LT3765440T - N-alkil-nitratoetilnitraminų gamybos būdas - Google Patents

N-alkil-nitratoetilnitraminų gamybos būdas

Info

Publication number
LT3765440T
LT3765440T LTEPPCT/EP2019/056379T LTEP2019056379T LT3765440T LT 3765440 T LT3765440 T LT 3765440T LT EP2019056379 T LTEP2019056379 T LT EP2019056379T LT 3765440 T LT3765440 T LT 3765440T
Authority
LT
Lithuania
Prior art keywords
nitratoethylnitramines
alkyl
preparation
Prior art date
Application number
LTEPPCT/EP2019/056379T
Other languages
English (en)
Inventor
Anian Nieder
Tobias WUENSCHE
Anne Theresa Friedrichs
Johannes Kainz
Alexander Huber
Original Assignee
Nitrochemie Aschau Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nitrochemie Aschau Gmbh filed Critical Nitrochemie Aschau Gmbh
Publication of LT3765440T publication Critical patent/LT3765440T/lt

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C241/00Preparation of compounds containing chains of nitrogen atoms singly-bound to each other, e.g. hydrazines, triazanes
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C243/00Compounds containing chains of nitrogen atoms singly-bound to each other, e.g. hydrazines, triazanes
    • C07C243/04N-nitroso compounds
    • C07C243/06N-nitroso-amines
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C241/00Preparation of compounds containing chains of nitrogen atoms singly-bound to each other, e.g. hydrazines, triazanes
    • C07C241/02Preparation of hydrazines
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • B01J19/002Avoiding undesirable reactions or side-effects, e.g. avoiding explosions, or improving the yield by suppressing side-reactions
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0093Microreactors, e.g. miniaturised or microfabricated reactors
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J3/00Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
    • B01J3/04Pressure vessels, e.g. autoclaves
    • B01J3/042Pressure vessels, e.g. autoclaves in the form of a tube
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C243/00Compounds containing chains of nitrogen atoms singly-bound to each other, e.g. hydrazines, triazanes
    • C07C243/02N-nitro compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002Chemical plants
    • B01J2219/00027Process aspects
    • B01J2219/00033Continuous processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00162Controlling or regulating processes controlling the pressure
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00788Three-dimensional assemblies, i.e. the reactor comprising a form other than a stack of plates
    • B01J2219/00792One or more tube-shaped elements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00851Additional features
    • B01J2219/00867Microreactors placed in series, on the same or on different supports
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/02Preparation of esters of nitric acid

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
LTEPPCT/EP2019/056379T 2018-03-15 2019-03-14 N-alkil-nitratoetilnitraminų gamybos būdas LT3765440T (lt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP18162059.2A EP3539943A1 (de) 2018-03-15 2018-03-15 Verfahren zur herstellung von n-alkyl-nitratoethylnitraminen
PCT/EP2019/056379 WO2019175296A1 (en) 2018-03-15 2019-03-14 Process for the preparation of n-alkyl-nitratoethylnitramines

Publications (1)

Publication Number Publication Date
LT3765440T true LT3765440T (lt) 2023-09-11

Family

ID=61692195

Family Applications (1)

Application Number Title Priority Date Filing Date
LTEPPCT/EP2019/056379T LT3765440T (lt) 2018-03-15 2019-03-14 N-alkil-nitratoetilnitraminų gamybos būdas

Country Status (15)

Country Link
US (1) US20190284131A1 (lt)
EP (2) EP3539943A1 (lt)
JP (1) JP7186792B2 (lt)
KR (1) KR102610017B1 (lt)
AU (1) AU2019233659B2 (lt)
CA (1) CA3092426C (lt)
DK (1) DK3765440T3 (lt)
ES (1) ES2960802T3 (lt)
FI (1) FI3765440T3 (lt)
HR (1) HRP20231004T1 (lt)
HU (1) HUE063118T2 (lt)
LT (1) LT3765440T (lt)
PL (1) PL3765440T3 (lt)
RS (1) RS64534B1 (lt)
WO (1) WO2019175296A1 (lt)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111763154A (zh) * 2019-04-01 2020-10-13 南京理工大学 一种二乙醇硝胺二硝酸酯的合成方法
CN111559964B (zh) * 2020-05-19 2021-04-20 启东市新晨企业管理咨询有限公司 一种硝酸甘油的绿色制备方法
CN115784924A (zh) * 2022-11-29 2023-03-14 天元航材(营口)科技股份有限公司 一种连续法制备高纯度Bu-NENA的新工艺

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2678946A (en) * 1944-12-30 1954-05-18 Us Navy Process of preparing nitroxy alkyl nitramines
CA2370145C (en) * 1999-10-14 2003-05-06 Dyno Nobel Asa Process of preparing a high-energy softening agent
US6262301B1 (en) 1999-10-15 2001-07-17 Dyno Asa Forsvarsprodukter Process of preparing a high-energy softening agent
ES2391601T3 (es) * 2007-12-20 2012-11-28 Dsm Fine Chemicals Austria Nfg Gmbh & Co Kg Formación de ésteres de nitrato en microreactores y milireactores usando una extracción de producto continua en un régimen de flujo turbulento
EP2172260A1 (en) 2008-09-29 2010-04-07 Corning Incorporated Multiple flow path microfluidic devices
CN101698646B (zh) 2009-11-04 2012-10-03 西安万德能源化学股份有限公司 一种硝酸异辛酯的连续生产工艺
EP2780304A1 (en) 2011-11-17 2014-09-24 Corning Incorporated Methods for asymmetric epoxidation using flow reactors

Also Published As

Publication number Publication date
JP7186792B2 (ja) 2022-12-09
AU2019233659B2 (en) 2021-04-29
HUE063118T2 (hu) 2024-01-28
EP3765440A1 (en) 2021-01-20
JP2021515795A (ja) 2021-06-24
DK3765440T3 (da) 2023-10-09
FI3765440T3 (fi) 2023-09-22
PL3765440T3 (pl) 2023-12-27
HRP20231004T1 (hr) 2023-12-08
RS64534B1 (sr) 2023-09-29
AU2019233659A1 (en) 2020-09-24
EP3539943A1 (de) 2019-09-18
CA3092426A1 (en) 2019-09-19
US20190284131A1 (en) 2019-09-19
KR20200133759A (ko) 2020-11-30
KR102610017B1 (ko) 2023-12-06
ES2960802T3 (es) 2024-03-06
WO2019175296A1 (en) 2019-09-19
CA3092426C (en) 2022-10-18
EP3765440B1 (en) 2023-07-19

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