KR920012171A - 고형물 함량이 높은 습윤지력 증강용 수지의 합성 방법 - Google Patents

고형물 함량이 높은 습윤지력 증강용 수지의 합성 방법 Download PDF

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Publication number
KR920012171A
KR920012171A KR1019910025509A KR910025509A KR920012171A KR 920012171 A KR920012171 A KR 920012171A KR 1019910025509 A KR1019910025509 A KR 1019910025509A KR 910025509 A KR910025509 A KR 910025509A KR 920012171 A KR920012171 A KR 920012171A
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KR
South Korea
Prior art keywords
composition
acid
polyaminoamide
epichlorohydrin
resin
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Application number
KR1019910025509A
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English (en)
Inventor
더블유. 마스랑카 윌리암
Original Assignee
스티븐 에이취. 마르코위츠
헤르큘레스 인코포레이티드
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Application filed by 스티븐 에이취. 마르코위츠, 헤르큘레스 인코포레이티드 filed Critical 스티븐 에이취. 마르코위츠
Publication of KR920012171A publication Critical patent/KR920012171A/ko

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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C08G69/48—Polymers modified by chemical after-treatment
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
    • C08G73/02—Polyamines
    • C08G73/028—Polyamidoamines
    • C08G73/0286—Preparatory process from polyamidoamines and epihalohydrins
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/20—Macromolecular organic compounds
    • D21H17/33—Synthetic macromolecular compounds
    • D21H17/46—Synthetic macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D21H17/54—Synthetic macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds obtained by reactions forming in the main chain of the macromolecule a linkage containing nitrogen
    • D21H17/55—Polyamides; Polyaminoamides; Polyester-amides
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
    • D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
    • D21H21/18—Reinforcing agents
    • D21H21/20—Wet strength agents

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Paper (AREA)
  • Polyamides (AREA)
  • Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)

Abstract

내용 없음

Description

고형물 함량이 높은 습윤지역 증강용 수지의 합성 방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (15)

  1. 이염기성 카복실산과 폴리알킬렌폴리아민을 반응시킴을 포함하는 폴리아미노아미드의 제조방법에 있어서, 상기 이염기성 카복실산과 상기 폴리알킬렌폴리아민을 산 촉매의 존재하에서 반응시킴을 포함하는, 개선된 폴리아미노아미드의 제조방법.
  2. 제1항에 있어서, 상기 산 촉매가 무기산인 방법.
  3. 제1항에 있어서, 상기 산 촉매가 염산, 황산, 인산, 포름산, 아세트산, 벤젠설폰사 또는 p-톨루엔설폰산인 방법.
  4. 제1항에 있어서, 상기 폴리아미노아미드를 에피클로로히드린과 반응시켜 수-용성 양이온계 폴리아미노-에피클로로히드린 수지를 제조함을 또한 포함하는 방법.
  5. 제4항에 있어서, 상기 에피클로로히드린을 30 내지 50℃의 온도에서 상기 폴리아미노아미드와 반응시키고 이어서 55 내지 75℃의 온도로 가열하는 방법.
  6. 제4항에 있어서, 에피클로로히드린 대 폴리아민의 몰 비율이 1.7/1 내지 1.9/1인 방법.
  7. 제4항에 있어서, 상기 에피클로로히드린을 43내지 48중량%의 전체 고형물 함량을 갖는 수용액중의 상기 폴리아미노아미드와 반응시키는 방법.
  8. 제1항의 방법에 따라 제조된 생성물.
  9. 제2항의 방법에 따라 제조된 생성물.
  10. 적어도 15중량%의 전체 고형물 함량을 갖는 양이온계 수용성 폴리아미노아미드-에피클로로히드린 수지의 용액을 포함하는 수성 조성물.
  11. 제10항에 있어서, 적어도 25중량%의 전체 고형물 함량을 갖는 조성물.
  12. 제10항에 있어서, 2.5 내지 4.5의 PH로 유지되는 조성물.
  13. 제10항에 있어서, 3.0 내지 4.0의 pH로 유지되는 조성물.
  14. 제10항의 조성물로 처리된 시이트형 셀룰로즈 섬유를 포함하는 개선된 습윤강도를 갖는 종이 제품.
  15. 제10항의 조성물을 종이 제품에 혼입시킴을 포함하는, 상기 조성물의 사용방법.
    ※ 참고사항: 최초출원 내용에 의하여 공개하는 것임.
KR1019910025509A 1990-12-31 1991-12-30 고형물 함량이 높은 습윤지력 증강용 수지의 합성 방법 KR920012171A (ko)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US63435590A 1990-12-31 1990-12-31
US634,355 1990-12-31
US65955291A 1991-02-22 1991-02-22
US659552 1991-02-22

Publications (1)

Publication Number Publication Date
KR920012171A true KR920012171A (ko) 1992-07-25

Family

ID=27092135

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019910025509A KR920012171A (ko) 1990-12-31 1991-12-30 고형물 함량이 높은 습윤지력 증강용 수지의 합성 방법

Country Status (10)

Country Link
US (2) US5644021A (ko)
EP (1) EP0493757A3 (ko)
JP (1) JPH05239206A (ko)
KR (1) KR920012171A (ko)
AU (1) AU654516B2 (ko)
BR (1) BR9105618A (ko)
CA (1) CA2058009C (ko)
FI (1) FI916063A (ko)
MX (1) MX9102798A (ko)
NO (1) NO915064L (ko)

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US5318669A (en) * 1991-12-23 1994-06-07 Hercules Incorporated Enhancement of paper dry strength by anionic and cationic polymer combination
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US5614597A (en) * 1994-12-14 1997-03-25 Hercules Incorporated Wet strength resins having reduced levels of organic halogen by-products
US5856427A (en) * 1996-01-16 1999-01-05 Solutia Inc. Process for the production of polysuccinimide
US6222006B1 (en) * 1997-08-13 2001-04-24 Fort James Corporation Wet strength thermosetting resin formulations and polyaminamide polymers suitable for use in the manufacture of paper products
US7344607B2 (en) * 1999-07-08 2008-03-18 Ge Betz, Inc. Non-chromate conversion coating treatment for metals
ES2251384T3 (es) 1999-07-08 2006-05-01 Hercules Incorporated Composiciones para impartir propiedades deseadas a materiales.
US6352613B1 (en) * 2000-03-14 2002-03-05 Hercules Incorporated Resin compositions having high solids contents
US7317053B1 (en) 2000-07-10 2008-01-08 Hercules Incorporated Compositions for imparting desired properties to materials
US20040118540A1 (en) * 2002-12-20 2004-06-24 Kimberly-Clark Worlwide, Inc. Bicomponent strengtheninig system for paper
US6908983B2 (en) * 2003-04-01 2005-06-21 Hercules Corporation Synthesis of high solids resins from amine terminated polyamides
US20060042726A1 (en) * 2004-09-02 2006-03-02 General Electric Company Non-chrome passivation of steel
US7491274B2 (en) * 2004-10-29 2009-02-17 Chemetall Corp. Non-chrome metal treatment composition
UA79720C2 (en) * 2006-09-29 2007-07-10 Ukrvodbezpeka Scient And Techn A method for obtaining polyguanidines
US7868071B2 (en) * 2007-07-30 2011-01-11 Georgia-Pacific Chemicals Llc Method of stabilizing aqueous cationic polymers
US8758567B2 (en) * 2009-06-03 2014-06-24 Hercules Incorporated Cationic wet strength resin modified pigments in barrier coating applications
US9580866B2 (en) 2009-06-03 2017-02-28 Solenis Technologies, L.P. Cationic wet strength resin modified pigments in water-based latex coating applications
MX354457B (es) 2011-04-21 2018-03-06 Ecolab Usa Inc Resinas de poliamidoamina-epihalohidrina, método de fabricación y usos de las mismas.
CN103866636B (zh) * 2014-02-28 2016-01-13 南通玖伍捌科技企业孵化器有限公司 一种脲醛树脂湿强剂及其制备方法

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US3086961A (en) * 1959-12-07 1963-04-23 American Cyanamid Co Water-soluble dibasic acid-polyalkylenepolyamine-alkylene glycol crosslinked polymer
US3352833A (en) * 1963-12-31 1967-11-14 Hercules Inc Acid stabilization and base reactivation of water-soluble wet-strength resins
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Also Published As

Publication number Publication date
CA2058009C (en) 1998-08-18
EP0493757A2 (en) 1992-07-08
AU654516B2 (en) 1994-11-10
BR9105618A (pt) 1992-09-01
FI916063A (fi) 1992-07-01
AU9010391A (en) 1992-07-02
CA2058009A1 (en) 1992-07-01
EP0493757A3 (en) 1993-07-07
NO915064D0 (no) 1991-12-20
US5644021A (en) 1997-07-01
NO915064L (no) 1992-07-01
US5668246A (en) 1997-09-16
JPH05239206A (ja) 1993-09-17
MX9102798A (es) 1992-06-01
FI916063A0 (fi) 1991-12-20

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