KR950007046B1 - The beauty wash containing a crude drug and it's preparation - Google Patents

The beauty wash containing a crude drug and it's preparation Download PDF

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KR950007046B1
KR950007046B1 KR1019920006037A KR920006037A KR950007046B1 KR 950007046 B1 KR950007046 B1 KR 950007046B1 KR 1019920006037 A KR1019920006037 A KR 1019920006037A KR 920006037 A KR920006037 A KR 920006037A KR 950007046 B1 KR950007046 B1 KR 950007046B1
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cinnamon
lotion
alum
skin
moisturizing
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KR930021192A (en
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이형주
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/26Aluminium; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin

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  • Health & Medical Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
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  • Engineering & Computer Science (AREA)
  • Dermatology (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Cosmetics (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The beauty wash contg. oriental herb medicine is prepd. by i) mixing 0.5-1.5 wt.% cinnamon bark, 0.5-1.5 wt.% momordicae semen, 0.35-1.05 wt.% alumen and pure water, ii) extracting the mixt. and filtering, and iii) concentrating the filted soln. to obtain the beauty wash of pH 4.5 and 40-50 Bx. contg. 3-4 w/v% cinnamon, 3-4 w/v% momordicae semen and 2-3 w/v% alumen.

Description

[발명의 명칭][Name of invention]

생약함유 화장수 및 그 제조방법Herbal lotion containing herbal medicine and its manufacturing method

[발명의 상세한 설명]Detailed description of the invention

본 발명은 생약을 함유한 신규의 화장수 및 그 제조방법에 관한것으로, 좀 더 부연하다면 계피(桂皮)와 목별자그리고 백반을 함유하며 보습의 지속정이 뛰어나고 해독작용을 갖는 화장수에 관한 것이다.The present invention relates to a novel cosmetic lotion containing a herbal medicine and a method for manufacturing the same, and more specifically, cinnamon and shepherds And alum Containing a moisturizing lotion containing excellent and lasting moisturizing.

종래부터, 계피(Cassiae Cortex 또는 Cinnamomi Cortex)는 중국 및 인도지나가 원산지이고 녹나무과(Lauraceae)에 속하는 상록의 교목인 계피나무(Cinnamomum Cassia Blume)의 줄기 및 가지의 껍질을 벗기어 코르크층을 다소 제거해서 말린것으로 정유성분인 신나믹알데히드(Cinnamic aldehyde), 신나밀 아세테이트(Cinnamyl acetate), 신나믹애시드(Cinnamic acid) 등이 주성분이고 그 밖에 유기산, 탄닌, 전분, 수지, 점액, 자당(mannitol) 및 광물성 물질등이 소량 들어있고, 한방에서는 방향성건위, 발한, 해열, 세균발육저지 및 방부수렴약 등으로 내복시에는 2∼4g을, 외용에는 정량이 없이 쓰이며, 또한 강한 향기를 갖는 계피유의 원료가 된다고 알려져 있다.Conventionally, the cinnamon (Cassiae Cortex or Cinnamomi Cortex) has been removed from the cork layer by peeling the stems and branches of Cinnamomum Cassia Blume, an evergreen tree that is native to China and Indochina and belongs to the family Lauraceae. Dried, the main ingredients are Cinnamic aldehyde, Cinnamic Acetate, Cinnamic acid, etc., and other organic acids, tannins, starches, resins, mucus, mannitol and minerals. It contains a small amount of substance, and in oriental medicine, it is used for aromatic dry stomach, sweating, antipyretic, bacteriostatic and antiseptic drugs. It is used as a raw material for cinnamon oil with 2-4g for internal use without quantification and for external use without quantification. Known.

그리고 목별자(Momordicae Semen)는 대만, 중국, 월남남부가 원산지이고 박과(Cucurbitaceae, 호로과라고도 한다)에 속하는 덩굴성 관목인 목별나무(Momordica Cochinsinensis sprenger)의 열매로서 원반형이며, 종자는 지방유가 들어있고 뿌리에는 사포닌 Momordin이 들어 있으며, 혈열(血熱)을 산(散)하여 종기독(癰毒)을 제거하는 요약으로 치질, 화농, 종기등에 내복시에는 1∼1.5g을, 외용에는 정량이 없이 쓴다고 알려져 있으며, 또한, 백반(Alumen)은 황산염류강에 속하며, 명반석(Alumite), 도토(Bolus) 점토등으로 제조하며 백색투명한 결정체[KA1(SO4)2·12H2O]로서, 수용액은 산성을 나타내며, 한방에서는 방수수렴제로서 분비를 저지하는 작용이 있어, 조습(燥濕), 해독, 지혈의 요약이 된다면 내복시 4-8g을, 외용에는 사용량의 제한없이 사용되어온 안전한 약물이다.Momordicae Semen is a fruit of the morphous shrub (Momordica Cochinsinensis sprenger), which is native to Taiwan, China and South and South Vietnam and belongs to the family Cucurbitaceae. The root contains saponin Momordin, and it is a summary that removes boil venom by acidifying blood fever, and it is 1 ~ 1.5g for internal use in hemorrhoids, purulent, boils, etc. Alumen is also belonging to sulfate steel, made of Alumite, Bolus clay, and white transparent crystals [KA1 (SO4) 2.12H2O]. In oriental medicine, it acts as a waterproofing astringent to prevent secretion, so if the summary of humidity (燥濕), detoxification, hemostasis 4-8g in internal use, it is a safe drug that has been used without restriction on the external use.

그러나, 지금까지 계피의 세균발육저지 및 방부 수렴작용과 특이한 계피향의 방향성, 목별자의 화농, 종기 및 화장독의 해독작용 그리고 백반의 피부 생육보호작용 및 방부 수렴작용등의 복합적인 상승작용에 의한 피부용 화장수 조성물의 개발은 전무하였다.However, until now, it is used for skin by complex synergistic effects such as bacteriostatic action of cinnamon and antiseptic convergence, specific cinnamon scent, shepherd purulent, boil and crematory detoxification and virulent skin growth protection and antiseptic convergence. There was no development of the lotion composition.

종래의 예를든다면 오이와 마를 주재로 하여 추출액에 부패를 방지하기 위한 살구씨(벤조알데히드)를 함유하는 세안세제가 개발된바 있으나 제제의 안정성, 화장독의 해독 및 보습효과가 바람직하지 못하였고(특허공고번호 제86-1560호 참조), 화장수를 포함한 스킨제어용 화장품의 보습작용을 충분히 주기위하여 종래 보습제와 함께 프로테오제펩톤을 첨가하여 높은 습도하에서도 끈적끈적 달라붙는 감촉을 줄일수 있는 방법이 소개되어 있으며(특허공고번호 제88-2222호 참조), 그 외에도 신선하고 피부에 독성이 적고 미용효과를 주기 위할 목적으로 살구씨, 녹차, 황금 및 프라센타의 추출물을 함유한 세안용 수렴 화장수가 개발되어 있고, 상백피, 백작약, 고삼, 감초의 생약성분을 함유한 화장수가 역시 제품화된바 있으나, 이들은 모두 제품의 안정성을 위하여 방부제나 보존제등의 안정화제를 필수적으로 포함할 뿐만 아니라 보습성의 지속효과도 바람직하지 못한 결점이 있었다.For example, cleansing agents containing apricot seed (benzoaldehyde) to prevent corruption in extracts have been developed mainly based on cucumbers and hemps, but the stability of the preparations, detoxification and moisturizing effects were not desirable. (See Patent Publication No. 86-1560), How to reduce the sticky texture even under high humidity by adding protease peptone together with the conventional moisturizer to sufficiently moisturize the skin control cosmetics including the lotion. (See Patent Publication No. 88-2222), besides, it is fresh, less toxic to the skin, and for the purpose of giving a cosmetic effect, facial cleansing astringents containing extracts of apricot seed, green tea, golden and placenta It has been developed, and cosmetic lotion containing herbal ingredients of lettuce, white ginseng, red ginseng and licorice has also been commercialized, but they are all stable To only essential to include a stabilizer, such as a preservative or as a preservative had a drawback undesirable FIG Passive Castle moisturizing.

따라서, 본 발명자들은 이와같은 결점을 보완함은 물론 천연생약의 추출물을 함유하는 화장수의 개발에 전념하던중, 천연생약중 단미제로서는 안정성이 확보된바 있는 세균발육억제, 방부수렴작용, 방향성을 갖는 계피를 화장수 주성분으로 함유하고, 피부해독작용, 화장해독작용을 갖는 목별자를 보조성분으로 함유하며, 방부수렴작용, 조습 및 해독작용을 갖는 백반을 기타 보조성분으로 함유하는 본 발명의 신규 화장수를 개발하고, 이를 특허로서 출원하는 바이다.Therefore, the inventors of the present invention, while devoted to the development of a lotion containing the extract of natural herbs, as well as to compensate for such drawbacks, the bacterium growth inhibitory, antiseptic convergence, fragrance that has been secured as a sweetener in natural herbs A novel lotion of the present invention containing cinnamon having a main ingredient as a cosmetic lotion, a woody detoxifying agent and a deciduous detoxifying agent as an auxiliary ingredient, and containing alum with other antiseptic, moisturizing and detoxifying functions as other auxiliary ingredients. Developed and filed as a patent.

본 발명에 따른 화장수는 계피와 목별자 그리고 백반의 정체수추출용액을 적당한 조도로 농축한후 제품화 하는것으로, 계피와 목별자 그리고 백반의 조성비율 0.5∼1.5 : 0.5∼1.5 : 0.35∼1.05, 바람직하게는 1 : 1 : 0.7의 중량비율로 혼합한후 100℃에서 정제수로 추출하고, 추출액으로부터 계피와 목별자의 잔사를 제거한 후, 증발, 농축시켜 계피 3∼4w/v%, 목별자 3∼4w/v%, 백반 2∼3w/v% 그리고 물을 함유하는 pH 4.5, 조도 40∼50°의 화장수를 얻는 것이다.The skin lotion according to the present invention is a product of concentrated cinnamon and wood starch and vitilized water extraction solution of alum with suitable roughness, and the composition ratio of cinnamon, wood starch and alum is 0.5 to 1.5: 0.5 to 1.5: 0.35 to 1.05, preferably Preferably, the mixture is mixed at a weight ratio of 1: 1: 0.7, extracted with purified water at 100 ° C, the residues of cinnamon and shepherd are removed from the extract, and then evaporated and concentrated to make 3-4w / v% cinnamon and 3-4w shepherd. A lotion having a pH of 4.5 and a roughness of 40 to 50 ° containing / v%, alum 2 to 3w / v% and water.

본 발명을 수행함에 있어 0.5중량부 이하의 계피의 사용은 계피향이 미진하고 1.5중량부 이상의 사용은 제제의 안정성을 해쳐 화장수로서 이용이 어려워지며, 0.5중량부 이하의 목별자를 함유시는 화장독 해독작용이나 보습력이 크게 떨어져 보습효과에 문제점이 있으며, 1.5중량부 이상의 함유는 보습성은 좋아지나 화장수에 퍽퍽한 질감이 있다. 백반의 함유량이 0.35중량부 이하로 갈수록 제제의 안정성에 나쁜 영향을 미치며 1.5중량부 이상이면 피부가 거칠어지고 건조해지는 결점이 있다.In the practice of the present invention, the use of cinnamon of 0.5 parts by weight or less is less cinnamon and the use of 1.5 parts by weight or more deteriorates the stability of the formulation, making it difficult to use as a lotion, crematory detoxifying action containing 0.5 parts by weight or less However, there is a problem in the moisturizing effect is greatly reduced moisturizing effect, containing more than 1.5 parts by weight of moisturizing is good but there is a puffy texture in the lotion. As the content of alum increases to 0.35 parts by weight or less, it adversely affects the stability of the preparation, and when it is 1.5 parts by weight or more, the skin becomes rough and dried.

본 발명의 화장수는 계피와 목별자, 백반 성분외에는 타 보존제나 향료, 안정화제가 포함되지 않아도 제제학적으로 매우 안정한 제제를 이룰수 있다는 장점과, 피부에 대한 친화력도 좋았으며 3일정도 장시간의 보습효과가 지속되었고, 피부에 윤기를 부여하고 건강하고 반들반들한 피부를 유지시키며, 화장독 및 피지에 의한 화농의 억제로 지루성 여드름에 탁월한 효과가 있는 미용 화장수이다.The skin lotion of the present invention has the advantage of being able to form a very stable formulation even without other preservatives, fragrances and stabilizers other than cinnamon, wood, and alum, and affinity for the skin. It is a beauty lotion that lasts, gives skin shine, maintains healthy and smooth skin, and has an excellent effect on seborrheic acne by suppressing suppuration by cremation poison and sebum.

이하 실시예를 들어 본 발명을 상세히 기재한다.The present invention is described in detail with reference to the following Examples.

[실시예 1]Example 1

세절하고 분발화된 계피 3.75kg, 목별자 3.75kg 및 백반 2.625kg을 170리터의 정제수로 100℃에서 추출한후, 추출액으로부터 계피와 목별자 잔사를 여과, 제거한다.3.75 kg of finely divided cinnamon, 3.75 kg of shepherds and 2.625 kg of alum are extracted with 170 liters of purified water at 100 ° C., and then filtered and removed from the extract.

여액이 100리터가 될때가지 증발, 농축시키고 냉각하여 pH 4.5, 조도 40∼50℃의 화장수를 얻는다.Evaporate, concentrate and cool until the filtrate reaches 100 liters to obtain a lotion having a pH of 4.5 and a roughness of 40 to 50 ° C.

〈화장수 용액 조성〉<Cosmetic solution composition>

계피 3.75kg3.75 kg of cinnamon

목별자 3.75kgShepherd 3.75kg

백반 2.625kgAluminous 2.625kg

물 89.875kgWater 89.875kg

[실시예 2-10]Example 2-10

계피 : 목별자 : 백반의 혼합조성비율을 1 : 1 : 0.7중량부를 준수하되 하기 표 1과 같은 분량으로 혼합한 후 실시예 1의 방법에 따라 처리하여 제품으로 한다. 그러나 하기 표 1에서와 같이 실시예 2 내지 7에서 얻는 추출액은 농축하고, 실시예 8 내지 10에서 얻은 추출액은 희석시키는 후처리 공정을 수행하여, 실시예 1의 화장수 용액 조성비율과 동일하게 조절하여 제품화 할수 있음을 잘 알수 있다.Cinnamon: Woodpecker: mixed ratio of alum and 1: 1: 0.7 parts by weight to comply with the same amount as in the following Table 1 after the treatment according to the method of Example 1 to give a product. However, as shown in Table 1 below, the extracts obtained in Examples 2 to 7 were concentrated, and the extracts obtained in Examples 8 to 10 were subjected to a post-treatment process to be diluted, and adjusted in the same manner as the cosmetic solution composition ratio of Example 1 You can see that it can be commercialized.

[표 1]TABLE 1

[비교예 1-3]Comparative Example 1-3

실시예 1에 따르되 계피 : 목별자 : 백반의 혼합조성비율을 하기 표 2에서와 같이 조성된 생약으로부터 화장수를 얻었다.According to Example 1, but cinnamon: shepherd: the mixed composition ratio of alum was obtained a lotion from the herbal composition as shown in Table 2.

[표 2]TABLE 2

[혼합비율에 따른 제제의 안정성 실험][Stability Test of Formulation According to Mixing Ratio]

실시예 1의 제품과 비교예 1-3의 대조품에 대하여 각 제제에 대하여 하기와 같이 안정성을 실험한 결과, 표 3에 기재된 바와 같이 본 발명에 따른 실시예 1의 제품은 제제학적으로도 매우 안정한 화장수임을 알수 있다.As a result of experiments on the stability of each product with respect to the product of Example 1 and the control products of Comparative Examples 1-3, as shown in Table 3, the product of Example 1 according to the present invention is very pharmaceutical You can see that it is a stable lotion.

[표 3]TABLE 3

[혼합비율에 따른 효과실험][Effect Experiment by Mixing Ratio]

실시예 1의 제품과 비교예 1-3의 대조품에 대하여 15세∼45세의 여성패널에 의한 화장수 사용감의 평가 테스트(블라인드테스트 ; 시험조건 : 25℃, 70%RH)를 행하였다.The evaluation test (blind test; test condition: 25 degreeC, 70% RH) of the cosmetics use feeling by the 15-45 year old female panel was done about the product of Example 1, and the control product of Comparative Examples 1-3.

그 결과는 다음의 표 4와 같으며, 실시예 1 제품은 대조품에 비하여 피부에 대한 친화감, 보습성, 윤택성, 피부의 윤기 및 화장독해독에 탁월하며 끈적끈적한 감도 없는 훌륭한 화장수임을 알수 있다.The results are shown in Table 4 below, and Example 1 product is excellent in affinity for skin, moisturizing, moisturizing, skin shine and detoxification of skin compared to the control, and it can be seen that it is an excellent lotion without sticky sensitivity.

[표 4]TABLE 4

주) A : 매우많다 B : 많다A) Very many B: Many

C : 보통 D : 거의없다C: Normal D: Almost none

숫자는 실험에 응한 여성패널인원수The number of female panelists who responded to the experiment

[실시예에 따른 효과실험][Effect Experiment According to Example]

본 발명의 최량의 태양인 실시예 1의 제품과 조성비율을 달리한 실시예 2 내지 10에 따라 제조되고 농축이나 희석등의 후처리하지 않은 상태에서의 제품과의 효과실험을 여성패널에 대하여 수생한 결과를 하기 표 5에 기재하였다. 여성패널에 대하여 표 5에 결과로부터 계피 : 목별자 : 백반을 1 : 1 : 0.7 비율로 혼합하여 정제수로 추출하되 최종조성이 계피 3-4w/v%, 목별자 3∼4w/v% 그리고 백반 2-3w/v%를 함유하는 실시예 1을 비롯하여 실시예 6,7,8에 따라 제조된 화장수가 피부의 친화감, 보습성, 윤택성, 화장독해독 작용이 탁월한 제품임을 알수 있다.The effects of the product of Example 1, which is the best embodiment of the present invention, and the product prepared according to Examples 2 to 10 with different composition ratios, and the product without the post-treatment such as concentration or dilution, were aquatic for female panels. The results are shown in Table 5 below. The results from the results in Table 5 for the female panel were extracted with purified water by mixing the ratio of cinnamon: alum: alum in a ratio of 1: 1: 0.7, and the final composition was 3-4w / v% cinnamon, 3-4w / v% of alum It can be seen that the lotion prepared according to Examples 6, 7, and 8, including Example 1 containing 2-3w / v%, was excellent in skin affinity, moisturizing, moisturizing, and detoxification.

[표 5]TABLE 5

주) A : 매우많다 B : 많다A) Very many B: Many

C : 보통 D : 거의없다C: Normal D: Almost none

숫자 : 실험에 응한 여성패널인원수Number: Number of female panelists who responded to the experiment

실험방법 및 조건 : 블라인드테스트, 25℃, 70% RHExperiment method and condition: Blind test, 25 ℃, 70% RH

Claims (4)

계피와 목별자 그리고 백반의 혼합분말을 정제수로 추출하고 여액을 증발, 농축시켜 얻은 계피 3∼4w/v%, 목별자 3∼4w/v%, 백반 2∼3w/v%를 포함하는 pH 4.5, 조도 40∼50°의 생약함유 화장수.PH 4.5 containing 3-4w / v% cinnamon, 3-4w / v% woody, 2-3-3w / vy woody, obtained by extracting mixed powder of cinnamon, wood and alum with purified water and evaporating and concentrating the filtrate. , Herbal lotion with roughness 40-50 °. 제1항에 있어서, 계피와 목별자 그리고 백반의 혼합 비율이 0.5∼1.5 : 0.5∼1.5 : 0.35 ∼1.05중량부임을 특징으로 하는 화장수.The skin lotion according to claim 1, wherein the mixing ratio of cinnamon, wood, and alum is 0.5 to 1.5: 0.5 to 1.5: 0.35 to 1.05 parts by weight. 제2항에 있어서, 계피와 목별자 그리고 백반의 혼합비율이 1 : 1 : 0.7임을 특징으로 하는 화장수.The lotion according to claim 2, wherein the mixing ratio of cinnamon, shepherd and alum is 1: 1: 0.7. 제1항에 있어서, 계피 0.75w/t%, 목별자 3.75w/t%, 백반 2.625w/t% 그리고 나머지가 정제수인 화장수.The lotion according to claim 1, wherein cinnamon 0.75w / t%, shepherd 3.75w / t%, alum 2.625w / t% and the remainder are purified water.
KR1019920006037A 1992-04-11 1992-04-11 The beauty wash containing a crude drug and it's preparation KR950007046B1 (en)

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US8158168B2 (en) 2005-12-20 2012-04-17 Sk Chemicals Co., Ltd. Anti-gastritis and anti-ulcer agent containing Momordicae semen extract and momordica saponin I isolated from the same
KR102122757B1 (en) * 2020-01-23 2020-06-17 협동조합 바이오융합기술 Composition for elimination of fine dust and adding of moisture to skin using antioxidant saponin

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KR100368126B1 (en) * 2000-10-06 2003-01-24 주식회사 태평양 Composition capable of inhibiting sebum secretion
KR20020044266A (en) * 2000-12-05 2002-06-15 양봉철 Skin protective cosmetic composition comprising extracts from complex crude drugs
KR20020044267A (en) * 2000-12-05 2002-06-15 양봉철 Cosmetic composition for skin whitening comprising an extract from rubus coreanus miq
KR100490365B1 (en) * 2002-04-25 2005-05-17 한불화장품주식회사 Cosmetics including nanovesicle

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8158168B2 (en) 2005-12-20 2012-04-17 Sk Chemicals Co., Ltd. Anti-gastritis and anti-ulcer agent containing Momordicae semen extract and momordica saponin I isolated from the same
KR102122757B1 (en) * 2020-01-23 2020-06-17 협동조합 바이오융합기술 Composition for elimination of fine dust and adding of moisture to skin using antioxidant saponin

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