KR900006496A - 수성매질에 분산시킨 희토류 할로겐화물의 분산액 - Google Patents

수성매질에 분산시킨 희토류 할로겐화물의 분산액 Download PDF

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KR900006496A
KR900006496A KR1019890014526A KR890014526A KR900006496A KR 900006496 A KR900006496 A KR 900006496A KR 1019890014526 A KR1019890014526 A KR 1019890014526A KR 890014526 A KR890014526 A KR 890014526A KR 900006496 A KR900006496 A KR 900006496A
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rare earth
acid
dispersion
radical
earth halides
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KR1019890014526A
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KR930000653B1 (ko
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세고 끄리스띠앙
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쟝-삐에르 에송
롱-쁠랑 쉬미
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Abstract

내용 없음

Description

수성매질에 분산시킨 희토류 할로겐화물 분산액
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (38)

  1. (a) 에틸렌계 불포화 카르복실산 또는 그의 유도체와 α-올레핀 화합물 및/또는 비닐 화합물의 공중합체. (b) 에틸렌계 불포화 카르복실산 또는 그의 유도체의 단복 중합체 또는 공중합체. (c) 하나이상의 에틸렌계 불포화 카르복실산과 하나이상의 에틸렌계 불포화 술폰산염의 공중합체. (d) (아릴알킬) 페놀의 산화 알킬렌, 경우에 따라 그의 인산염 또는 황산염의 중합체로 이루어진 군중에서 선택되는 하나 이상의 분산체, 및 하나이상의 희토류 할로겐화물을 포함함을 특징으로 하는 수성매질 중의 희토류 할로겐화물을 포함함을 특징으로 하는 수성매질 중의 희토류 할로겐화물 분산액.
  2. 제1항에 있어서, 희토류 할로겐화물이 희토류 삼플루오르 화합물임을 특징으로 하는 할로겐화물의 분산액.
  3. 제1 또는 2항에 있어서. 희토류 할로겐화물이 세륨, 란탄, 프라세오디뮴, 네오디뮴 및/또는 사마륨임을 특징으로 하는 희토류 할로겐화물 분산액.
  4. 제1 내지 3항중 어느 한항에 있어서, 희토류 할로겐화물이 0.1 내지 0.5㎛의 결정립 평균직경을 나타내는 삼플루오르화 세륨임을 특징으로 하는 희토류 할로겐화물 분산액.
  5. 제1 내지 4항중 어느 한 항에 있어서, 분산제가 하기로 부터 수득된 공중합체(a)임을 특징으로 하는 희토류 할로겐화물 분산액.
    * 식(I)의 불포화 카르복실산 또는 그의 유도체중 하나,
    (식(I)중, -X는 수소원자, 또는 무기 또는 유기염기의 잔기를 나타내고, -Ra는 수소원자 경우에 따라 -COOX기를 보유하는 1내지 10개의 탄소원자를 갖는 알킬 라디칼이고, -Rb는 수소원자 또는 -COOX기이다)
    * 식(II)에 해당하는 α-올레핀 화합물 및/또는 식(III)의 비닐 화합물,(II);CH2 (III) 식(II) 및 (III)중, -RC는 수소원자 또는 1내지 4개의 탄소원자를 갖는 직쇄 또는 분지된 알킬 라디칼을 나타내고, -Rd는 1내지 12개의 탄소원자를 갖는 직쇄 또는 분지된 알킬 라디칼을 나타내고, -Re는 수소원자 또는 1내지 4개의 탄소원자를 갖는 직쇄 또는 분지된 알킬 라디칼을 나타내고, -Rf는 하기의 기중 하나를 나타낸다.: Rg는 수소원자, 또는 1내지 4개의 탄소원자를 갖는 하나이상의 알킬 라디칼을 나타낸다.
    ·Cl
    ·OOC-Rh: Rh는 1내지 8개의 탄소원자를 갖는 알킬 라디칼이다.
    ·O-Rj: Rj는 Rh와 동일한 의미를 갖는다.
    ·COOX
    ·COO-Rj는 Rh와 동일한 의미를 갖는다.
    ·CO-NH2
    ·C=N
  6. 제5항에 있어서, 공중합체(a)의 성분으로 사용되는 에틸렌계 불포화 카르복실산 또는 유도체가 말레산 또는 푸마르산 또는 에스테르, 헤미에스테르 같은 그의 유도체; 이타콘산, 시크라콘산; 말레산 무수물; 모노-및 디알킬 말레산, 밀 모노- 및 디알킬 푸마르산(알킬라디칼은 1 내지 4개의 탄소원자를 갖는다) 임을 특징으로 하는 희토류 할로겐화물의 분산액.
  7. 제5 또는 6항에 있어서, 공중합체(a)의 성분으로 사용되는 α-올레핀 화합물이 에틸렌, 프로필렌, 1-부텐, 이소부틸렌, n-1-펜텐, 이소프렌, 2-메틸-1-부텐, n-1-헥센, 2-메틸-1-펜텐, 4-메틸-1-펜텐, 2-에틸-1-부텐, 2,4,4-트리메틸-1-펜텐(디이소부틸렌이라고 불림), 1,3-부라디엔, 1,3-펜타디엔, 1,3-헥사디엔, 1,3-옥타디엔, 2-메릴-3,3-디메틸-1-펜텐, 2-메틸-4,4-디메틸-1-펜텐임을 특징으로 하는 희토류 할로겐화물의 분산액.
  8. 제5 내지 7항중 어느 한 항에 있어서, 공중합체(a)의 성분으로 사용되는 비닐 화합물이 스티렌, 염화비닐; 아세트산 비닐,프로피온산 비닐, 부티르산 비닐 같은 1내지 8개의 탄소원자를 가진 지방족산의 비닐 에스테르; 산화메틸 및 산화비닐 같은 비닐 에테르; 아크릴산 또는 메타크릴산 및 아크릴산 메틸, 아크릴산 에틸, 아크릴산 부틸, 메타크릴산 메틸, 메타크릴산 에틸, 메타크릴산 부틸 같은 1내지 8개의 탄소원자를 함유하는 알킬 에스테르, 아크릴아미도, 메타크릴아미도, 아크릴로니트릴, 메타크릴로니트릴 임을 특징으로 하는 희토류 할로겐화물의 분산액.
  9. 제5항에 있어서, 공중합체(a)가 무수 말레산-디이소부틸렌 공중합체임을 특징으로 하는 희토류 할로겐화물의 분산액.
  10. 제5 내지 9항중 어느 한 항에 있어서, 공중합체(a)가 500 내지 50,000의 중량 평균 분자량을 가짐을 특징으로 하는 희토류 할로겐화물의 분산액.
  11. 제10항에 있어서, 공중합체(a)가 500 내지 15,000의 중량평균 분자량을 가짐을 특징으로 하는 희토류 할로겐화물의 분산액.
  12. 제5 내지 11항중 어느 한 항에 있어서, 식(I)의 카르복실산/식(II) 및/또는(III)의 불포화 화합물의 몰비가 1임을 특징으로 하는 희토류 할로겐화물의 분산액.
  13. 제5 내지 12항중 어느 한 항에 있어서, 공중합체(a)가 유기용매내에서 라디칼 중합에 의한 수득됨을 특징으로 하는 희토류 할로겐화물의 분산액.
  14. 제13항에 있어서, 공중합체(a)가, pH 8내지 12로 수득될때까지 염기의 첨가에 의해 중화됨을 특징으로 하는 희토류 할로겐화물의 분산액.
  15. 제1 내지 4항중 어느 한 항에 있어서, 분산제가 하기식(IV)에 해당하는 하나이상의 에틸렌계 불포화 카르복실산 도는 그의 유도체 중 하나를 중합시킨 중합체(b)임을 특징으로 하는 희토류 할로겐화물의 분산액.
    (식(IV)중, -R'는 수소원자, 염소원자 또는 경우에 따라 -COOX기를 보유하는 1내지 4개의 탄소원자를 갖는 직쇄 또는 분지된 알킬 라디칼을 나타내고, -R"는 수소원자 또는 1내지 4개의 탄소원자를 갖는 직쇄 또는 분지된 알킬 라디칼을 나타내고, -R"'은 수소원자, 1내지 4개의 탄소원자를 갖는 직쇄 또는 분지된 알킬 라디칼, 또는 -COOX기를 나타내고, -X는 상기 주어진 의미를 갖는다).
  16. 제15항에 있어서, 중합체(b)가 아크릴 또는 메타크릴산 및 메틸, 에틸 또는 부틸의 아크릴레이트 또는 메타크릴레이트, 에타크릴산, α-클로로아클리산, 크로톤산, 아타콘산, 말레산, 푸마르산, 시트라콘산, 메사콘산 등과 같은 1내지 4개의 탄소원자를 포함하는 그의 알킬 에스테르의 중합으로 부터 생성됨을 특징으로 하는 희토류 할로겐화물의 분산액.
  17. 제16항에 있어서, 중합체(b)가 아크릴산 및/또는 메타크릴산의 중합으로 부터 생성됨을 특징으로 하는 희토류 할로겐화물의 분산액.
  18. 제16 또는 17항에 있어서, 중합체(b)가 수산화나트륨, 수산화칼륨, 수산화 암모늄, 또는 수산화 알킬을 아민 같은 염기에 의해 처리됨을 특징으로 하는 희토류 할로겐화물의 분산액.
  19. 제1 내지 4항중 어느 한 항에 있어서, 공중합체(c)의 성분으로 사용되는 에틸렌계 불포화 카르복실산의 아크릴산, 메타크릴산, 에타크릴산, α-클로로아크릴산, 크로톤산, 이타콘산, 말레산, 푸마르산, 시트라콘산, 메사콘산임을 특징으로 하는 희토류 할로겐화물의 분산액.
  20. 제19항에 있어서, 에틸렌계 불포화 카르복실산의 아크릴산 또는 메타크릴산임을 특징으로 하는 희토류 할로겐화물의 분산액.
  21. 제19항 또는 20항의 에틸렌계 불포화 카르복실산이 0.05/l 내지 10/l의 몰비에 따른 아크릴산 및 메타크릴산의 혼합물임을 특징으로 하는 희토류 할로겐화물의 분산액.
  22. 제21항에 있어서, 에틸렌계 불포화 카르복실산이 0.10/l 내지 6/l의 몰비에 따른 아크릴산 및 메타크릴산의 혼합물임을 특징으로 하는 희토류 할로겐화물의 분산액.
  23. 제19 내지 22항중 어느 한 항에 있어서, 공중합체(c)의 조성 내에 도입되는 에틸렌계 불포화 술폰산의 염기 알킬술폰산, 메탈릴술폰산, 비닐술폰산 또는 스티렌 술폰산의 알칼리 금속염 또는 암모늄염임을 특징으로 하는 희토류 할로겐화물의 분산액.
  24. 제23항에 있어서, 에틸렌계 불포화 술폰산의 염이 메탈릴술폰산 나트륨 또는 메탈릴 술폰산 칼륨임을 특징으로 하는 희토류 할로겐화물의 분산액.
  25. 제19 내지 24항중 어느 한 항에 있어서, 에틸렌계 불포화 술폰산 염의 몰 백분율이 전체 모노머 혼합물의 1내지 60몰%를 나타냄을 특징으로 하는 희토류 할로겐화물의 분산액.
  26. 제25항에 있어서, 상기 몰 백분율이 전체 모노리 혼합물의 3 내지 8몰%를 나타냄을 특징으로 하는 희토류 할로겐화물의 분산액.
  27. 제19내지 26항중 어느 한 항에 있어서, 공중합체(c)가 500 내지 8,000의 중량 평균 분자량을 가짐을 특징으로 하는 희토류 할로겐화물의 분산액.
  28. 제27항에 있어서, 공중합체(c)가 1,500 내지 4,000의 중량 평균 분자량을 가짐을 특징으로 하는 희토류 할로겐화물의 분산액.
  29. 제1 내지 4항중 어느 한 항에 있어서, 분산제가 하기식(V) 내지 (VII)중 하나에 해당하는 중합체(d)임을 특징으로 하는 희토류 할로겐화물의 분산액.
    식(V)내지 식(VII)중, -n은 1내지 40이고, -X는 수소원자 또는 상기 정의한 것과 같은 무기 또는유기염기의 잔기이고, -R은 2내지 4개의 탄소원자를 갖는 알킬렌 라디칼이고, -R2는 잔기 X(R2=X일때, 두개의 잔기 X는 동일하거나 상이할 수 있다)이거나, R1-(O-R)-n 라디칼중 하나 (R2라디칼 및 R1-(O-R)-n 라디칼은 동일하거나 상이할 수 있다)이고, -R1식 (VIII)로 기호화된 라디칼을 나타낸다.
    식(VIII)중, m은 1,2 및 3의 정수이고, P는 1 또는 2의 정수이고, R4는 수소원자 또는 1내지 4개의 탄소원자를 갖는 알킬라디칼이고, R3라디칼은 하기식(IX)의 라디칼을 신호로 나타낸 것이다.
    식중, R5는 수소원자, 1내지 4개의 탄소원자를 갖는 알킬라디칼, 또는 페닐 라디칼을 나타낸다.
  30. 제29항에 있어서, 분산제가 하기 사항에 해당하는 식(V) 내지 (VII)중 하나인 중합체(d)임을 특징으로 하는 희토류 할로겐화물의 분산액.
    -R은 에틸렌 라디칼을 나타내고, -R1은 하기사항을 나타내는 식(VIII)의 라디칼을 나타내고, 식(VIII)중, m은 2 또는 3의 정수이고, R4는 수소원자이고, R3라디칼은 하기식(IX)의 라디칼이다.
    식중, R5는 수소원자, 메틸 또는 페닐 라디칼이다.
    -R2는 잔기 X(R2=X일때, 두개의 잔기 X는 동일하다)이거나, R1-(O-OH2-CH2)-n 라디칼 (R2라디칼 및 R1-(O-CH1-CH2)-n 라디칼은 동일하다)이다.
  31. 제29 또는 30항에 있어서, 분산제가 하기 사항에 해당하는 식(V) 내지 (VII)중 하나인 중합체(d)임을 특징으로 하는 희토류 할로겐화물의 분산액.
    -n은 3내지 40이고, -X는 수소원자, 나트륨원자, 칼륨원자, 암모늄라디칼, 모노에탈올아민, 디에탄올아민, 트리에탄올아민이고, -R은 에틸렌라디칼이고, -R1은 하기사항을 나타내는 식(VIII)의 라디칼을 나타내고, 식(VIII)중, m은 2 또는 3의 정수이고, R4는 수소원자이고, R3라디칼은 하기식(IX)의 라디칼이다.
    -R2는 잔기 X(R2=X일때, 두개의 잔기 X는 동일하다)이거나, R1-(O-OH2-CH2)-n 라디칼 (R2라디칼 및 R1-(O-CH1-CH2)-n 라디칼은 동일하다)이다.
  32. 제29내지 31항중 어느 한 항에 있어서, 분산제가 하기중에서 선택되는 중합체(d)임을 특징으로 하는 희토류 할로겐화물의 분산액.
    * 페놀몰당 10 내지 40몰의 산화 에틸렌(E.O.)을 갖는 트리-(1-페닐에틸)페놀폴리옥시에틸렌.
    * 페놀몰당 3 내지 20몰의 산화 에틸렌을 갖는 디-(1-페닐에틸)페놀폴리옥시에틸렌.
    * 페놀몰당 10 내지 40몰의 산화 에틸렌을 갖는, 산 또는 중화된 형의 트리-(1-페닐에틸)페놀폴리옥시에틸렌의 황산염.
    * 페놀몰당 3 내지 20몰의 산화 에틸렌을 갖는, 산 또는 중화된 형의 디-(1-페닐에틸)페놀 폴리옥시에틸렌의 황산염.
    * 페놀몰당 10 내지 40몰의 산 에틸렌을 갖는, 산화 또는 중화된 형의 트리-(1-페닐에틸)페놀 폴리옥시에틸렌 인산 모노- 및 디에스테르.
    * 페놀몰당 3 내지 20몰의 산 에틸렌을 갖는, 산화 또는 중화된 형의 디-(1-페닐에틸)페놀폴리옥시에틸렌의 인산 모노- 및 디에스테르.
  33. 제1 내지 32항중 어느 한항에 있어서, 겔화방지제 및/또는 발포방지제를 또한 포함함을 특징으로 하는 희토류 할로겐화물의 분산액.
  34. 제1 내지 33항중 어느 한 항에 있어서, 하기의 것을 포함함을 특징으로 하는 희토류 할로겐화물의 분산액.
    - 5내지 80%의 하나이상의 희토류 할로겐화물, - 0.1 내지 12%의 분산제(a),(b),(c) 및/또는 (d), - 0 내지 5%의 발포방지제, - 0 내지 20%의 겔화방지제, -100%를 수득하기 위한 충분량의 물.
  35. 제34항에 있어서, 하기의 것을 포함함을 특징으로 하는 희토류 할로겐화물의 분산액.
    - 20 내지 60%의 하나이상의 희토류 할로겐화물, - 0.4 내지 8%의 분산제(a),(b),(c) 및/또는 (d), - 0 내지 3%의 발포방지제, - 0 내지 15%의 겔화방지제, -100%를 수득하기 위한 충분량의 물.
  36. 분산제(a)(b)(c) 및 또는 (d), 경우에 따라 겔화방지제, 분산매질을 구성하는 물을 포함하는 용액을 제조하고, 하나이상의 회토류 할로겐화물을 교반하에서 분산시킨 후, 분산액을 분쇄하고, 경우에 따라 수득된 분산의 기체를 제거하는 것으로 구성됨을 특징으로 하는 제1 내지 35항중 어느 한항에 기재된 수성 매질중 희토류 할로겐화물 분산액의 제조방법.
  37. 제36항에 있어서, 발포방지제가 분쇄 과정중 또는 기체 제거시에 첨가됨을 특징으로 하는 방법.
  38. 윤활제 분야에서의, 제1 내지 35항중 한 항에 기재된 희토류 할로겐화물의 분산액의 용도.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019890014526A 1988-10-10 1989-10-10 수성매질에 분산시킨 희토류 할로겐화물의 분산액 KR930000653B1 (ko)

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GB2228274B (en) * 1989-01-12 1992-01-02 Sandoz Ltd Surface active compositions their production and use
FR2732620B1 (fr) * 1995-04-10 1997-05-09 Coatex Sa Copolymeres utilises comme dispersant ameliorant la resistance a l'eau des films de compositions aqueuses chargees et/ou pigmentees ainsi que les compositions les contenant
CN1058985C (zh) * 1998-10-08 2000-11-29 中国科学院兰州化学物理研究所 纳米氟化稀土润滑油添加剂
CN1058984C (zh) * 1998-10-08 2000-11-29 中国科学院兰州化学物理研究所 纳米氢氧化稀土润滑油添加剂
JP5532199B2 (ja) * 2008-11-07 2014-06-25 株式会社豊田中央研究所 金属化合物のコロイド溶液およびその製造方法

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FR1279937A (fr) * 1960-07-29 1961-12-29 Cincinnati Milling Machine Co Solution aqueuse de refroidissement, pour l'usinage de matières ferreuses
DE1594511A1 (de) * 1966-01-21 1970-12-17 Dow Corning Gmbh Gesenkschmierstoffe
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JPS53129200A (en) * 1977-04-18 1978-11-10 Shiraishi Kogyo Kk Dispersant for calcium carbonate
FR2483932B1 (fr) * 1980-06-09 1985-08-02 Rhone Poulenc Spec Chim Nouvelles compositions polymere acrylique, procede pour leur obtention, et application notamment comme agents antitartres
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DE3508704A1 (de) * 1985-03-12 1986-09-18 Basf Ag, 6700 Ludwigshafen Verwendung von copolymerisaten auf basis von alkyl (meth)-acrylaten als dispergiermittel fuer pigmente und waessrige pigmentanschlaemmungen
FR2581323B1 (fr) * 1985-05-06 1987-05-29 Rhone Poulenc Spec Chim Nouvelle composition tensio-active, son procede d'obtention et ses applications
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KR930000653B1 (ko) 1993-01-29
NO894000D0 (no) 1989-10-06
NO894000L (no) 1990-04-11
FI894794A (fi) 1990-04-11
EP0364328B1 (fr) 1992-06-24
US4946607A (en) 1990-08-07
EP0364328A2 (fr) 1990-04-18
DE68901909D1 (de) 1992-07-30
FI894794A0 (fi) 1989-10-09
GR3005761T3 (ko) 1993-06-07
ZA897657B (en) 1990-07-25
DE68901909T2 (de) 1993-02-04
EP0364328A3 (en) 1990-07-04
JPH02164715A (ja) 1990-06-25
AU4269689A (en) 1990-04-12
BR8905084A (pt) 1990-05-15
AU613798B2 (en) 1991-08-08
ATE77645T1 (de) 1992-07-15

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