KR940002290A - 코팅의 광-보조 경화방법 - Google Patents

코팅의 광-보조 경화방법 Download PDF

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KR940002290A
KR940002290A KR1019930014387A KR930014387A KR940002290A KR 940002290 A KR940002290 A KR 940002290A KR 1019930014387 A KR1019930014387 A KR 1019930014387A KR 930014387 A KR930014387 A KR 930014387A KR 940002290 A KR940002290 A KR 940002290A
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coating
acetoacetyl
substrate
ammonia
primary amine
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KR1019930014387A
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KR100303124B1 (ko
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아서 보어스 다니엘
스코트 에드워드스 스티븐
데이비드 이몽스 윌리엄
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윌리엄 이. 램버트 3세
롬 앤드 하스 캄파니
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
    • C09D133/04—Homopolymers or copolymers of esters
    • C09D133/06—Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, the oxygen atom being present only as part of the carboxyl radical
    • C09D133/10—Homopolymers or copolymers of methacrylic acid esters
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
    • C09D133/04—Homopolymers or copolymers of esters
    • C09D133/14—Homopolymers or copolymers of esters of esters containing halogen, nitrogen, sulfur or oxygen atoms in addition to the carboxy oxygen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D3/00—Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials
    • B05D3/06—Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials by exposure to radiation
    • B05D3/061—Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials by exposure to radiation using U.V.
    • B05D3/065—After-treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D7/00—Processes, other than flocking, specially adapted for applying liquids or other fluent materials to particular surfaces or for applying particular liquids or other fluent materials
    • B05D7/24—Processes, other than flocking, specially adapted for applying liquids or other fluent materials to particular surfaces or for applying particular liquids or other fluent materials for applying particular liquids or other fluent materials
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F8/00—Chemical modification by after-treatment
    • C08F8/44—Preparation of metal salts or ammonium salts
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D157/00—Coating compositions based on unspecified polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C09D157/06—Homopolymers or copolymers containing elements other than carbon and hydrogen
    • C09D157/12—Homopolymers or copolymers containing elements other than carbon and hydrogen containing nitrogen atoms
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/31504—Composite [nonstructural laminate]
    • Y10T428/31855—Of addition polymer from unsaturated monomers
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/31504—Composite [nonstructural laminate]
    • Y10T428/31942—Of aldehyde or ketone condensation product

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Wood Science & Technology (AREA)
  • Life Sciences & Earth Sciences (AREA)
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  • Chemical Kinetics & Catalysis (AREA)
  • Polymers & Plastics (AREA)
  • Health & Medical Sciences (AREA)
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  • General Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Plasma & Fusion (AREA)
  • Paints Or Removers (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Surface Treatment Of Glass Fibres Or Filaments (AREA)
  • Other Resins Obtained By Reactions Not Involving Carbon-To-Carbon Unsaturated Bonds (AREA)
  • Macromonomer-Based Addition Polymer (AREA)
  • Polymerisation Methods In General (AREA)
  • Optical Fibers, Optical Fiber Cores, And Optical Fiber Bundles (AREA)
  • Graft Or Block Polymers (AREA)
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Abstract

본 발명은 코팅의 경화속도를 증대시키기에 충분한 엔아민 함량을 코팅제에 부가하여 이루어지는 코팅의 광-보조 경화 방법에 관한 것으로, (a) 아세토아세틸 작용기를 갖는 비닐 중합체를, 이 아세토아세틸기를 엔아민으로 전환시기기에 충분한 양의 암모니아 또는 일차 아민과 혼합하고, (b) 반응물이 평형이 되기에 충분한 시간동안 이 혼합물을 저장하고. (c) pH를 9로 상승시키기에 충분한 양의 암모니아 또는 일차 아민을 첨가하고 (d) 코팅제가 기재에 처리될 때까지 pH를 9로 유지하는 것을 특징으로 하는 코팅제의 제조방법을 제공한다.
이 코팅은 광에 노출시켰을 때에는 개선된 내후성과 광택유지를 나타낸다.

Description

코팅의 광-보조 경화방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (10)

  1. 자외선에 노출되는 기재에 처리하는 코팅제의 제조방법에 있어서, (a)아세토아세틸 작용기를 갖는 비닐중합체를, 이 아세토아세틸기를 엔아민으로 전환시기기에 충분한 양의 암모니아 또는 일차 아민과 혼합하고, (b)반응물이 평행이 되기에 충분한 시간동안 이 혼합물을 저장하고, (c) pH를 9로 상승시키기에 충분한 양의 암모니아 또는 일차 아민을 첨가하고 (d) 코팅제가 기재에 처리될 때까지 pH를 9로 유지하는 것을 특징으로 하는 방법.
  2. 제1항에 있어서, pH가 9.5로 조절되는 것을 특징으로 하는 방법.
  3. 기재표면상에 경화된 코팅을 제조하는 방법에 있어서, 제1항에 의해 제조된 코팅제를 기재에 처리하고, 코팅된 기재를 요망되는 정도외 경화가 이루어지기에 충분한 시간 동안 자외선에 노출시키는 것을 특징으로 하는 방법.
  4. 태양광에 노출되었을 때에 향상된 경화속도를 나타내는 외부 코팅을 아세토아세틸기를 갖고 있는 비닐 중합체로부터 제조하는 방법어 있어서, (a) 아세토아세틸 작용기를 갖는 비닐 중합체를, 아세토아세틸기를 엔아민으로 전환시기기에 충분한 양의 암모니아 또는 일차 아민과 혼합하고, (b) 반응물이 평행이 되기에 충분한 시간동안 이 혼합물을 저장하고, (c) pH를 9로 상승시키기에 충분한 양의 암모니아 또는 일차 아민을 첨가하고 (d) 코팅제가 기재에 처리될 때까지 pH를 9로 유지하고 (e) 이 코팅제를 기재상에 처리하고, (f) 기재상에 처리된 코팅을 태양광에 소정시간 이상 노출시키는 것을 특징으로 하는 방법.
  5. 제1항의 방법으로 만든 생성물로 되는 코팅.
  6. 촉진된 광경화능력을 나타내는 아세토아세틸 작용기를 갖는 비닐중합체로부터 제조되는 외부코팅으로써, 수성 매체중의 아세토아세틸 작용성 중합체와, 아세토아세틸 작용기 및 공중합된 산기를 기준으로 과잉몰의 암모니아 또는 일차 아민으로 이루어지고, pH 9로 조절된 것을 특징으로 하는 외부 코팅.
  7. 아세토아세틸기를 암모니아 또는 일차 아민과 반응시킨 생성물인 엔아민 작용기를 가진 비닐 중합체로 이루어지며, pH가 9로 조절된 외부 코팅조성물.
  8. 제7항에 있어서, 코팅의 pH 9.5인 것을 특징으로 하는 코팅 조성물.
  9. 제7항에 있어서. 상기 중합체가 비전환 아세토아세틸기를 함유하지 않는 것을 특징으로 하는 코팅 조성물.
  10. 제8항에 있어서, 상기 중합체가 비전환 아세토아세틸기를 함유하지 않는 것을 특징으로 하는 코팅 조성물.
    ※ 참고사항 : 최초출월 내용에 의하여 공개하는 것임.
KR1019930014387A 1992-07-28 1993-07-28 코팅의광-보조경화방법 KR100303124B1 (ko)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
JP920,972 1992-07-28
US07/920,972 US5296530A (en) 1992-07-28 1992-07-28 Method for light-assisted curing of coatings
US920,972 1992-07-28
JP92-211546 1992-08-07

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KR940002290A true KR940002290A (ko) 1994-02-17
KR100303124B1 KR100303124B1 (ko) 2001-11-22

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US (2) US5296530A (ko)
EP (1) EP0584916B1 (ko)
JP (1) JP3611587B2 (ko)
KR (1) KR100303124B1 (ko)
CN (2) CN1055945C (ko)
AT (1) ATE142243T1 (ko)
AU (1) AU668728B2 (ko)
BR (1) BR9303010A (ko)
CA (1) CA2100985A1 (ko)
CZ (1) CZ153793A3 (ko)
DE (1) DE69304472T2 (ko)
FI (1) FI933356A (ko)
HK (1) HK216796A (ko)
HU (1) HU9302174D0 (ko)
IL (1) IL106331A0 (ko)
MX (1) MX9304213A (ko)
MY (1) MY110672A (ko)
NO (1) NO932626L (ko)
PL (1) PL299813A1 (ko)
SI (1) SI9300400A (ko)
SK (1) SK78893A3 (ko)
TW (1) TW264507B (ko)
ZA (1) ZA935226B (ko)

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CN1084537A (zh) 1994-03-30
CN1331960C (zh) 2007-08-15
CN1263135A (zh) 2000-08-16
AU668728B2 (en) 1996-05-16
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CZ153793A3 (en) 1994-03-16
US5562953A (en) 1996-10-08
US5296530A (en) 1994-03-22
CA2100985A1 (en) 1994-01-29
FI933356A0 (fi) 1993-07-27
DE69304472D1 (de) 1996-10-10
ATE142243T1 (de) 1996-09-15
DE69304472T2 (de) 1997-02-20
MY110672A (en) 1999-01-30
MX9304213A (es) 1994-04-29
FI933356A (fi) 1994-01-29
TW264507B (ko) 1995-12-01
HU9302174D0 (en) 1993-11-29
EP0584916A3 (en) 1994-06-15
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JP3611587B2 (ja) 2005-01-19
NO932626D0 (no) 1993-07-21
EP0584916A2 (en) 1994-03-02
KR100303124B1 (ko) 2001-11-22
BR9303010A (pt) 1994-02-16
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EP0584916B1 (en) 1996-09-04
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