisation associée. La méthode de préparation comprend : le mélange respectif d'une solution de sel mixte métallique et d'une solution de dihydrogénophosphate d'ammonium avec une solution organique pour obtenir une solution mixte de sel métallique et une solution mixte de phosphate ; l'ajout simultané de la solution mixte de sel métallique, de la solution mixte de phosphate et d'une première solution d'ammoniac dans une solution de base pour une réaction ; et la réalisation d'une séparation solide-liquide pour obtenir du phosphate d'ammonium-manganèse-fer. Une solution de sel métallique mixte de source de manganèse et de source ferreuse et une source de phosphore sont soumises à une réaction de coprécipitation dans une phase organique, de telle sorte que le phosphate d'ammonium-manganèse-fer à haute densité de compactage à grosses particules est préparé au moyen d'une synthèse ; et une fois le phosphate d'ammonium-manganèse-fer mélangé avec une source de lithium et une source de carbone, le frittage peut être effectué pour préparer un matériau d'électrode positive de phosphate de lithium-manganèse-fer.
MA65125A 2022-06-28 2024-03-28 Méthode de préparation de phosphate d'ammonium-manganèse-fer, et phosphate de lithium-manganèse-fer et utilisation associée MA65125A1 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CN202210741388.5A CN115043387B (zh) 2022-06-28 2022-06-28 磷酸锰铁铵的制备方法、磷酸锰铁锂及其应用
PCT/CN2022/119985 WO2024000840A1 (fr) 2022-06-28 2022-09-20 Méthode de préparation de phosphate d'ammonium-manganèse-fer, et phosphate de lithium-manganèse-fer et utilisation associée

Publications (1)

Publication Number Publication Date
MA65125A1 true MA65125A1 (fr) 2025-09-30

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
MA65125A MA65125A1 (fr) 2022-06-28 2024-03-28 Méthode de préparation de phosphate d'ammonium-manganèse-fer, et phosphate de lithium-manganèse-fer et utilisation associée

Country Status (6)

Country Link
US (1) US20250214841A1 (fr)
DE (1) DE112022002449B4 (fr)
ES (1) ES3010782A2 (fr)
GB (1) GB2624951A (fr)
HU (1) HU231686B1 (fr)
MA (1) MA65125A1 (fr)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN118598108B (zh) * 2024-08-01 2025-05-13 新洋丰农业科技股份有限公司 一种磷酸铁锰铵和磷酸铁锰锂的制备方法
CN120829147B (zh) * 2025-09-18 2025-12-09 湖南长远锂科新能源有限公司 磷酸锰铁锂正极材料及其制备方法和锂离子电池

Citations (2)

* Cited by examiner, † Cited by third party
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CN104681795A (zh) * 2015-01-29 2015-06-03 北大先行科技产业有限公司 一种磷酸铁锰锂/碳复合材料的制备方法
CN113659133A (zh) * 2021-07-09 2021-11-16 江苏乐能电池股份有限公司 一种高压实磷酸铁锰锂正极材料的制备方法

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JP5835334B2 (ja) 2011-09-14 2015-12-24 住友金属鉱山株式会社 リン酸アンモニウムマンガン鉄とその製造方法、および該リン酸アンモニウムマンガン鉄を用いたリチウム二次電池用正極活物質の製造方法
CN103000898A (zh) * 2012-12-11 2013-03-27 中国电子科技集团公司第十八研究所 锂离子电池用碳复合磷酸锰铁锂的制备方法
CN105990562B (zh) * 2015-02-11 2019-11-05 中国科学院宁波材料技术与工程研究所 一种核壳结构的纳米磷酸锰铁锂复合材料及其制备方法和应用
CN106207164A (zh) 2015-04-30 2016-12-07 深圳市崧鼎科技有限公司 磷酸锰铁锂复合材料的制备方法
CN106816582B (zh) * 2015-11-30 2019-08-13 比亚迪股份有限公司 一种磷酸锰铁锂类材料及其制备方法以及电池浆料和正极与锂电池
CN105655584B (zh) 2016-03-07 2017-12-01 昆明理工大学 一种用于制备锂电池正极材料的磷酸锰铁铵的制备方法
CN106477545B (zh) 2016-10-14 2018-08-31 山东省科学院能源研究所 一种以NH4MnPO4为前驱体制备LiMnPO4/C复合材料的方法
CN109650367B (zh) * 2018-10-11 2020-09-22 广东光华科技股份有限公司 磷酸锰铁锂及其制备方法
WO2021003568A1 (fr) * 2019-07-08 2021-01-14 Klox Technologies Inc. Systèmes biophotoniques revêtus de polymère inerte
CN115043387B (zh) * 2022-06-28 2023-07-07 广东邦普循环科技有限公司 磷酸锰铁铵的制备方法、磷酸锰铁锂及其应用

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104681795A (zh) * 2015-01-29 2015-06-03 北大先行科技产业有限公司 一种磷酸铁锰锂/碳复合材料的制备方法
CN113659133A (zh) * 2021-07-09 2021-11-16 江苏乐能电池股份有限公司 一种高压实磷酸铁锰锂正极材料的制备方法

Also Published As

Publication number Publication date
US20250214841A1 (en) 2025-07-03
HUP2400049A1 (hu) 2024-07-28
GB2624951A (en) 2024-06-05
DE112022002449T5 (de) 2024-02-22
DE112022002449B4 (de) 2025-08-28
ES3010782A2 (es) 2025-04-04
GB202310156D0 (en) 2023-08-16
HU231686B1 (hu) 2025-09-28

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