KR920004275A - 황산 암모늄 결정의 크기를 증가시키는 방법 및 장치 - Google Patents

황산 암모늄 결정의 크기를 증가시키는 방법 및 장치 Download PDF

Info

Publication number
KR920004275A
KR920004275A KR1019910014838A KR910014838A KR920004275A KR 920004275 A KR920004275 A KR 920004275A KR 1019910014838 A KR1019910014838 A KR 1019910014838A KR 910014838 A KR910014838 A KR 910014838A KR 920004275 A KR920004275 A KR 920004275A
Authority
KR
South Korea
Prior art keywords
ammonium sulfate
chamber
crystal
crystals
flow
Prior art date
Application number
KR1019910014838A
Other languages
English (en)
Other versions
KR0166374B1 (ko
Inventor
월터지.톰슨
케이.크라머 조나단
Original Assignee
윌리암 엠. 케비스톤
바스프 코포레이션
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 윌리암 엠. 케비스톤, 바스프 코포레이션 filed Critical 윌리암 엠. 케비스톤
Publication of KR920004275A publication Critical patent/KR920004275A/ko
Application granted granted Critical
Publication of KR0166374B1 publication Critical patent/KR0166374B1/ko

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C01B17/96—Methods for the preparation of sulfates in general
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00—Ammonia; Compounds thereof
    • C01C1/24—Sulfates of ammonium
    • C01C1/248—Preventing coalescing or controlling form or size of the crystals
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S423/00—Chemistry of inorganic compounds
    • Y10S423/09—Reaction techniques
    • Y10S423/16—Fluidization
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T117/00—Single-crystal, oriented-crystal, and epitaxy growth processes; non-coating apparatus therefor
    • Y10T117/10—Apparatus
    • Y10T117/1024—Apparatus for crystallization from liquid or supercritical state

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Fertilizers (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)

Abstract

내용 없음

Description

황산 암모늄 결정의 크기를 증가시키는 방법 및 장치
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
제 1 도는 본 발명에 따른 황산 암모늄 결정의 확대장치의 개략적인 정면도이다.

Claims (2)

  1. 다음의 a), b)로 이루어진 a)공급물 결정의 하강 비율을 지체시키는 가스의 향류흐름에 대해 결정의 접촉기간이 하강되면서, 95내지 110℃에서 약 0.15내지 약 0.45㎜의 평균 크기를 갖는 황산 암모늄 결정의 공급물에 농축된 황산 암모늄 수용액을 분무하는 단계(이때 농축된 황산 암모늄 수용액은 적어도 1.0㎜의 평균 크기를 갖는 확대된 황산 암모늄 결정이 얻어지도록 충분해야 한다), b)이들의 물 함량이 약 1중량% 이하로 감소되도록 가스의 농축된 흐름에 대해 하강하면서 110 내지 125℃온도에서 확대된 황산 암모늄 결정을 가열하는 단계로 이루어진 황산 암모늄 결정의 평균 크기를 증가시키는 방법
  2. a)한 단부에서 황산 암모늄 결정의 공급물을 수용하고 및 다른 단부에서 비교적 높은 물 함량을 확대된 황산 암모늄 결정을 배출하기 위한 제1챔버(chamber), b)제1챔버안으로 황산 암모늄 수용액을 분무하여 실제적으로 개개의 황산 암모늄 공급물 결정이 황산 암모늄 용액에 의해 접촉되도록 수단 c)제1챔버에서 그것을 통해 황산 암모늄 결정의 흐름에 반하여 흐르는 가스의 흐름을 제공하는 수단, d)적어도 그러한 결정이 황산 암모늄 용액과 접촉하여 이 용액이 비교적 높은 물 함량을 갖는 확대된 황산 암모늄 결정으로 얻어진 공급물 결정상에서 적어도 부분적으로 건조가 수행되도록 제1챔버에서 황산 암모늄 공급물 결정을 가열하는 수단, e)한 단부에서 제1챔버로 부터 배출된 비교적 높은 물 함량을 갖는 확대된 황산 암모늄 결정을 수용하고 및 다른 단부에서 확대되고, 건조된 황산 암모늄 결정을 배출하기 위한 제2챔버, f)제2챔버에서 그것을 통새 확대된 황산 암모늄 결정의 흐름에 반하여 흐르는 가스 흐름을 제공하는 수단, g)제2챔버에서 확대된 황산 암모늄 결정을 가열하여 결정의 물 함량을 감소시키는 수단, h)장치로부터 가스의 상한 누출을 막기에 충분한 것으로, 제2챔버의 한 단부로부터 배출된 감소된 물 함량을 갖는 확대된 황산 암모늄 결정을 수용하는 제3챔버, i)제3챔버로 부터의 감소된 물 함량을 갖는 확장된 황산 암모늄 결정을 운반하기 위한 이송수단로 이루어진 황산 암모늄 결정의 확대장치.
    ※ 참고사항 : 최초출원 내용에 의하여 공개되는 것임.
KR1019910014838A 1990-08-28 1991-08-27 황산 암모늄 결정의 크기를 증가시키는 방법 및 장치 KR0166374B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US57420590A 1990-08-28 1990-08-28
US574,205 1990-08-28

Publications (2)

Publication Number Publication Date
KR920004275A true KR920004275A (ko) 1992-03-27
KR0166374B1 KR0166374B1 (ko) 1999-01-15

Family

ID=24295123

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019910014838A KR0166374B1 (ko) 1990-08-28 1991-08-27 황산 암모늄 결정의 크기를 증가시키는 방법 및 장치

Country Status (6)

Country Link
US (2) US5330544A (ko)
EP (1) EP0475131B1 (ko)
JP (1) JPH04231322A (ko)
KR (1) KR0166374B1 (ko)
DE (1) DE69119516T2 (ko)
ES (1) ES2086446T3 (ko)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5618658A (en) * 1995-02-22 1997-04-08 Fuji Hunt Photographic Chemicals, Inc. Process for producing an ammonium thiosulfate product
DE19514187C1 (de) * 1995-04-21 1996-05-15 Degussa Verfahren und Vorrichtung zur Herstellung von Granulaten durch Wirbelschicht-Sprühgranulation
US5820787A (en) * 1997-04-14 1998-10-13 Basf Corporation Process for dust suppression in solids
US6015445A (en) * 1997-04-14 2000-01-18 Basf Corporation Anti-caking solids
US5980601A (en) * 1997-04-14 1999-11-09 Basf Corporation Anti-caking solids
US5885320A (en) * 1997-04-14 1999-03-23 Basf Corporation Anti-caking process
US5855816A (en) * 1997-04-14 1999-01-05 Basf Corporation Dust suppression in solids
US6361720B1 (en) 1999-02-12 2002-03-26 Honeywell International Inc. Process for granule production
DE60122336D1 (de) * 2000-03-08 2006-09-28 Isg Resources Inc Kontrolle der ammoniakemissionen von mit ammoniak beladener flugasche in beton
WO2010012635A1 (en) * 2008-07-31 2010-02-04 Dsm Ip Assets B.V. Pelletized ammonium sulfate particles
CN102390844B (zh) * 2011-08-08 2013-05-29 河北科技大学 一种大颗粒硫酸铵结晶制备工艺
ES2674950T3 (es) * 2012-09-11 2018-07-05 Cap Iii B.V. Proceso y aparato para iniciar un proceso de cristalización de sulfato de amonio
US8974763B1 (en) * 2013-12-18 2015-03-10 Rentech, Inc. System and method for production of granular ammonium sulfate
DE102015108344A1 (de) * 2015-05-27 2016-12-01 Thyssenkrupp Ag Granulation von Ammoniumsulfat

Family Cites Families (41)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1266212A (en) * 1917-09-17 1918-05-14 Felix Capron Production of neutral ammonium sulfate.
US1919707A (en) * 1929-03-20 1933-07-25 Gas Light & Coke Co Production of sulphate of ammonia
US2102107A (en) * 1933-10-16 1937-12-14 Directie Staatsmijnen Nl Production of ammonium sulphate
US2099079A (en) * 1934-01-19 1937-11-16 Ig Farbenindustrie Ag Production of coarsely crystalline ammonium sulphate
US2092073A (en) * 1934-06-09 1937-09-07 Ig Farbenindustrie Ag Production of ammonium sulphate in the form of scales
US2043067A (en) * 1935-01-10 1936-06-02 Ig Farbenindustrie Ag Production of coarsely crystalline ammonium sulphate
US2228742A (en) * 1936-11-11 1941-01-14 Ici Ltd Manufacture of ammonium sulphate
GB484921A (en) * 1936-11-11 1938-05-11 John Wilfred Richard Rayner Improvements in or relating to the manufacture of ammonium sulphate
US2226101A (en) * 1938-05-30 1940-12-24 Ici Ltd Manufacture of ammonium sulphate
US2368901A (en) * 1940-09-25 1945-02-06 Semet Solvay Eng Corp Ammonium sulphate production
US2423794A (en) * 1943-08-25 1947-07-08 Fuel Refining Corp Production of ammonium sulphate
US2424207A (en) * 1944-05-30 1947-07-15 Otto Carl Production of ammonium sulphate
US2599067A (en) * 1947-12-17 1952-06-03 Otto Carl Production of ammonium sulfate
US2631843A (en) * 1948-10-28 1953-03-17 Chrysler Corp Spring cover
US2631084A (en) * 1948-12-29 1953-03-10 Phillips Petroleum Co Ammonium sulfate production
US2659659A (en) * 1950-12-07 1953-11-17 Standard Oil Dev Co Ammonium sulfate production
US2805125A (en) * 1952-12-02 1957-09-03 Koppers Co Inc Methods and apparatus for the manufacture of ammonium sulfate
US2782097A (en) * 1953-06-25 1957-02-19 Phillips Petroleum Co Ammonium sulfate production
US2795487A (en) * 1954-02-02 1957-06-11 Otto Carl Apparatus for producing ammonium sulfate crystals
US2895800A (en) * 1954-08-27 1959-07-21 Otto Carl Method of and apparatus for producing ammonium sulphate crystals
US2874028A (en) * 1956-04-25 1959-02-17 United States Steel Corp Method of producing natural rhombic shaped ammonium sulphate crystals
US3159456A (en) * 1959-05-06 1964-12-01 Hertha M Schulze Apparatus for producing ammonium salt crystals
US3600818A (en) * 1969-04-17 1971-08-24 Grun Kg Maschinenfabrik Geb Method of and apparatus for treating powdery or granular materials with gaseous, liquid or solid agents or stabilizers
US3632257A (en) * 1969-09-04 1972-01-04 Naoyoshi Ashizawa Apparatus for making granules
US3794099A (en) * 1970-06-13 1974-02-26 N Ganiaris Fluidized bed process for drying ammonium sulphate
GB1381480A (en) * 1971-06-18 1975-01-22 Struthers Scient International Fluidized bed process and apparatus
US3933434A (en) * 1972-07-13 1976-01-20 Edwin Matovich High temperature chemical reactor
DE2602454C3 (de) * 1976-01-23 1988-09-29 Luco-Sprühmisch-Technic GmbH, 6474 Ortenberg Vorrichtung zur Durchführung des Verfahrens nach Patent 26 60 533
FR2430917A1 (fr) * 1978-07-11 1980-02-08 Comp Generale Electricite Procede et dispositif d'elaboration de silicium polycristallin
EP0013108B1 (en) * 1978-12-22 1983-11-23 Adelaide & Wallaroo Fertilizers Ltd. Improvements in and relating to granulation
IT1121993B (it) * 1979-07-02 1986-04-23 Montedison Spa Procedimento migliorato per l'essiccamento di materiali incoerenti
DE3108986A1 (de) * 1981-03-10 1982-05-13 Buckau-Walther AG, 4048 Grevenbroich "verfahren zum herstellen von ammoniumsulfatgranulaten"
DE3565475D1 (en) * 1984-04-07 1988-11-17 Bayer Ag Process and apparatus for the production of granules
DE3435862A1 (de) * 1984-09-29 1986-04-10 Degussa Ag, 6000 Frankfurt Kontinuierliches verfahren zur mehrstufigen behandlung feinteiliger feststoffe mit gasen
JPS61256917A (ja) * 1985-05-09 1986-11-14 Nippon Kokan Kk <Nkk> 粉粒体硫安の製造方法
JPS6246920A (ja) * 1985-08-23 1987-02-28 Kawasaki Steel Corp 硫安の製造方法
DE3532957A1 (de) * 1985-09-14 1987-03-19 Metallgesellschaft Ag Verfahren und vorrichtung zum extrahieren von wertstoffen aus koernigem einsatzgut
NL8700913A (nl) * 1987-04-16 1988-11-16 Nl Stikstof Werkwijze voor het vervaardigen van kunstmestgranules.
FI82612C (fi) * 1987-05-08 1991-04-10 Ahlstroem Oy Foerfarande och anordning foer behandling av processgaser.
US4859315A (en) * 1987-11-05 1989-08-22 Bartholic David B Liquid-solid separation process and apparatus
JP2763806B2 (ja) * 1989-10-20 1998-06-11 フロイント産業株式会社 造粒コーティング方法および装置

Also Published As

Publication number Publication date
US5408953A (en) 1995-04-25
EP0475131B1 (en) 1996-05-15
ES2086446T3 (es) 1996-07-01
JPH04231322A (ja) 1992-08-20
DE69119516D1 (de) 1996-06-20
US5330544A (en) 1994-07-19
DE69119516T2 (de) 1996-10-02
EP0475131A1 (en) 1992-03-18
KR0166374B1 (ko) 1999-01-15

Similar Documents

Publication Publication Date Title
KR920004275A (ko) 황산 암모늄 결정의 크기를 증가시키는 방법 및 장치
JPS52104097A (en) Field effect liquid crystal display
JPS5278800A (en) Drying of ammonia gas flow
JPS5343277A (en) Liquid tank
JPS52107787A (en) Pressure converter
JPS5428255A (en) Hastelloy-clad steellplate with superior dendability and its manufacture
JPS5223514A (en) Treatment method for metal melt
JPS52137223A (en) Address expansion system of channel
JPS52119411A (en) High carbon chromium-nickel steel
JPS53142593A (en) Stabilization of urokinase by heating
JPS52124463A (en) Coagulation treatment of suspension
JPS5383163A (en) Dehydrator
Kubomura Appearences of Landside at the 7 th Shiboro Kabetsu River Bridge near Shimizuzawa along Yubari line, JNR
JPS5269533A (en) Double keying prevention circuit
JPS5426629A (en) Microcomputer unit
JPS548571A (en) Pressure measuring device
JPS52111473A (en) Ribbon crystal growth method
JPS51143587A (en) Ozonizer
JPS53137422A (en) Chain gutter
JPS5376724A (en) Information process system
JPS51139581A (en) Liquid crystal compounds and liquid crystal mixtures
JPS51120743A (en) Electrical-optical cell
JPS5393404A (en) Constant flow cnstant pressure pump
JPS5328008A (en) Cutting-out apparatus for shaft furnace
JPS5360762A (en) Cold air stagnation preventive device

Legal Events

Date Code Title Description
A201 Request for examination
E701 Decision to grant or registration of patent right
GRNT Written decision to grant
FPAY Annual fee payment

Payment date: 20020823

Year of fee payment: 5

LAPS Lapse due to unpaid annual fee