KR930021591A - 1,1-디클로로-1-플루오로에탄의 정제방법 - Google Patents
1,1-디클로로-1-플루오로에탄의 정제방법 Download PDFInfo
- Publication number
- KR930021591A KR930021591A KR1019930006006A KR930006006A KR930021591A KR 930021591 A KR930021591 A KR 930021591A KR 1019930006006 A KR1019930006006 A KR 1019930006006A KR 930006006 A KR930006006 A KR 930006006A KR 930021591 A KR930021591 A KR 930021591A
- Authority
- KR
- South Korea
- Prior art keywords
- chlorine
- process according
- treatment
- dichloro
- fluoroethane
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
- C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
- C07C17/395—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to a chemical modification of at least one compound
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C19/00—Acyclic saturated compounds containing halogen atoms
- C07C19/08—Acyclic saturated compounds containing halogen atoms containing fluorine
- C07C19/10—Acyclic saturated compounds containing halogen atoms containing fluorine and chlorine
- C07C19/12—Acyclic saturated compounds containing halogen atoms containing fluorine and chlorine having two carbon atoms
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/06—Reactor-distillation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
초기 1, 1-디클로로-1-플루오로에탄을 유기 유리기 개시체의 존재하에 염소로 처리한 다음 증류하여서 하는 정제방법.
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (10)
- 초기 1, 1-디클로로-1-플루오로에탄을 염소로 처리한 다음 증류하여서 하는 정제방법에 있어서, 염소로의 처리를 유기 유리기 개시체의 존재하에서 행함을 특징으로 하는 정제방법.
- 제1항에 있어서, 유기 개시체를 과산화물 또는 디아조 화합물에서 선택함을 특징으로 하는 정제방법.
- 제2항에 있어서, 유기 개시체를 과산화 화합물에서 선택함을 특징으로 하는 정제방법.
- 제3항에 있어서, 과산화 화합물을 디아실 과산화묽돐 퍼옥시디카보네이트에서 선택함을 특징으로 하는 정제방법.
- 제4항에 있어서, 과산화 화합물을 디라우로일 과산화물, 디벤조일 과산화물과 디세틸 퍼옥시카보네이트에서 선택함을 특징으로 하는 정제방법.
- 전술한 항중 어느 한항에 있어서, 유기 개시체를 염소와의 처리온도에서 약 1시간의 반감기를 나타내는 화합물에서 선택함을 특징으로 하는 정제방법.
- 전술한 항중 어느한 항에 있어서, 염소로의 처리를초기 1, 1-디클로로-1-플루오로에탄의 중량에 대하여 약 10중량ppm 이상의 유기 개시체의 존재하에 행함을 특징으로 하는 정제방법.
- 전술한 항중 어느 한 항에 있어서, 초기 1,1-디클로로―1―플루오로에 탄에서 불포화 불순물의 몰당 약15몰을 초과하지 않고 3몰 이상의 비율로 염소를 사용항을 특징으로 하는 정제방법.
- 전술한 항중 어느 한 항에 있어서, 염소외의 처리를 약40-150℃의 온도에서 행함을 특징으로 하는 정제방법.
- 전술한 항중 어느 한 항에 있어서, 염소와의 처리기간이 약 60분임을 특징으로 하는 정제방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
BE09200357 | 1992-04-17 | ||
BE9200357A BE1005731A3 (fr) | 1992-04-17 | 1992-04-17 | Procede pour l'epuration de 1,1-dichloro-1-fluoroethane. |
BE9200357 | 1992-04-17 |
Publications (2)
Publication Number | Publication Date |
---|---|
KR930021591A true KR930021591A (ko) | 1993-11-22 |
KR100281363B1 KR100281363B1 (ko) | 2001-02-01 |
Family
ID=3886230
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019930006006A KR100281363B1 (ko) | 1992-04-17 | 1993-04-10 | 1,1-디클로로-1-플루오로에탄의 정제방법 |
Country Status (12)
Country | Link |
---|---|
US (1) | US5318673A (ko) |
EP (1) | EP0566190B1 (ko) |
JP (1) | JP3372287B2 (ko) |
KR (1) | KR100281363B1 (ko) |
AT (1) | ATE142188T1 (ko) |
AU (1) | AU663767B2 (ko) |
BE (1) | BE1005731A3 (ko) |
CA (1) | CA2094201A1 (ko) |
DE (1) | DE69304387T2 (ko) |
DK (1) | DK0566190T3 (ko) |
ES (1) | ES2093912T3 (ko) |
TW (1) | TW279156B (ko) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2009013198A1 (en) * | 2007-07-20 | 2009-01-29 | Solvay Fluor Gmbh | Process for obtaining a purified hydrofluoroalkane |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB1401541A (en) * | 1972-03-02 | 1975-07-16 | Ici Ltd | Purification of halothane |
JPH0613578B2 (ja) * | 1988-11-08 | 1994-02-23 | 工業技術院長 | 親水性−疎水性熱可逆型高分子化合物及びその製造方法 |
US4948479A (en) * | 1989-06-07 | 1990-08-14 | Atochem North America, Inc. | Removal of unsaturated carbon compounds from 1,1-dichloro-1-fluoroethane |
FR2651775B1 (fr) * | 1989-09-12 | 1993-02-19 | Atochem | Purification du dichloro-1,1 fluoro-1 ethane. |
JPH04264039A (ja) * | 1991-02-20 | 1992-09-18 | Central Glass Co Ltd | 1,1−ジクロロ−1−フルオロエタン中の1,1−ジクロロエチレンの除去方法 |
-
1992
- 1992-04-17 BE BE9200357A patent/BE1005731A3/fr not_active IP Right Cessation
-
1993
- 1993-03-30 AU AU35553/93A patent/AU663767B2/en not_active Ceased
- 1993-03-31 TW TW082102381A patent/TW279156B/zh active
- 1993-04-06 EP EP93201013A patent/EP0566190B1/fr not_active Expired - Lifetime
- 1993-04-06 AT AT93201013T patent/ATE142188T1/de not_active IP Right Cessation
- 1993-04-06 ES ES93201013T patent/ES2093912T3/es not_active Expired - Fee Related
- 1993-04-06 DE DE69304387T patent/DE69304387T2/de not_active Expired - Fee Related
- 1993-04-06 US US08/043,310 patent/US5318673A/en not_active Expired - Fee Related
- 1993-04-06 DK DK93201013.5T patent/DK0566190T3/da active
- 1993-04-10 KR KR1019930006006A patent/KR100281363B1/ko not_active IP Right Cessation
- 1993-04-16 CA CA002094201A patent/CA2094201A1/fr not_active Abandoned
- 1993-04-19 JP JP09109393A patent/JP3372287B2/ja not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
JP3372287B2 (ja) | 2003-01-27 |
TW279156B (ko) | 1996-06-21 |
EP0566190B1 (fr) | 1996-09-04 |
DE69304387T2 (de) | 1997-03-27 |
AU663767B2 (en) | 1995-10-19 |
JPH069450A (ja) | 1994-01-18 |
ES2093912T3 (es) | 1997-01-01 |
CA2094201A1 (fr) | 1993-10-18 |
KR100281363B1 (ko) | 2001-02-01 |
ATE142188T1 (de) | 1996-09-15 |
BE1005731A3 (fr) | 1994-01-11 |
AU3555393A (en) | 1993-10-21 |
DK0566190T3 (ko) | 1997-02-24 |
DE69304387D1 (de) | 1996-10-10 |
EP0566190A1 (fr) | 1993-10-20 |
US5318673A (en) | 1994-06-07 |
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