KR960014781B1 - Process for the preparation of toothpaste composition - Google Patents

Abstract

The process comprises inorganic composition prepared by the following steps : (1) pulverizing sericite, halloysite, muscovite, actinolite and steatite into a particle size having more than 280 mesh, after separating the inorganic matter from ore and drying,; (2) removing iron content from the pulverized said powder by means of adsorption, transmitting a magnetic force or stirring a magnet; (3) separating the powder by collecting the only powder, which can be dispersed in air, having a particle size more than 280 mesh among the powder removed iron, or which can be floatted on the upper portion of water having 10-20 times against the volume of the powder; (4) mixing the powder homogeneously via the above process in the proportion of 15-20 wt% of sericite, 30-50 wt.% of halloysite, 20-30 wt.% of muscovite, and 5-10 wt.% of actinolite; (5) plasticizing the mixed powder at 300-350deg.C for 30-60 min. by subjecting the powder to heat-treatment. Said inorganic composition get compounded 20-60 wt.% against the common toothpaste composition containing abrasive, damping agent, bonding agent, sweetening agent, antiseptic, medicine and spices.

Description

Toothpaste Composition

The present invention relates to a method for preparing a toothpaste composition containing a large amount of minerals that can promote oral health.

Various types of ointment or solid toothpaste, which are buried in ordinary toothbrushes before and after meals, are commercially available.These ingredients include various abrasives and surfactants as well as flavor components, skin protectants, and friction reinforcing agents. To obtain a variety of toothpaste compositions are provided.

In the present invention, an inorganic composition obtained by processing a mineral mixture containing a large amount of various inorganic components is blended with a conventional toothpaste composition. The inorganic composition of the present invention has been proved to be effective in the method of manufacturing a cosmetic soap of Korean Patent Publication No. 90-2937. The purpose of the present invention is to improve the oral health of the toothpaste by containing this component in toothpaste.

That is, the present invention is a known toothpaste composition composed of an abrasive, a humectant, a binder, a foaming agent, a sweetener, a preservative, a medicinal agent, a fragrance, etc., Sericite (Hillysite), Haloysite (Halloysite), Musco Combining bitcoin (Muscovite), actinite (Actinolite) and talc in a proportion, the inorganic composition (hereinafter referred to as "cerion composition") produced through the manufacturing process of grinding, iron removal and high temperature baking It is an object of the present invention to provide a method for manufacturing a new toothpaste composition that improves the resistance of teeth in oral skin protection.

Hereinafter, the method of manufacturing the toothpaste composition of the present invention will be described for each step.

[Inorganic composition manufacturing method]

1. Crushing process

Serisite, halosite, muscobite, actinite and talc ore are collected and thoroughly dried. In the sorting process, a large amount of unnecessary foreign matter is first sorted by a mechanical method, and then put into a conventional friction drum type or rotary grinding machine, and ground at a speed of at least 280 mesh by high-speed grinding.

2. De-ironing Process

A strong magnetic force line is transmitted through a powder pulverized drum or a conveyor belt that is primarily crushed so that iron is buried out of the powder along the magnetic line. In addition, the electromagnet is bent in the powder to sufficiently adsorb and remove iron.

3. Sorting process

1) Dry selection method

Air is blown at a speed at which the powder of 280 mesh or more is scattered in the air, and only the scattered powder is collected through a separate collection amount.

2) defense

The powder is suspended in 10 to 20 times of water and collected only for floating in the upper water layer. The dry method and the defensive method mentioned above can also be employ | adopted and used simultaneously.

4. Mixing process

Take 15 to 25% by weight of sericite, 30 to 50% by weight of halosite, 20 to 30% by weight of muscobite, 5 to 10% by weight of actinite, and 10 to 20% by weight of talc. .

5. Firing process

Those sufficiently trained in the compounding process are placed in a closed reducing furnace at 300-350 ° C. and left for at least 30 minutes.

[Toothpaste Manufacturing]

The cerion composition powder having the above firing process is cooled and blended with 20 to 60% by weight based on the weight of the known toothpaste composition. In other words, the more effective as possible, the better the effect, but if blended more than 60% by weight of the other components of the training is lowered because the extremely poor consistency is difficult to use. Since blending less than 20 weight% cannot exhibit the desired pharmacological effect originally, 20 weight% was made into the minimum compounding quantity.

The abrasive used in the present invention may be a mixture of one or two or more selected from calcium monohydrogen phosphate, precipitated silica, silica gel, calcium carbonate, hydrous alumina, insoluble sodium phosphate, calcium pyrophosphate, zirconium carbonate, hydroxyapatite and the like. 90% by weight is used, which can be adjusted according to the polishing power, application, efficacy and effect of the toothpaste, preferably 1 to 50% by weight is appropriate. The humectant prevents the toothpaste from solidifying when exposed to the air.The humectant is a mixture of one or two or more of polyhydric alcohols of sorbitol solution (70%), glycerin (TG), polyethylene glycol (PEG) and propylene glycol (PG). To 70% by weight.

The binder is any one of CMC (carboxymethylcellulose) which combines solid and liquid to prevent solid-liquid separation, calcium or sodium type of carrageenan, water-soluble polyvinylacrylic resin, polyvinylpyrrolidone, xanthan gum and magnesium aluminule silicate. Or 0.1 to 3.0% by weight of two or more mixtures.

Foaming agent acts more aggressively by lowering the interfacial tension, and is an anionic surfactant such as sodium alkyl sulfate, sodium lauroyl sarcoyl sulfate, polyoxyethylene polyoxypropylene condensation polymer material, polyoxyethylene curing 0.1 to 5% by weight of any one or a mixture of two or more of nonionic surfactants such as castor oil, polyoxyethylene sorbitan fatty acid ester, soletan fatty acid ester and sucrose fatty acid ester can be blended and the surface tension is 40 to 50 dyne / It is preferable that it is cm <2>.

As the sweetening agent, synthetic or natural non-fermentable sugars are mainly used. Examples of the sweeteners include sodium saccharin, aspartame, stevioside, acetosulfame, ammonium of licorice or licorice, potassium salt, isomerized sugar, sorbitol, etc. The amount of use is suitably 0.01 to 0.5% by weight.

The fragrance can be used by adding anise, methyl salicylate, lemon oil, eucalypton, cinnamon aldehyde, etc., with the theme of peppermint, spearmint, menthol, and guardbone, and the amount is 0.05 to 1.5% by weight.

In addition, 0.01 to 0.5% by weight of a food preservative for foods such as paraoxybenzoic acid ester, benzoic acid, sodium benzoate and salicylic acid can be used.

The cerion composition blended with the above toothpaste composition has been used for medicinal purposes since ancient times. Actinite is mixed with milky white, bluish-white to bluish-grey or yellowish brown color. Taken as a powder, halosite is effective for febrile diarrhea, intestinal bleeding, congestion, gastric ulcer, duodenal ulcer, vomiting, and trauma, and muscobite is effective for congestion, enteritis, diarrhea, traumatic bleeding, and venom.

Meanwhile, the following pharmacological effects of selenium contained in sericite have been reported. Nelson et al. (1943), Clock and Hendrick (1954), Bulgave and Chercus (1967) report that high concentrations of selenium are effective for cancer suppression. Schroeder and Michener (1971), Gardner (1973) and Van Howelling (1979) have been proven by Richard A. In addition to the pharmacologically effective action of selenium, the toothpaste composition containing the selenium powder composition of the present invention is produced in Dr. Passwater's "Selenium as a food and medicament" in US Connecticut, New Canaan, and Kids Publishing. Toothpaste composition containing a large amount of ultra rare metals.

In general, nutrients that are beneficial to the human body include large amounts such as C, H, N, P, O, and S, and macro minerals such as Na, K, Mg, Ca, Cl, PO ₄ , and SO ₄ . In addition, trace amounts such as Fe, Zn, and Ca are required, as well as non-metallic substances such as F, I, Se, Si, As, and B, and Mn, Mo, Co, V, Ni, Ca, Sn, There are metal materials such as Pb and Li.

Except for special cases such as fluorine and boron in the human body, the trace amount required for such traces is less than 10 mg in adults, and the chemical reactions in the human body for these components have not yet been experimentally identified, partially acknowledged, empirical, and result. Its significance is recognized as a theoretical experimental data. In other words, trace elements for living organisms, as stated in the paper "New Perspectives on the essential trace elements" (Florida State University, Tallahasse, Ulfried, V01. 62, 11, Nov. 1985). When the result of the stepwise test such as deficiency, titration, and toxicity is less or more than a certain amount, it is extremely toxic to the living body and has an extremely beneficial character.

In other words, while manganese is deficient in growth growth, bone malformation, biological membrane malformation, while adequate supply promotes carbohydrate metabolism, SOD mutagenicity is involved.

In the case of molybdenum, growth is inhibited when it is insufficient, but is involved in oxidase when titrated. In the case of cobalt, anemia and growth retardation is insufficient, and it becomes a component of vitamin B ₁₂ when titrated. Insufficient chromium also interferes with insulin secretion but contributes to insulin activation when titrated. Lack of barium also leads to growth inhibition, and when appropriate, it acts on the inhibition of Na-neurotransmission pump regulation and APT degrading enzymes.

Nickel reduces growth retardation, N utilization, and Fe metabolism when lacking, and becomes urease component when titrated, and hemolysis is reduced.

Cadmium delays growth and decreases regeneration when insufficient, and stimulates elongation of ribosomes when titrated.

Tin is delayed by growth and runs with flavin when titrated. Lead causes growth retardation and regeneration reduction when insufficient, and acts on Na pump when titrated.

Silicon is inhibited by growth, lack of bone and vesicle malformation, and plays a structural role in connective tissue and bone cells when appropriate. Arsenic causes problems with growth, regeneration, and heart rate when deficient, and is involved in the increase of arginine degradation and metabolism of methyl compounds when titrated. Boron is inhibited by nitrogen fixation and growth of anglos perm when insufficient, and is involved in membrane function, nucleic acid biosynthesis and lignin synthesis when titrated.

As described above, the toothpaste composition of the present invention containing a large amount of various metals or non-metallic materials essential for maintaining and regenerating the human body may help various resilience and regeneration of the human body for a long time to obtain various effective effects.

In other words, soils grown in heavily polluted metropolitan areas, or where pesticides or synthetic fertilizers are used, are acidified, and Ti, Mn, Co, Fe, Aℓ, Mg, Ca, Se, etc. are desorbed. As it is below 100 ~ 1/1000, such separate mineral supply has become essential in modern times, and the manufacturing method of toothpaste composition of the present invention is also completed based on such mineral supply, and these ingredients act on the tooth surface, oral surface, etc. during brushing. To exhibit the above pharmacological effect. As a result, it is effective in preventing and treating odor, tooth decay, bad breath, and oral cancer.

In other words, the minerals have been described as having a protective effect on peroxides during intracellular penetration, maintenance of cell respiration, hepatoprotection, promotion of detoxification of mutant attractants or cancer attractants, strengthening of myocardium, reduction of intravascular fibrosis or oxygen production. It has been identified as having a pharmacological effect. Most specifically, Dr. Klaus Schwarz (MD 1914-1978) demonstrated that selenium's anti-aging and immune-enhancing effects were attributed to selenium membrane protection, further improving the mitochondrial function of cells and prostaglandin hormones. It is directly involved in the production of analogues and has also demonstrated the effect of promoting excretion of cadmium heavy metals.

EXAMPLE

As a result of the actual use of the product of the present invention, the placebo effect is expected to be somewhat reduced, but the appearance of gums is reduced by at least three times. The infiltration into the gum epidermis of the mineral prevents excessive friction of the cells and at the same time, the fine mineral prevents excessive friction. It is also expected to suppress the direct friction of.

In addition, as the content of the cerion inorganic composition of the invention was increased, the prevention effect of epidermal appearance was excellent. Especially, the prevention of bad breath, the pain simplicity of the landscape patients, and the shortening of the treatment period of the stomatitis patients were more significant than the comparative examples.

Claims (1)

In the toothpaste composition consisting of abrasives, humectants, binders, foaming agents, sweeteners, preservatives, medicinal agents, fragrances, etc., after sericite, halosite, muscobite, actinite, talc ore is selected and dried, Grinding process to grind to 280 mesh or more, iron removal process to permeate magnetic wires or stir the magnets by stirring magnets, and to remove the iron by adsorbing and removing only iron powder. Screening process to collect only what has been made or to float the powder in 10-20 times of water and collect only what is suspended in the water layer, 15 to 20% by weight of sericite, 30 to 50 halidesite Blending process for homogeneous training at a ratio of weight%, muscobite 20-30% by weight, and actinite 5-10% by weight, and a firing process for heating the blended powder at a temperature of 300-350 ° C. for 30 to 60 minutes. A method for preparing a toothpaste composition, characterized in that 20 to 60% by weight of the inorganic composition prepared in the present invention is trained in a known toothpaste composition.