KR960703956A - 아크릴릭-포화 고무 하이브리드 감압 접착제 - Google Patents

아크릴릭-포화 고무 하이브리드 감압 접착제

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Publication number
KR960703956A
KR960703956A KR1019960700058A KR19960700058A KR960703956A KR 960703956 A KR960703956 A KR 960703956A KR 1019960700058 A KR1019960700058 A KR 1019960700058A KR 19960700058 A KR19960700058 A KR 19960700058A KR 960703956 A KR960703956 A KR 960703956A
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South Korea
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macromer
graft copolymer
weight percent
graft
amount
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KR1019960700058A
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English (en)
Inventor
말리아 프라카쉬
씨 스미스 콜린
Original Assignee
로버트 지. 반 슌넨베르그
애버리 데니슨 코포레이션
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Publication of KR960703956A publication Critical patent/KR960703956A/ko

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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J155/00—Adhesives based on homopolymers or copolymers, obtained by polymerisation reactions only involving carbon-to-carbon unsaturated bonds, not provided for in groups C09J123/00 - C09J153/00
    • C09J155/005—Homopolymers or copolymers obtained by polymerisation of macromolecular compounds terminated by a carbon-to-carbon double bond
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08C—TREATMENT OR CHEMICAL MODIFICATION OF RUBBERS
    • C08C19/00—Chemical modification of rubber
    • C08C19/02—Hydrogenation
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08C—TREATMENT OR CHEMICAL MODIFICATION OF RUBBERS
    • C08C19/00—Chemical modification of rubber
    • C08C19/30—Addition of a reagent which reacts with a hetero atom or a group containing hetero atoms of the macromolecule
    • C08C19/34—Addition of a reagent which reacts with a hetero atom or a group containing hetero atoms of the macromolecule reacting with oxygen or oxygen-containing groups
    • C08C19/38—Addition of a reagent which reacts with a hetero atom or a group containing hetero atoms of the macromolecule reacting with oxygen or oxygen-containing groups with hydroxy radicals
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F265/00—Macromolecular compounds obtained by polymerising monomers on to polymers of unsaturated monocarboxylic acids or derivatives thereof as defined in group C08F20/00
    • C08F265/04—Macromolecular compounds obtained by polymerising monomers on to polymers of unsaturated monocarboxylic acids or derivatives thereof as defined in group C08F20/00 on to polymers of esters
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F290/00—Macromolecular compounds obtained by polymerising monomers on to polymers modified by introduction of aliphatic unsaturated end or side groups
    • C08F290/02—Macromolecular compounds obtained by polymerising monomers on to polymers modified by introduction of aliphatic unsaturated end or side groups on to polymers modified by introduction of unsaturated end groups
    • C08F290/04—Polymers provided for in subclasses C08C or C08F
    • C08F290/042—Polymers of hydrocarbons as defined in group C08F10/00
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J151/00—Adhesives based on graft polymers in which the grafted component is obtained by reactions only involving carbon-to-carbon unsaturated bonds; Adhesives based on derivatives of such polymers
    • C09J151/003—Adhesives based on graft polymers in which the grafted component is obtained by reactions only involving carbon-to-carbon unsaturated bonds; Adhesives based on derivatives of such polymers grafted on to macromolecular compounds obtained by reactions only involving unsaturated carbon-to-carbon bonds

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • General Chemical & Material Sciences (AREA)
  • Macromonomer-Based Addition Polymer (AREA)
  • Adhesives Or Adhesive Processes (AREA)

Abstract

에틸렌-부틸렌과 에틸렌-프로필렌 매크로머 그리고 그들의 혼합물로 이루어진 군에서 선택된 매크로머, 상기한 매크로머는 약 2,000 내지 30,000의 분자량, 약 0℃ 이하의 유리전이온도 그리고 아크릴레이트 또는 메타크릴레이의 말단 반응기를 갖는 매크로머의 존재하에서 약 4 내지 8개의 탄소 원자를 갖는 알킬기를 포함하는 적어도 하나 이상의 알킬아크릴레이트 에스테르를 포함하는 아크릴릭 모노머 시스템을 반응시킴으로써 감압 접착제 그라프트 공중합체를 제공한다.

Description

아크릴릭-포화 고무 하이브리드 감압 접착제
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (25)

  1. 에틸렌-부틸렌, 에틸렌-프로필렌 그리고 그들의 혼합물로 이루어진 있는 군에서 선택된 매크로머, 상기 매크로머의 각각은 약 2,000 내지 30,000의 분자량, 약 0℃ 이하의 유리전이온도와 아크릴레이트와 메타크릴레이트로 이루어진 군에서 선택되는 말단 반응기를 갖는 것인 매크로머의 존재하에서 약 4 내지 약 8개의 탄소 원자를 갖는 알킬기를 갖는 적어도 하나 이상의 알킬아크릴FP이트 에스테르를 포함하는 아크릴릭 모노머 시스템을 반응시킴으로써 형성되는 감압 접착제 그라프트 공중합체.
  2. 제 1항에 있어서, 상기 매크로머는 약 -20 내지 약 -50℃의 유리전이온도를 갖는 그라프트 공중합체.
  3. 제 1항에 있어서, 상기 아크릴릭 모노머 시스템은 약 95 내지 약 90중량%의 2-에틸헥실아크릴레이트와 약 5 내지 약 10중량%의 아크릴릭에시드를 포함하는 그라프트 공중합체.
  4. 제 2항에 있어서, 상기 아크릴릭 모노머 시스템은 약 95 내지 약 90중량%의 2-에틸헥실아크릴레이트와 약 5 내지 약 10중량%의 아크릴릭에시드를 포함하는 그라프트 공중합체.
  5. 제 1항에 있어서, 상기 매크로머는 매크로머와 아크릴릭 모노머 시스템이 5 내지 약 50중량%의 양으로 존재하는 그라프트 공중합체.
  6. 제 4항에 있어서, 상기 매크로머는 매크로머와 아크릴릭 모노머 시스템이 5 내지 약 50중량%의 양으로 존재하는 그라프트 공중합체.
  7. 제 1항에 있어서, 상기 매크로머는 매크로머와 아크릴릭 모노머 시스템이 10 내지 약 30중량%의 양으로 존재하는 그라프트 공중합체.
  8. 제 4항에 있어서, 상기 매크로머는 매크로머와 아크릴릭 모노머 시스템이 10 내지 약 30중량%의 양으로 존재하는 그라프트 공중합체.
  9. 제 1항에 있어서, 상기 매크로머는 매크로머와 아크릴릭 모노머 시스템이 15 내지 약 25중량%의 양으로 존재하는 그라프트 공중합체.
  10. 제 4항에 있어서, 상기 매크로머는 매크로머와 아크릴릭 모노머 시스템이 15 내지 약 25중량%의 양으로 존재하는 그라프트 공중합체.
  11. 제 1항에 있어서, 점착제, 가소제, 오일 그리고 그들의 혼합물로 이루어진 군에서 선택되는 매크로머 조절제가 존재하고, 상기 조절제는 실질적으로 자유 라디칼의 활성에 대하여 실질적으로 민감하지 않는 매크로머 조절제인 그라프트 공중합체.
  12. 제 4항에 있어서, 점착제, 가소제, 오일 그리고 그들의 혼합물로 이루어진 군에서 선택되는 매크로머 조절제가 존재하고, 상기 조절제는 실질적으로 자유 라디칼의 활성에 대하여 실질적으로 민감하지 않는 매크로머 조절제인 그라프트 공중합체.
  13. 제 7항에 있어서, 점착제, 가소제, 오일 그리고 그들의 혼합물로 이루어진 군에서 선택되는 매크로머 조절제가 존재하고, 상기 조절제는 실질적으로 자유 라디칼의 활성에 대하여 실질적으로 민감하지 않는 매크로머 조절제인 그라프트 공중합체.
  14. 제10항에 있어서, 점착제, 가소제, 오일 그리고 그들의 혼합물로 이루어진 군에서 선택되는 매크로머 조절제가 존재하고, 상기 조절제는 실질적으로 자유 라디칼의 활성에 대하여 실질적으로 민감하지 않는 매크로머 조절제인 그라프트 공중합체.
  15. 제11항에 있어서, 상기 매크로머 조절제는 매크로머 조절첨가물의 중량에 대하여 약 45 내지 약 70중량%의 양으로 존재하는 그라프트 공중합체.
  16. 제12항에 있어서, 상기 매크로머 조절제는 매크로머 조절첨가물의 중량에 대하여 약 45 내지 약 70중량%의 양으로 존재하는 그라프트 공중합체.
  17. 제 1항에 있어서, 상기 그라프트 중합체는 가교결합된 그라프트 공중합체.
  18. 제 4항에 있어서, 상기 그라프트 중합체는 가교결합된 그라프트 공중합체.
  19. 제12항에 있어서, 상기 그라프트 중합체는 가교결합된 그라프트 공중합체.
  20. 제17항에 있어서, 상기 그라프트 중합체는 가교결합제로서 알루미늄 아세틸아세톤에이트를 사용하여 가교결합된 그라프트 공중합체.
  21. 제18항에 있어서, 상기 그라프트 중합체는 가교결합제로서 알루미늄 아세틸아세톤에이트를 사용하여 가교결합된 그라프트 공중합체.
  22. 제20항에 있어서, 상기 가교결합제는 상기 중합체의 약 0.2 내지 약 0.3중량%의 양으로 존재하는 그라프트 공중합체.
  23. 제21항에 있어서, 상기 화학적인 가교결합제는 상기 중합체의 약 0.2 내지 약 0.3중량%의 양으로 존재하는 그라프트 공중합체.
  24. 아크릴레이트와 메타크릴레이트로 이루어진 군에서 선택되는 반응기의 말단기를 갖는 수소화된 에틸렌-부티렌 공중합체인 매크로머로서 상기 매크로머는 약 2,000 내지 30,000의 분자량과 약 0℃ 이하의 유리전이온도를 갖는 매크로머.
  25. 아크릴레이트와 메타크릴레이트로 이루어진 군에서 선택되는 반응기의 말단기를 갖는 수소화된 에틸렌-프로필렌 공중합체인 매크로머로서 상기 매크로머는 약 2,000 내지 30,000의 분자량과 약 0℃ 이하의 유리전이온도를 갖는 매크로머.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019960700058A 1993-07-08 1994-07-08 아크릴릭-포화 고무 하이브리드 감압 접착제 KR960703956A (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US8926093A 1993-07-08 1993-07-08
US08/089260 1993-07-08
PCT/US1994/007619 WO1995002003A1 (en) 1993-07-08 1994-07-08 Acrylic-saturated rubber hybrid pressure-sensitive adhesives

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KR960703956A true KR960703956A (ko) 1996-08-31

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Country Link
US (1) US5625005A (ko)
EP (1) EP0707604B1 (ko)
JP (1) JPH09502467A (ko)
KR (1) KR960703956A (ko)
AU (1) AU7324994A (ko)
DE (1) DE69424423T2 (ko)
TW (1) TW419516B (ko)
WO (1) WO1995002003A1 (ko)

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US5625005A (en) 1997-04-29
EP0707604A1 (en) 1996-04-24
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EP0707604B1 (en) 2000-05-10
DE69424423T2 (de) 2001-01-25
TW419516B (en) 2001-01-21

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