KR940003840A - 고순도 디보란의 제조방법 - Google Patents

고순도 디보란의 제조방법 Download PDF

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Publication number
KR940003840A
KR940003840A KR1019920014448A KR920014448A KR940003840A KR 940003840 A KR940003840 A KR 940003840A KR 1019920014448 A KR1019920014448 A KR 1019920014448A KR 920014448 A KR920014448 A KR 920014448A KR 940003840 A KR940003840 A KR 940003840A
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KR
South Korea
Prior art keywords
dimethyl ether
glycol dimethyl
diborane
solution
boron halide
Prior art date
Application number
KR1019920014448A
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English (en)
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KR950010793B1 (ko
Inventor
이사오 아카마
다케오 사세
이사무 미나가와
다이조 이치다
Original Assignee
오세 고오노스케
다이요산소 가부시키가이샤
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Application filed by 오세 고오노스케, 다이요산소 가부시키가이샤 filed Critical 오세 고오노스케
Priority to KR1019920014448A priority Critical patent/KR950010793B1/ko
Publication of KR940003840A publication Critical patent/KR940003840A/ko
Application granted granted Critical
Publication of KR950010793B1 publication Critical patent/KR950010793B1/ko

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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B6/00—Hydrides of metals including fully or partially hydrided metals, alloys or intermetallic compounds ; Compounds containing at least one metal-hydrogen bond, e.g. (GeH3)2S, SiH GeH; Monoborane or diborane; Addition complexes thereof
    • C01B6/06—Hydrides of aluminium, gallium, indium, thallium, germanium, tin, lead, arsenic, antimony, bismuth or polonium; Monoborane; Diborane; Addition complexes thereof
    • C01B6/10—Monoborane; Diborane; Addition complexes thereof

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

본 발명은 할로겐화 붕소를 액온 0∼30℃로 보지한 글리콜 디메틸에텔 용매중에 용해하므로써 할로겐화 붕소-글리콜 디메틸에텔 부가화합물을 냉각하에서 생성시킨 다음 이 반응혼합물을 30∼40℃로 가온한 후, 이 용액에 별도 조제한 알카리금속 붕수소화믈의 글리콜 디메틸에텔 용액을 혼합하여 디보란 합성을 위한 반응을 행하는 것을 포함하는 고순도 디보란 제조방법에 관한 것이다.

Description

고순도 디보란의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (2)

  1. 할로겐화 붕소를 액온 0-30℃로 보지한 글리콜 디메틸에텔 용매중에 용해하므로써 할로겐화 붕소-글리콜 디메틸에텔 부가화합물을 냉각하에서 생성시켜, 이어 이 반응액을 30-40℃로 가온한 후, 이 용액에 별도조제한 알카리금속 붕수소화물의 글리콜 디메틸에텔 용액을 혼합하여 디보란 합성을 위한 반응을 하는 것을 특징으로 하는 고순도 디보란의 제조방법.
  2. 제 1 항에 있어서, 글리콜 디메틸에텔은 디에틸렌 글리콜 디메틸에텔임을 특징으로 하는 제조방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019920014448A 1992-08-11 1992-08-11 고순도 디보란의 제조방법 KR950010793B1 (ko)

Priority Applications (1)

Application Number Priority Date Filing Date Title
KR1019920014448A KR950010793B1 (ko) 1992-08-11 1992-08-11 고순도 디보란의 제조방법

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
KR1019920014448A KR950010793B1 (ko) 1992-08-11 1992-08-11 고순도 디보란의 제조방법

Publications (2)

Publication Number Publication Date
KR940003840A true KR940003840A (ko) 1994-03-12
KR950010793B1 KR950010793B1 (ko) 1995-09-23

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ID=19337836

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019920014448A KR950010793B1 (ko) 1992-08-11 1992-08-11 고순도 디보란의 제조방법

Country Status (1)

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KR (1) KR950010793B1 (ko)

Also Published As

Publication number Publication date
KR950010793B1 (ko) 1995-09-23

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