LU73132A1 - - Google Patents

Info

Publication number
LU73132A1
LU73132A1 LU73132A LU73132A LU73132A1 LU 73132 A1 LU73132 A1 LU 73132A1 LU 73132 A LU73132 A LU 73132A LU 73132 A LU73132 A LU 73132A LU 73132 A1 LU73132 A1 LU 73132A1
Authority
LU
Luxembourg
Prior art keywords
precipitate
ceramic
hydroxylapatite
polycrystalline
collagen
Prior art date
Application number
LU73132A
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed filed Critical
Publication of LU73132A1 publication Critical patent/LU73132A1/xx

Links

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L27/00Materials for grafts or prostheses or for coating grafts or prostheses
    • A61L27/40Composite materials, i.e. containing one material dispersed in a matrix of the same or different material
    • A61L27/44Composite materials, i.e. containing one material dispersed in a matrix of the same or different material having a macromolecular matrix
    • A61L27/46Composite materials, i.e. containing one material dispersed in a matrix of the same or different material having a macromolecular matrix with phosphorus-containing inorganic fillers
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00Phosphorus; Compounds thereof
    • C01B25/16Oxyacids of phosphorus; Salts thereof
    • C01B25/26Phosphates
    • C01B25/32Phosphates of magnesium, calcium, strontium, or barium
    • C01B25/327After-treatment
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61CDENTISTRY; APPARATUS OR METHODS FOR ORAL OR DENTAL HYGIENE
    • A61C13/00Dental prostheses; Making same
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K6/00Preparations for dentistry
    • A61K6/50Preparations specially adapted for dental root treatment
    • A61K6/54Filling; Sealing
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K6/00Preparations for dentistry
    • A61K6/70Preparations for dentistry comprising inorganic additives
    • A61K6/78Pigments
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K6/00Preparations for dentistry
    • A61K6/80Preparations for artificial teeth, for filling teeth or for capping teeth
    • A61K6/831Preparations for artificial teeth, for filling teeth or for capping teeth comprising non-metallic elements or compounds thereof, e.g. carbon
    • A61K6/838Phosphorus compounds, e.g. apatite
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L27/00Materials for grafts or prostheses or for coating grafts or prostheses
    • A61L27/02Inorganic materials
    • A61L27/12Phosphorus-containing materials, e.g. apatite
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/447Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on phosphates, e.g. hydroxyapatite
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61FFILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
    • A61F2310/00Prostheses classified in A61F2/28 or A61F2/30 - A61F2/44 being constructed from or coated with a particular material
    • A61F2310/00005The prosthesis being constructed from a particular material
    • A61F2310/00179Ceramics or ceramic-like structures
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61FFILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
    • A61F2310/00Prostheses classified in A61F2/28 or A61F2/30 - A61F2/44 being constructed from or coated with a particular material
    • A61F2310/00005The prosthesis being constructed from a particular material
    • A61F2310/00179Ceramics or ceramic-like structures
    • A61F2310/00185Ceramics or ceramic-like structures based on metal oxides
    • A61F2310/00203Ceramics or ceramic-like structures based on metal oxides containing alumina or aluminium oxide
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61FFILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
    • A61F2310/00Prostheses classified in A61F2/28 or A61F2/30 - A61F2/44 being constructed from or coated with a particular material
    • A61F2310/00005The prosthesis being constructed from a particular material
    • A61F2310/00179Ceramics or ceramic-like structures
    • A61F2310/00293Ceramics or ceramic-like structures containing a phosphorus-containing compound, e.g. apatite

Landscapes

  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Oral & Maxillofacial Surgery (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Animal Behavior & Ethology (AREA)
  • Organic Chemistry (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Epidemiology (AREA)
  • Inorganic Chemistry (AREA)
  • Ceramic Engineering (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Medicinal Chemistry (AREA)
  • Dermatology (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Manufacturing & Machinery (AREA)
  • Transplantation (AREA)
  • Composite Materials (AREA)
  • Dentistry (AREA)
  • Plastic & Reconstructive Surgery (AREA)
  • Dental Preparations (AREA)
  • Compositions Of Oxide Ceramics (AREA)
  • Materials For Medical Uses (AREA)
  • Dental Prosthetics (AREA)
  • Porous Artificial Stone Or Porous Ceramic Products (AREA)

Abstract

1522182 Calcium phosphate ceramics STERLING DRUG Inc 22 July 1975 [2 Aug 1974 7 July 1975] 30706/75 Heading C1A A polycrystalline, sintered ceramic for use as a bone or tooth substitute is made by reacting calcium ion with phosphate ions in aqueous medium at pH of 10-12 to produce a gelatinous calcium phosphate precipitate having a Ca:P molar ratio of 1À44-1À72, separating the precipitate from the solution and heating the precipitate to above 1000‹C but below the temperature at which appreciable decomposition of hydroxylapatite occurs and maintaining said temperature for a sufficient time to effect sintering and maximum densification. When the Ca:P molar ratio is in the range 1À62-1À72 a translucent, isotropic, polycrystalline hydroxylapatite having an average crystalite size of 0À2-3 microns, a density of 3À1-3À14 g/cm<SP>3</SP>, substantially no pores and having cleavage along smooth curved planes is obtained. When the Ca:P ratio is in the range 1À44-1À60, preferably 1À46-1À57 a dense isotropic two-phase ceramic is obtained comprising 14-98% hydroxylapatite and 2-86% whitlockite, said ceramic having substantially no pores and having cleavage along smooth curved planes. The reactants are preferably Ca(NO 3 ) 2 and (NH 4 ) 2 HPO 4 . 0À4-0À6% of an organic binder, e.g. collagen, may be added to the precipitate to prevent cracking during drying. Porous forms of the ceramic may be made by including 5-25% by weight of organic binders such as powdered cellulose, starch, cotton or collagen to the precipitate. Fluoride ions may be introduced into the ceramic, e.g. by standing in 0À5-5% aqueous NaF for 12 hours-5 days.
LU73132A 1974-08-02 1975-08-01 LU73132A1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US49424074A 1974-08-02 1974-08-02
US59330375A 1975-07-07 1975-07-07

Publications (1)

Publication Number Publication Date
LU73132A1 true LU73132A1 (en) 1976-07-01

Family

ID=27051362

Family Applications (1)

Application Number Title Priority Date Filing Date
LU73132A LU73132A1 (en) 1974-08-02 1975-08-01

Country Status (20)

Country Link
JP (1) JPS5941946B2 (en)
AR (1) AR210581A1 (en)
AT (1) AT370067B (en)
AU (1) AU500991B2 (en)
BR (1) BR7504887A (en)
CA (1) CA1096582A (en)
CH (2) CH618951A5 (en)
DE (1) DE2534504A1 (en)
DK (1) DK347975A (en)
FI (1) FI64131C (en)
FR (1) FR2283104A1 (en)
GB (1) GB1522182A (en)
IE (1) IE42442B1 (en)
IL (1) IL47794A (en)
IT (1) IT1044406B (en)
LU (1) LU73132A1 (en)
NL (1) NL182859C (en)
NO (1) NO138802C (en)
NZ (1) NZ178266A (en)
SE (3) SE426386B (en)

Families Citing this family (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AT352867B (en) * 1976-05-12 1979-10-10 Battelle Institut E V BONE REPLACEMENT, BONE COMPOUND OR PROSTHESIS ANCHORING MATERIAL AND PROCESS FOR ITS PRODUCTION
DE2620907C3 (en) * 1976-05-12 1984-09-20 Battelle-Institut E.V., 6000 Frankfurt Anchoring for highly stressed endoprostheses
US4075092A (en) * 1976-08-10 1978-02-21 Research Corporation High surface area permeable material
CH608957A5 (en) * 1977-02-25 1979-02-15 Leuthard Paul E
IL56141A (en) * 1977-12-23 1981-10-30 Sterling Drug Inc Whitlockite ceramic and its manufacture
JPS54147940A (en) * 1978-05-09 1979-11-19 Sakurai Seiya Method for supplying trace nutritious elements to food * controlling oxidation and genera bacteria by basic pentacalcium triiphosphate
JPS5550349A (en) * 1978-10-09 1980-04-12 Kureha Chemical Ind Co Ltd Dental compound material
FR2460657A1 (en) * 1979-07-12 1981-01-30 Anvar BIODEGRADABLE IMPLANT FOR USE AS A BONE PROSTHESIS PIECE
JPS5645814A (en) * 1979-09-25 1981-04-25 Kureha Chem Ind Co Ltd Hydroxyapatite, its ceramic material and its manufacture
FR2478650A1 (en) * 1980-03-24 1981-09-25 Commissariat Energie Atomique CEMENT FOR USE IN FIXING BONE PROSTHESES
FR2485504A1 (en) * 1980-06-30 1981-12-31 Centre Nat Rech Scient Sintered fluoro:apatite for bone prostheses - made with porous structure free from foreign phases
FR2527779B1 (en) * 1982-05-25 1985-05-31 Commissariat Energie Atomique BONE TISSUE SIMULATOR MATERIAL, PREPARATION METHOD THEREOF AND USES THEREOF
CA1247960A (en) 1983-03-24 1989-01-03 Hideki Aoki Transcutaneously implantable element
DE3424777C2 (en) * 1983-07-08 1995-08-03 Kyushu Refractories Artificial dental materials
NL8402158A (en) * 1983-07-09 1985-02-01 Sumitomo Cement Co POROUS CERAMIC MATERIAL AND METHOD FOR THE PREPARATION THEREOF.
FR2577142B1 (en) * 1985-02-13 1987-03-06 Commissariat Energie Atomique BONE IMPLANT IN CARBON FIBER REINFORCED EPOXIDE RESIN AND PROCESS FOR PRODUCING THE SAME
JPH0624964B2 (en) * 1985-09-23 1994-04-06 東燃株式会社 Calcium phosphate-based hydroxyapatite and method for producing the same
DE3609432A1 (en) * 1986-03-20 1987-09-24 Kerstin Koerber Sinterable dental impression compounds and their use
JPH0720486B2 (en) * 1986-10-30 1995-03-08 京セラ株式会社 Calcium phosphate-based bioprosthetic material and method for producing the same
US4861733A (en) * 1987-02-13 1989-08-29 Interpore International Calcium phosphate bone substitute materials
JP2608721B2 (en) * 1987-05-12 1997-05-14 旭光学工業株式会社 Method for producing calcium phosphate-based material
EP0347776B2 (en) * 1988-06-21 2002-07-10 Vita Zahnfabrik H. Rauter GmbH &amp; Co. KG Dispersed ceramic material
EP0410010B1 (en) * 1989-07-22 1993-10-27 Johannes Friedrich Prof. Dr. Osborn Osteotropic implant material
DE3935060C2 (en) * 1989-10-20 1996-05-30 Herbst Bremer Goldschlaegerei Process for the production of a ceramic material for the dental field and its use
DE4302072A1 (en) * 1993-01-26 1994-07-28 Herbst Bremer Goldschlaegerei Ceramic material for dental fillings and / or dental prostheses and method for producing the same
GB9310194D0 (en) * 1993-05-18 1993-06-30 Millenium Bioligix Inc Assessment of osteoclast activity
DE10027946A1 (en) * 2000-06-08 2001-12-13 Wolfgang Wiedemann Dental ceramic used in dentistry as filling material and tooth replacement is anisotropic and contains a large amount of hydroxylapatite
US20170087060A1 (en) * 2011-11-18 2017-03-30 Sofsera Corporation Tooth surface repairing material
CN114890816B (en) * 2022-04-20 2023-04-25 广东欧文莱陶瓷有限公司 Ceramic tile with tree leaf surface and preparation method thereof
CN115651634B (en) * 2022-10-24 2024-07-19 大连工业大学 Perovskite quantum dot/hydroxyapatite composite luminescent material with high thermal stability, and preparation method and application thereof

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR618953A (en) 1927-03-24
US2508816A (en) * 1947-01-25 1950-05-23 Ment Jack De Prosthetic tooth composition
US3609867A (en) 1969-03-10 1971-10-05 Research Corp Plastic bone composition
US3787900A (en) * 1971-06-09 1974-01-29 Univ Iowa State Res Found Artificial bone or tooth prosthesis material
ZA741576B (en) * 1973-04-02 1975-02-26 Lee Pharmaceuticals Dental adhesive composition
JPS5645814A (en) 1979-09-25 1981-04-25 Kureha Chem Ind Co Ltd Hydroxyapatite, its ceramic material and its manufacture
JPS58134992A (en) 1982-01-21 1983-08-11 Kitasato Inst:The Antibiotic substance am-2604-a and its preparation

Also Published As

Publication number Publication date
IE42442B1 (en) 1980-08-13
SE7804813L (en) 1978-04-26
AU500991B2 (en) 1979-06-07
DE2534504A1 (en) 1976-02-19
SE7508751L (en) 1976-02-03
DE2534504C2 (en) 1989-02-16
NO138802C (en) 1978-11-15
JPS5941946B2 (en) 1984-10-11
AR210581A1 (en) 1977-08-31
NL182859B (en) 1988-01-04
SE425563B (en) 1982-10-11
DK347975A (en) 1976-02-03
IL47794A0 (en) 1975-11-25
IT1044406B (en) 1980-03-20
ATA599475A (en) 1982-07-15
AU8358275A (en) 1977-02-03
NL7509243A (en) 1976-02-04
FR2283104B1 (en) 1983-04-29
FR2283104A1 (en) 1976-03-26
CH618952A5 (en) 1980-08-29
CH618951A5 (en) 1980-08-29
NO138802B (en) 1978-08-07
FI752194A (en) 1976-02-03
NO752712L (en) 1976-02-03
JPS5140400A (en) 1976-04-05
SE426386B (en) 1983-01-17
FI64131C (en) 1983-10-10
IE42442L (en) 1976-02-02
FI64131B (en) 1983-06-30
GB1522182A (en) 1978-08-23
NL182859C (en) 1988-06-01
AT370067B (en) 1983-02-25
NZ178266A (en) 1978-04-03
CA1096582A (en) 1981-03-03
IL47794A (en) 1978-07-31
BR7504887A (en) 1976-08-31

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