KR930702263A - 신규의 화합물 및 분리제 - Google Patents

신규의 화합물 및 분리제

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Publication number
KR930702263A
KR930702263A KR1019930701370A KR930701370A KR930702263A KR 930702263 A KR930702263 A KR 930702263A KR 1019930701370 A KR1019930701370 A KR 1019930701370A KR 930701370 A KR930701370 A KR 930701370A KR 930702263 A KR930702263 A KR 930702263A
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KR
South Korea
Prior art keywords
compound
guest
optical isomer
separation
mixture
Prior art date
Application number
KR1019930701370A
Other languages
English (en)
Other versions
KR960004181B1 (ko
Inventor
후미오 도다
Original Assignee
고지마 아끼로오
다이셀 가가꾸 고오교오 가부시끼가이샤
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 고지마 아끼로오, 다이셀 가가꾸 고오교오 가부시끼가이샤 filed Critical 고지마 아끼로오
Publication of KR930702263A publication Critical patent/KR930702263A/ko
Application granted granted Critical
Publication of KR960004181B1 publication Critical patent/KR960004181B1/ko

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/26—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member
    • C07D307/30—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D307/32—Oxygen atoms
    • C07D307/33—Oxygen atoms in position 2, the oxygen atom being in its keto or unsubstituted enol form
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C33/00—Unsaturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C33/28—Alcohols containing only six-membered aromatic rings as cyclic part with unsaturation outside the aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B57/00—Separation of optically-active compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B63/00—Purification; Separation; Stabilisation; Use of additives
    • C07B63/02—Purification; Separation; Stabilisation; Use of additives by treatment giving rise to a chemical modification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C33/00—Unsaturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C33/40—Halogenated unsaturated alcohols
    • C07C33/46—Halogenated unsaturated alcohols containing only six-membered aromatic rings as cyclic parts
    • C07C33/48—Halogenated unsaturated alcohols containing only six-membered aromatic rings as cyclic parts with unsaturation outside the aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C33/00—Unsaturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C33/40—Halogenated unsaturated alcohols
    • C07C33/46—Halogenated unsaturated alcohols containing only six-membered aromatic rings as cyclic parts
    • C07C33/48—Halogenated unsaturated alcohols containing only six-membered aromatic rings as cyclic parts with unsaturation outside the aromatic rings
    • C07C33/486—Polycyclic
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/587—Unsaturated compounds containing a keto groups being part of a ring
    • C07C49/613—Unsaturated compounds containing a keto groups being part of a ring polycyclic
    • C07C49/617—Unsaturated compounds containing a keto groups being part of a ring polycyclic a keto group being part of a condensed ring system
    • C07C49/643—Unsaturated compounds containing a keto groups being part of a ring polycyclic a keto group being part of a condensed ring system having three rings

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

일반식 (Ⅰ)로 표시되는 화합물 및 이 화합물로 된 분리제이다.
(식중, Ar, Ar'는 방향족기를 표시하고, 중앙의 벤젠환의 2개의 치환기의 위치관계는 오르토, 메타, 파라의 어느것이라도 좋다)
많은 종류의 화합물의 분리정제가 가능하게 되어, 의약품의 중간체등, 각종의 정제화학 분야에 유용한 화합물, 특히 광학활성체를 높은 순도로 다량으로 공급할 수 있다.

Description

신규의 화합물 및 분리제
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (12)

  1. 일반식(Ⅰ)로 표시되는 화합물.
  3. (식중, Ar, Ar'는 방향족기를 표시하고, 중앙의 벤젠환의 2개의 치환기의 위치관계는 오르토, 메타, 파라의 어느것이라도 좋다)
  4. 제1항에 있어서, Ar과 Ar'가 동일한 기인 화합물.
  5. 제1항에 있어서, Ar과 Ar'가 다른 기인 화합물.
  6. 제3항에 있어서, 광학활성체인 화합물.
  7. 제1항에 있어서, Ar가 페닐기, Ar'가 o-클로로페닐기인 화합물.
  8. 제1항에 기재된 화합물로 이루어진 분리제.
  9. 제1항에 있어서, 기재된 화합물(호스트화합물)과 다른 화합물(게스트화합물)이 클라드레트 화합물을 형성하는 것을 이용하여, 그 게스트화합물을 혼합물중에서 분리하거나, 또는 그 게스트화합물에 의하여 오염되어 있는 제3의 물질을 정제하는 것을 특징으로 하는 분리, 정제방법.
  10. 제4항에 기재된 화합물 (호스트화합물)이 게스트화합물의 광학 이성체 혼합물로 부터 한쪽의 광학이성체만을 선택적으로 함유한 클라드레트화합물을 형성하는 것을 이용하여, 그 게스트화합물의 광학이성체를 분리 하는 것을 특징으로 하는 분리방법.
  11. 제4항에 기재된 화합물을 화학적 또는 물리적 방법에 의하여 고정상으로 결합하고, 그 다음에 코로마토그래피를 행하는 것을 특징으로 하는 광학이성체 혼합물로부터 한쪽의 광학이성체를 분리하는 방법.
  12. ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019930701370A 1991-09-09 1992-08-27 신규의 화합물 및 분리제 KR960004181B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP03227991A JP3128281B2 (ja) 1991-09-09 1991-09-09 新規な化合物及び分離剤
JP91-227991 1991-09-09
PCT/JP1992/001083 WO1993005004A1 (en) 1991-09-09 1992-08-27 Novel compound and separating agent

Publications (2)

Publication Number Publication Date
KR930702263A true KR930702263A (ko) 1993-09-08
KR960004181B1 KR960004181B1 (ko) 1996-03-27

Family

ID=16869461

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019930701370A KR960004181B1 (ko) 1991-09-09 1992-08-27 신규의 화합물 및 분리제

Country Status (6)

Country Link
US (2) US5334776A (ko)
EP (1) EP0565727B1 (ko)
JP (1) JP3128281B2 (ko)
KR (1) KR960004181B1 (ko)
DE (1) DE69219582T2 (ko)
WO (1) WO1993005004A1 (ko)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6706839B1 (en) 1999-02-10 2004-03-16 University Of Pittsburgh Chemical partitioning agents and methods of using same
US6224140B1 (en) * 1999-10-05 2001-05-01 Kbs Industries Ltd. Tonneau cover
JP4311415B2 (ja) 2006-06-26 2009-08-12 株式会社日立製作所 冷却装置，冷却装置を用いたガスタービンシステム，冷却機構を用いたヒートポンプシステム，冷却方法，冷却装置の運転方法
JP5821661B2 (ja) * 2012-01-26 2015-11-24 デクセリアルズ株式会社 新規なビス又はトリス（３−ヒドロキシ−３，３−ジフェニル−１−プロピニル）アリール化合物類、光情報記録材料及び光情報記録媒体
JP6313596B2 (ja) * 2013-12-29 2018-04-18 株式会社綜合プラスチック 組立式ブロック構造に用いられるロック解除具
WO2017151601A1 (en) 2016-03-01 2017-09-08 Dirtt Environmental Solutions, Inc. Millwork leveler

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4089908A (en) * 1974-06-17 1978-05-16 Sandoz, Inc. Substituted methanols
US4223172A (en) * 1978-12-07 1980-09-16 Gulf Research & Development Company Process for the preparation of bromoarylacetylene and aryldiacetylene precursors
JPS58150526A (ja) * 1982-03-04 1983-09-07 Ube Ind Ltd 光学活性プロパルギルアルコ−ル類およびその製法
EP0178331A4 (en) * 1984-03-26 1987-01-20 Kyowa Hakko Kogyo Kk ALKYNOL COMPOUNDS AND ALCOHOL SEPARATING AGENTS.
JPH0615511B2 (ja) * 1986-06-03 1994-03-02 宇部興産株式会社 光学活性なプロピオン酸アミドの製造方法
US4918190A (en) * 1986-08-06 1990-04-17 Ube Industries, Ltd. Crystalline complex compounds of propargyl alcohols and tertiary diamines, and process of separation and purification of propargyl alcohols using the same

Also Published As

Publication number Publication date
WO1993005004A1 (en) 1993-03-18
KR960004181B1 (ko) 1996-03-27
US5334776A (en) 1994-08-02
JP3128281B2 (ja) 2001-01-29
EP0565727A4 (en) 1993-11-24
EP0565727A1 (en) 1993-10-20
DE69219582D1 (de) 1997-06-12
EP0565727B1 (en) 1997-05-07
US5395985A (en) 1995-03-07
DE69219582T2 (de) 1997-09-11
JPH0565238A (ja) 1993-03-19

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