KR920002632B1 - Preparation method of decorative glass plate - Google Patents

Preparation method of decorative glass plate Download PDF

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KR920002632B1
KR920002632B1 KR1019900004062A KR900004062A KR920002632B1 KR 920002632 B1 KR920002632 B1 KR 920002632B1 KR 1019900004062 A KR1019900004062 A KR 1019900004062A KR 900004062 A KR900004062 A KR 900004062A KR 920002632 B1 KR920002632 B1 KR 920002632B1
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layer
color
mirror
glass plate
screen printing
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KR1019900004062A
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Korean (ko)
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KR910016638A (en
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김중형
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김중형
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    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/28—Surface treatment of glass, not in the form of fibres or filaments, by coating with organic material
    • C03C17/32—Surface treatment of glass, not in the form of fibres or filaments, by coating with organic material with synthetic or natural resins

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Surface Treatment Of Glass (AREA)
  • Joining Of Glass To Other Materials (AREA)
  • Mirrors, Picture Frames, Photograph Stands, And Related Fastening Devices (AREA)

Abstract

A making process for ornamental glass plate with sectioned multi color mirror is characterized by following processes; (1) spreading a mixture of 100 g PVA (polyvinyl alcohol), 1000 cc methanol, 400 acetone and 10-15 g dye on the surface of glass plate by brushing and forming color layer (2); (2) forming mirror layer on the surface color layer by deposition of aluminum; (3) establishing printed layer (4) by screen printing of epoxy ink; (4) removing mirror layer (3) and color layer (2) away from none screen printed layer (5) by a solution of 1 part of FeCl3 and 3 parts of methanol. The color and mirror layer make it possible to remove non printed layer thoroughly away from glass plate. It has advantages of promoting reflectance and defintion of mirror and is suitable to ornamental glass plate for building, watch glass, photo frame and furniture, etc.

Description

다색도 부분 칼라경을 갖는 장식용 유리판의 가공방법Processing method of decorative glass plate with multicolor partial color diameter

제1도는 본 발명이 실시된 상태의 유리판사시도.1 is a glass judge perspective view of the embodiment of the present invention.

제2a,b,c도 본 발명의 공정상태는 나타낸 단면도.2a, b, c are sectional views showing the process state of the present invention.

제2a도는 칼라층 형성과정의 단면도.Figure 2a is a cross-sectional view of the color layer forming process.

제2b도는 알루미늄 진공증착층을 형성시킨 상태의 단면도.2b is a cross-sectional view of the aluminum vacuum deposition layer formed.

제2c도는 스크린 인쇄층을 형성시킨 단면도.2C is a cross-sectional view of the screen printing layer formed.

제2d도는 본 발명의 최종 완성상태의 단면도.Figure 2d is a cross-sectional view of the final completion state of the present invention.

* 도면의 주요부분에 대한 부호의 설명* Explanation of symbols for main parts of the drawings

1 : 판유리 2 : 칼라층1: plate glass 2: color layer

3 : 거울층 4 : 스크린 인쇄층3: mirror layer 4: screen printing layer

5 : 비 스크린 인쇄층 6 : 장식용 판유리5: non-screen printing layer 6: decorative pane

본 발명은 폴리비닐알코올(PVA)을 주제로 하여 일반 판유리상에 부분적으로 다색도를 갖는 거울 처리하여 장식성을 가일층 배가시켜 줄 수 있도록 한 다색도 부분 칼라경을 갖는 장식용 판유리의 가공방법에 관한 것으로, 특히 본 발명은 폴리비닐알코올(PVA)을 메칠알코올에 1차 교반, 용해한 후 이를 중탕하고 냉각시킨 다음, 이 용액과 아세톤에 소망하는 색상의 염료를 용해시켜 준 용액을 투입, 교반하여 혼합한 용액을 얻은 다음, 이 혼합용액을 가공코져 하는 판유리 전표면상에 브럿싱가공 방법등에 의해 전면도포하여 코팅처리한 후 이를 건조하여 칼라층을 형성하고 코팅처리된 이 칼라층 전표면상에 공지한 방법으로 알루미늄 진공증착(또는 은경반응)하여 염료에 의한 색상을 나타내는 전면 칼라거울판을 얻은 다음, 이를 다시 소망하는 문자나 도형에 따라 수지잉크등으로 알루미늄 진공 증착층상에 스크린 인쇄방법에 의하여 문자나 도형에 의한 인쇄층을 형성하여 준 다음, 이 표면을 염화제 2철을 메칠알코올에 투입하여 혼합시킨 용액으로 처리하여 비 스크린 인쇄층의 알루미늄 진공 증착층과 폴리비닐알코올, 메칠알코올 및 아세톤, 염료등의 표면 칼라 코팅층이 제거되고 스크린 인쇄층의 부위만을 판유리상에 존재하게 되어 다양한 색상의 소망하는 무늬, 모양의 부분 칼라경을 표현하게 되어 유리 특히 거울효과를 갖는 판유리의 장식성을 가일층 향상시켜 줄 수 있도록 함으로서, 건축자재는 물론 사진틀, 시계유리판, 장식유리판 등 다양한 용도로 사용할 수 있는 다색도 칼라경을 갖는 장식용 판유리를 제공할 수 있게 한 것이다.The present invention relates to a processing method of a decorative glass plate having a multi-colored partial color diameter to be able to further enhance the decorative properties by partially mirrored on a common glass plate on the basis of polyvinyl alcohol (PVA) In particular, in the present invention, polyvinyl alcohol (PVA) is firstly stirred and dissolved in methyl alcohol, followed by agitation and cooling of the polyvinyl alcohol (PVA), and then a solution obtained by dissolving a dye of a desired color in a solution and acetone is added and stirred. After the solution is obtained, the mixed solution is coated on the entire surface of the plate glass to be processed by a brushing method or the like, and then coated and dried to form a color layer. Vacuum deposition (or silver hardening) of aluminum gives a full-color mirror plate that shows the color of the dye, and then again According to the figure, a printing layer formed by letters or figures is formed on the aluminum vacuum deposition layer by a resin ink or the like by using a screen printing method, and then the surface is treated with a solution in which ferric chloride is added to methyl alcohol and mixed. The aluminum vacuum deposition layer of the screen printing layer and the surface color coating layers such as polyvinyl alcohol, methyl alcohol, acetone, and dyes are removed, and only the portions of the screen printing layer are present on the plate glass, so that the desired patterns and shapes of various colors are formed. By expressing the mirror, it is possible to further improve the decorativeness of glass, especially the glass plate with a mirror effect.The decorative plate glass with multicolored color mirror which can be used for various purposes such as photo frame, clock glass plate, decorative glass plate as well as building materials. It is to be provided.

일반적으로 다색경은 이미 소개되어 있으나 이는 판유리상에 안료나 염료를 투입한 상태에서 알루미늄 진공증착이나 질산은경 증착을 하여 전면 다색경을 얻는 방법이 대부분이다. 그러나 상기와 같은 방법은 안료나 염료의 색상이 알루미늄 진공증착이나 질산은경 증착작업시 유리자체에 침투되기 때문에 알루미늄 진공 증착된 부분등을 제거하게 되더라도 유리표면상에 안료 염료등의 색상이 그대로 존재하게 되어, 이들의 제거가 불가능하게 됨으로서 부분 칼라경의 판유리의 제조가 불가능하였다. 따라서 이러한 실정을 감안하여 유리일부에 거울이 형성되는 거울 유리장식판이 사진틀이나 건축자재의 장식용 판유리를 등장하고 있으나, 이는 단순히 알루미늄 진공증착한 후 스크인인쇄방법에 의해 염화제2철로 부분적으로 알루미늄 진공증착면을 제거하여 무늬모양이나 문자상의 부분거울 장식판을 형성하게 됨으로서 이는 단색 특히 일반거울색상의 판유리만을 얻을 수 없는 단조로움이 있어 다양한 색상의 장식성을 부여할 수 없는 폐단이 있었다.Generally, multicolor mirrors have already been introduced, but most of these methods are obtained by vacuum deposition of aluminum or silver nitrate with the addition of pigments or dyes on plate glass. However, since the pigment or dye color penetrates into the glass itself during aluminum vacuum deposition or silver nitrate deposition, the color of the pigment dye remains on the glass surface even if the aluminum vacuum deposited portion is removed. Thus, the removal of these was impossible, and thus the manufacture of the plate glass of the partial collar diameter was impossible. Therefore, in view of this situation, the mirror glass decorative plate in which the mirror is formed on the glass part has appeared in the decorative frame glass of the photo frame or the building material, but this is simply aluminum vacuum deposited by ferric chloride and then partially vacuumed by aluminum printing. By removing the deposition surface to form a decorative pattern of the mirror or pattern of letters, there is a monotony that can not be obtained only the plate glass of a single color, especially the general mirror color, there was a closed end that can not give a variety of decorative colors.

또한, 판유리상에 특별히 다양한 색상의 무늬 모양을 얻기 위한 경우에는 판유리상에 염료가 배합된 수지 잉크로서 스크린인쇄하여 여러 가지 색상의 칼라 무늬를 형성하는 장식용 판유리도 존재하고 있으나, 이는 단순히 판유리상에 스크린 인쇄방법에 의하여 무늬모양층을 형성하는 것이기 때문에 완벽한 거울의 효과등을 나타낼 수 없는 것이어서 거울장식판으로서의 장식성이나 기능은 기대할 수 없는 단조로움이 있었다.In addition, in order to obtain a pattern of a variety of colors on the plate glass, there is also a decorative plate glass that forms a color pattern of various colors by screen printing as a resin ink in which dyes are mixed on the plate glass, it is simply on the plate glass Since the pattern printing layer is formed by the screen printing method, the effect of the perfect mirror cannot be exhibited, and thus the decorativeness and function as the mirror decorative plate were unpredictable.

본 발명은 상기와 같은 점을 감안하여 다양한 색상을 지니는 부분 칼라경을 판유리상에 표현하여 거울을 겸할 수 있는 장식용 판유리를 제공함에 목적을 두고 있으며, 판유리상에 형성되는 거울면에 소망하는 다양한 색상을 부여함으로서 다색도 칼라경의 무늬, 모양을 갖는 판유리의 장식성 등을 가일층 배가시켜 줄 수 있도록 함에 또다른 목적을 두고 있는 것이다.In view of the above, the present invention aims to provide a decorative plate glass that can serve as a mirror by expressing a partial color mirror having various colors on a plate glass, and various colors desired on a mirror surface formed on the plate glass. Another purpose is to further increase the decoration of the plate glass having a multi-colored color mirror pattern, shape, etc. by giving a.

이러한 목적을 달성하기 위해 본 발명은 폴리비닐알코올(PVA)를 주제로 하고, 이를 메칠알코올에 용해시켜 중탕, 냉각한 용액에 염료를 아세톤에 용해시킨 용액을 혼합, 교반한 용액을 판유리 일측면 전면에 도포, 코팅하여 건조하여서 칼라층을 형성하고 표면에 알루미늄 진공증착에 의하여 거울면을 형성하는 알루미늄 진공증착층을 형성시켜 준다음, 이 표면을 다시 수지잉크나 페인트 등으로 소망하는 무늬나 문자를 스크린인쇄하여 무늬문자의 스크린 인쇄층을 형성하여 준 후 이를 염화제2철과 알코올을 혼합한 제거액을 도포하여 비스크린 인쇄층의 알루미늄 진공증착층과 염료가 혼합된 폴리비닐알코올(PVA)층을 제거함을 특징으로 하는 것으로, 이를 첨부한 도면과 그 실시예에 의거 더욱 상술하면 다음과 같다.In order to achieve the above object, the present invention is based on polyvinyl alcohol (PVA), mixed with a solution of dye dissolved in acetone in a bath and cooled solution by dissolving it in methyl alcohol, and stirring the solution in front of the plate glass. After coating, coating, and drying to form a color layer, the aluminum vacuum deposition layer forming a mirror surface by aluminum vacuum deposition is formed on the surface. After screen printing to form a screen printing layer of the pattern character, and then apply the removal solution mixed with ferric chloride and alcohol to the polyvinyl alcohol (PVA) layer mixed with aluminum vacuum deposition layer and dye of the non-screen printing layer It is characterized in that the removal, in more detail based on the accompanying drawings and embodiments thereof as follows.

[제1공정][Step 1]

본 공정은 판유리(1)상에 다색도 칼라를 갖는 칼라층(2)을 형성하기 위한 조성물의 조성에 대한 공정이다. 본 공정에 있어서의 코팅도포용액을 폴리 비닐알코올(PVA)을 교반기에 투입하고, 이 폴리비닐 알코올(PVA) 100g 중량에 대하여 메칠알코올 1000cc를 서서히 투입하면서 10-20분간 교반하여 용해시킨다.This step is a step for the composition of the composition for forming the color layer 2 having the multi-colored color on the pane 1. The polyvinyl alcohol (PVA) is put into a stirrer for the coating solution in this process, and it melt | dissolves for 10-20 minutes, gradually adding 1000 cc of methyl alcohol with respect to 100 g weight of this polyvinyl alcohol (PVA).

이와 같이 된 용액을 40-50℃ 정도의 미열로서 중탕한 후 냉각시킨 다음, 아세톤 800cc에 대하여 소망하는 색상의 염료 20-30g의 비율로 용해시킨 액을 상기 폴리비닐알코올(PVA)와 메칠알콜 용액에 1 : 2의 비율로 투입, 교반하여 희석한다.The solution thus obtained was bathed with mild heat of about 40-50 ° C., cooled, and then dissolved in a ratio of 20-30 g of a dye of a desired color with respect to acetone 800 cc. The polyvinyl alcohol (PVA) and methyl alcohol solution Into a 1: 2 ratio, dilute by stirring.

이때의 각 조성물은 다음과 같다.Each composition at this time is as follows.

[조성예][Composition example]

Figure kpo00001
Figure kpo00001

[제2공정][Step 2]

본 공정은 판유리(1)상에 칼라층(2)과 알루미늄 진공증착에 의한 거울층(3)을 형성하기 위한 공정으로서 상기와 같이 조성된 코팅도포용액을 판유리(1)의 일전표면의 브럿싱도포 방법에 의하여 전면도포하여 코팅하고, 이 코팅처리된 판유리(1)의 표면을 열풍기로서 80-150℃의 온도로 3-7분 정도 건조시켜 경화시켜 칼라층(2)을 형성시켜 준 다음, 이 표면에 공지한 방법으로 알루미늄 진공증착하여 거울층(3)을 형성한다.This process is a process for forming the color layer 2 and the mirror layer 3 by aluminum vacuum deposition on the plate glass 1, and the coating coating solution prepared as described above is brushed on the entire surface of the plate glass 1. After coating and coating the entire surface by a coating method, the surface of the coated glass 1 is dried with a hot air at a temperature of 80-150 ° C. for 3 to 7 minutes and cured to form a color layer 2, The mirror layer 3 is formed by vacuum-depositing aluminum on this surface by a well-known method.

(첨부도면 제2a,c도 참조)(See also attached drawings 2a, c)

[제3공정][Step 3]

본 공정은 상기 제1, 제2공정에 의하여 판유리(1)의 일측전면상에 형성된 거울층(3) 상부에 문자나 무늬를 형성시키는 공정으로서 소정하는 무늬나 문자를 수지잉크나 페인트등을 사용하여 스크린 인쇄방법에 의하여 스크린 인쇄하여 인쇄층(4)를 형성하고 이를 건조시켜 준 다음, 염화제2철과 메칠알코올을 1 : 3의 비율로 혼합한 제거액으로 스크린 인쇄된 판유리(1)을 표면을 닦아 판유리(1)의 표면상의 스크린인쇄층(4) 부분을 제외한 비 스크린인쇄층(5)의 거울층(3)과 칼라층(2)을 분해, 제거하여 준다음 수세하여 본 발명의 다색도칼라경을 갖는 장식용 판유리(6)를 얻게 되는 것이다. (제2b,c도 참조)This process is to form a character or pattern on the mirror layer 3 formed on the front surface of one side of the plate glass 1 by the first and second processes, using a resin ink or paint for a predetermined pattern or character. Screen printing by the screen printing method to form a printing layer (4) and drying it, and then screen-printed the plate glass (1) with a removal liquid mixed with ferric chloride and methyl alcohol in a ratio of 1: 3 Wipe off the mirror layer (3) and the color layer (2) of the non-screen printing layer (5) except for the screen printing layer (4) portion on the surface of the plate glass 1, and then washed with water to remove the multicolor of the present invention. The decorative plate glass 6 which has a doppler diameter is obtained. (See also 2b, c)

한편, 상기 제1공정에 있어서 판유리(1)상에 도포코팅되는 칼라층(2)을 한가지 안료로 코팅처리한 상태로 설명하였으나, 판유리(1)상에 각기 다른 색상의 칼라층(2)을 부분적으로 도포, 코팅하면 판유리(1)상에 다색도의 칼라를 갖는 거울층(3)을 형성시킬 수 있게 되는 것이다. 또한 본 발명은 제1 및 제2공정에 의하여 칼라층(2)과 거울층(3)을 형성시킴에 있어 알루미늄 진공증착에 의한 거울층(3)은 판유리체(1)와의 사이에 얇은 박막의 폴리비닐알코올(PVA) 등으로 된 칼라피막이 코팅되어 있으므로서 염화제2철과 메칠알코올에 의하여 비 스크린 인쇄층(5)이 완벽하게 제거되어 투명한 상태를 유지하여, 포리염화비닐(PVA)에 의하여 형성되는 칼라층(2)은 박막상태로 존재하게 되어 거울층(3)의 반사효과나 상의선명도에 아무런 영향을 미치지 않고 완벽한 거울의 효과와 기능을 발휘하게 되는 것이다. 또한 본 발명에 있어 최종적인 다색도 칼라경을 스크린인쇄기법에 의하여 정교한 무늬형태로 어떠한 위치에서도 배시할 수 있어 건축재 장식용판유리는 물론 부분적인 거울효과를 요구하는 장치품예로서 시계유리, 사진틀, 가구용유리등 다용도로 사용할 수 있는 특징을 지니고 있는 것이다.Meanwhile, in the first step, the color layer 2 applied and coated on the plate glass 1 is described with one pigment, but the color layers 2 of different colors on the plate glass 1 are applied. Partially applied and coated, it is possible to form a mirror layer 3 having a multicolored color on the pane 1. In the present invention, in the formation of the color layer 2 and the mirror layer 3 by the first and second processes, the mirror layer 3 by vacuum deposition of aluminum is formed of a thin film between the plate glass body 1. The non-screen printing layer 5 is completely removed by ferric chloride and methyl alcohol while maintaining a transparent state by coating a color film made of polyvinyl alcohol (PVA) or the like, and by polyvinyl chloride (PVA) The color layer 2 to be formed is in a thin film state and exhibits the effect and function of the perfect mirror without affecting the reflection effect or the image sharpness of the mirror layer 3. In addition, the final multi-color color mirror in the present invention can be displayed at any position in the form of elaborate pattern by the screen printing method, such as the glass plate for building materials, as well as a device product that requires a partial mirror effect, such as watch glass, photo frame, furniture glass It has features that can be used for many purposes.

Claims (3)

폴리비닐알코올(PVA) 100g 중량에 대하여 메칠알코올 1000cc를 서서히 투입교반하여 용해시킨 다음 40-50℃정도의 온도로 중탕한 후 냉각하고, 이에 아세톤 400cc에 대하여 염료 10-15g을 용해시켜 투입, 교반한 다음 이를 판유리(1) 표면에 브럿싱도포, 코팅처리하여 칼라층(2)을 형성시킨 다음, 이 상면에 공지와 같이 알루미늄 진공증착하여 거울층(3)을 형성하고, 이 상면에 수지잉크로 스크린인쇄하여 스크린인쇄층(4)을 형성한 다음, 비 스크린 인쇄층(5)의 거울층(3)과 칼라층(2)을 염화제2철과 메칠알코올을 1 : 3의 비율로 혼합된 용액으로 제거함을 특징으로 하는 다색도 부분칼라경을 갖는 장식용 유리판의 가공방법.1000cc of methyl alcohol is slowly added and stirred to dissolve 100g of polyvinyl alcohol (PVA), followed by agitation at a temperature of about 40-50 ° C, followed by cooling. Then, brushing and coating the surface of the plate glass (1) to form a color layer (2), and then vacuum-deposited aluminum on this upper surface to form a mirror layer (3), the resin ink on the upper surface Screen printing to form a screen printing layer (4), then mixing the mirror layer (3) and color layer (2) of the non-screen printing layer (5) in a ratio of 1: 3 ferric chloride and methyl alcohol Process for processing a decorative glass plate having a multi-color partial color mirror, characterized in that the removal with a solution. 청구범위 제1항에 있어서, 칼라층은 다음 조성비로 됨을 특징으로 하는 다색도 부분칼라경을 갖는 장식용 유리판의 가공방법.The method for processing a decorative glass plate according to claim 1, wherein the color layer has a next composition ratio. [조성비][Composition ratio]
Figure kpo00002
Figure kpo00002
 청구범위 제1항에 있어서, 비 스크린 인쇄층(5)의 칼라층(2) 및 거울층(3)의 제거액은 염화제2철과 메칠알코올을 1 : 3의 비율로 혼합함을 특징으로 하는 다색도 부분칼라경을 갖는 장식용 유리판의 가공방법.The method of claim 1, wherein the removal liquid of the color layer 2 and the mirror layer 3 of the non-screen printing layer 5 is characterized in that the ferric chloride and methyl alcohol are mixed in a ratio of 1: 3. A method for processing a decorative glass plate having a multi-color partial color diameter.
KR1019900004062A 1990-03-26 1990-03-26 Preparation method of decorative glass plate KR920002632B1 (en)

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