KR890009450A - 다중 흡착 베드를 이용한 흡착분리 - Google Patents
다중 흡착 베드를 이용한 흡착분리 Download PDFInfo
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- KR890009450A KR890009450A KR1019880018222A KR880018222A KR890009450A KR 890009450 A KR890009450 A KR 890009450A KR 1019880018222 A KR1019880018222 A KR 1019880018222A KR 880018222 A KR880018222 A KR 880018222A KR 890009450 A KR890009450 A KR 890009450A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
- B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
- B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
- B01D53/047—Pressure swing adsorption
- B01D53/0476—Vacuum pressure swing adsorption
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
- B01D2253/10—Inorganic adsorbents
- B01D2253/102—Carbon
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
- B01D2253/10—Inorganic adsorbents
- B01D2253/106—Silica or silicates
- B01D2253/108—Zeolites
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2257/00—Components to be removed
- B01D2257/10—Single element gases other than halogens
- B01D2257/102—Nitrogen
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2257/00—Components to be removed
- B01D2257/50—Carbon oxides
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2259/00—Type of treatment
- B01D2259/40—Further details for adsorption processes and devices
- B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
- B01D2259/40043—Purging
- B01D2259/4005—Nature of purge gas
- B01D2259/40052—Recycled product or process gas
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2259/00—Type of treatment
- B01D2259/40—Further details for adsorption processes and devices
- B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
- B01D2259/40058—Number of sequence steps, including sub-steps, per cycle
- B01D2259/40062—Four
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2259/00—Type of treatment
- B01D2259/40—Further details for adsorption processes and devices
- B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
- B01D2259/40058—Number of sequence steps, including sub-steps, per cycle
- B01D2259/40064—Five
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2259/00—Type of treatment
- B01D2259/40—Further details for adsorption processes and devices
- B01D2259/403—Further details for adsorption processes and devices using three beds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2259/00—Type of treatment
- B01D2259/40—Further details for adsorption processes and devices
- B01D2259/404—Further details for adsorption processes and devices using four beds
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02C—CAPTURE, STORAGE, SEQUESTRATION OR DISPOSAL OF GREENHOUSE GASES [GHG]
- Y02C20/00—Capture or disposal of greenhouse gases
- Y02C20/40—Capture or disposal of greenhouse gases of CO2
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- Engineering & Computer Science (AREA)
- Analytical Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Separation Of Gases By Adsorption (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
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Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
제 1 도는 4개의 평행한 흡착 베드와 생산물 건조 단계를 이용한 본 발명의 바람직한 구체화의 개요도이다.
제 2 도는 주요 성분 저장기 및 생성물 건조단계와 3개의 평행한 흡착 베드를 이용한 본 발명의 따른 구체화의 개요도이다.
Claims (28)
- 다수의 평행흡착 베드를 사용하여 주요성분을 함유하는 기체혼합물로부터 높은 순도 및 더욱 큰 선택도로 흡착된 주요성분과 하나 또는 그 이상으로 적온선택성으로 흡착된 이온성분을 산출하는 공정에 있어서 ; (a)진공화된 평행베드의 유출단부에 제 1흡착베드의 유출단부를 연결시켜 제1흡착베드의 공급단부를 지나 상기 기체혼합물을 통과시켜 상기 주요성분을 제 1 흡착베드상에 선택적으로 흡착시키고 하나 또는 그 이상의 제2성분을 상기 제 1 베드에 통과시키고 ; (b)상기 제 1베드를 고순도의 주요성분으로 병류세정하여 모든 공동-흡착된 제 2성분을 제거하여 상기 베드로부터 제 2성분의 공간을 비우고 ; (c)하나 또는 그 이상의 단계에서 준 대기압으로 감압하여 상기 제 1베드를 역류탈착시켜 단계(b)의 상기 다수단 이외에서 세정기체와 고순도 주요성분 생성물을 회수하고 (d)단계 (c)마지막의 준 대기압하의 제 1베드의 유출단부를 단계(a)의 흡착이 실시되는 다수의 다른 베드유출단부와 연결하여 상기 제1베드를 역류재가압하고 ; (e)이러한 일련의 단계를 다수의 베드로연결시켜 고순도 주요성분을 생성하는 연속공정으로 구성되는 것을 특징으로 하는 공정.
- 제 1항에 있어서, 단계(c)에서 작동하는 하나의 베드로 부터 회수되는 세정기체가 단계(b)에서 작용하는 다른 베드의 세정기체로 직접 사용되는 것을 특징으로 하는 공정.
- 제 1항에 있어서, 단계(c)가 2단계를 포함하는데, 제1단계를 흡착된 기체가 평행베드를 세정하는데 사용되는 주위압력에서 끝나고 제 2 단계는 탈착된 기체가 주요성분생성물인 상기 준대기압에서 끝나는 것으로 구성되는 것을 특징으로 하는 공정.
- 제 1항에 있어서, 기체 혼합물에 함유된 모든 물과 이산화탄소가 상기 다수베드의 흡착제의 초기부에 흡착되는 것을 특징으로 하는 공정.
- 제 4항에 있어서, 각각의 흡착베드가 유출단에 근접한 초기부내의 물과 이산화탄소를 선택적인 흡착제와 베드의 잔류부에 있는 주요성분에 선택적인 흡착제를 함유하는 것을 특징으로 하는 공정.
- 제1항에 있어서, 단계(d)재가압에서 작동하는 베드가 약14.7psia의 압력으로 재가압 되는 것을 특징으로 하는 공정.
- 제1항에 있어서, 단계(a)주입이 약12.7psia와 약 14.7psia사이의 다양한 입력으로 실시되는 것을 특징으로 하는 공정.
- 제1항에 있어서, 단계(c)의 진공화가 약50-250Torr의 압력으로 실시되는 것을 특징으로 하는 공정.
- 제1항에 있어서, 주요성분의 순도가 95%이상인 것을 특징으로 하는 공정.
- 제1항에 있어서, 주요성분의 순도가 약99.9%인 것을 특징으로 하는 공정.
- 제1항에 있어서, 4개의 평행베드가 사용되는 공정.
- 제1항에 있어서, 단계(c)에서 회수되는 주요성분이 주요성분 저장용기로 공급되는 것을 특징으로 하는 공정.
- 제1항에 있어서, (a)주입, (b)세정, (c)탈착 및 (d)재가압 단계 각각은 동일시간으로 실시되는 것을 특징으로 하는 공정.
- 제1항에 있어서, 휴지단계를 상기 제1베드가 활성 가동되지 않는 재가압 단계후에 수반되는 것을 특징으로 하는 공정.
- 제14항에 있어서, 3개의 평행베드가 이용되는 것을 특징으로 하는 공정.
- 제14항에 있어서, (a)주입단계 및(b)세정단계의 총시간은 (c)탈착단계와 동일하며, (d)로 재가압 및 휴지 단계의 총시간은 (c)탈착단계동일한것을 특징으로 하는 공정.
- 제14항에 있어서, (c)탈착단계에 회수되는 주요성분은 주요성분 저장용기에 공급되는 것을 특징으로 하는 공정.
- 제1항에 있어서, (a)단계중의 상기 제1베드를 통과하는 이차성분분액은 제2성분 생성물로서 회수되는 것을 특징으로 하는 공정.
- 내용 없음
- 제1항에 있어서, (b)세정단계로부터의 유출물은 재회수되어(a)단계의 가스혼합물과 혼합되는 것을 특징으로 하는 공정.
- 제1항에 있어서, 주요성분은 질소, 일산화탄소, 일산화탄소 또는 저급알킬 탄화수소(C2+)로 구성되는 그룹으로부터 선택되는 것을 특징으로 하는 공정.
- 제1항에 있어서, 주입가스 혼합물의 얍력은 10psig또는 그 이하인것을 특징으로 하는 공정
- 제1항에 있어서, 주입가스 혼합물의 압력은 5psig또는 그 이하인것을 특징으로 하는 공정.
- 제1항에 있어서, 주요성분은 이산화탄소이고, 흡착제는 소디움 X제오랄이트인것을 특징으로 하는 공정.
- 제1항에 있어서, 주요성분은 일산화탄소이고 흡착제는 칼슘 5A제올라이트인것을 특징으로 하는 공정.
- 제1항에 있어서, 주요성분은 저급알킬이고, 흡착제는 소디움 X제올라이트 또는 활성탄소인 것을 특징으로 하는 공정
- 제1항에 있어서, 질소가 주요성분이고, 흡착제는 칼슘 X제올라이트인것을 특징으로 하는 공정.
- 제1항에 있어서, (b)단계후에 약14.7psia로 역감압이 수반되는 것을 특징으로 하는 공정.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US07/138,983 US4813977A (en) | 1987-12-29 | 1987-12-29 | Adsorptive nitrogen generation utilizing multiple adsorption beds |
US138,983 | 1987-12-29 | ||
US87-138,983 | 1987-12-29 | ||
US88-285,468 | 1988-12-16 | ||
US07/285,468 US4892565A (en) | 1987-12-29 | 1988-12-16 | Adsorptive separation utilizing multiple adsorption beds |
Publications (2)
Publication Number | Publication Date |
---|---|
KR890009450A true KR890009450A (ko) | 1989-08-02 |
KR910004122B1 KR910004122B1 (ko) | 1991-06-22 |
Family
ID=26836750
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019880018222A KR910004122B1 (ko) | 1987-12-29 | 1988-12-29 | 다중 흡착베드를 이용한 흡착분리 |
Country Status (6)
Country | Link |
---|---|
US (1) | US4892565A (ko) |
EP (1) | EP0327732A1 (ko) |
JP (1) | JPH01258721A (ko) |
KR (1) | KR910004122B1 (ko) |
CA (1) | CA1313630C (ko) |
MX (1) | MX166768B (ko) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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KR100535153B1 (ko) * | 2000-06-19 | 2005-12-07 | 현대중공업 주식회사 | 가열세정을 이용한 강흡착 성분 흡착분리방법 |
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-
1988
- 1988-12-16 US US07/285,468 patent/US4892565A/en not_active Expired - Fee Related
- 1988-12-29 CA CA000587206A patent/CA1313630C/en not_active Expired - Fee Related
- 1988-12-29 KR KR1019880018222A patent/KR910004122B1/ko not_active IP Right Cessation
- 1988-12-29 MX MX014393A patent/MX166768B/es unknown
- 1988-12-29 EP EP88121864A patent/EP0327732A1/en not_active Withdrawn
-
1989
- 1989-01-04 JP JP64000055A patent/JPH01258721A/ja active Pending
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR100535153B1 (ko) * | 2000-06-19 | 2005-12-07 | 현대중공업 주식회사 | 가열세정을 이용한 강흡착 성분 흡착분리방법 |
Also Published As
Publication number | Publication date |
---|---|
EP0327732A1 (en) | 1989-08-16 |
MX166768B (es) | 1993-02-03 |
US4892565A (en) | 1990-01-09 |
JPH01258721A (ja) | 1989-10-16 |
KR910004122B1 (ko) | 1991-06-22 |
CA1313630C (en) | 1993-02-16 |
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