KR870001272A - 디아조화 용액중 과량의 아질산염 제거방법 - Google Patents
디아조화 용액중 과량의 아질산염 제거방법 Download PDFInfo
- Publication number
- KR870001272A KR870001272A KR1019860005676A KR860005676A KR870001272A KR 870001272 A KR870001272 A KR 870001272A KR 1019860005676 A KR1019860005676 A KR 1019860005676A KR 860005676 A KR860005676 A KR 860005676A KR 870001272 A KR870001272 A KR 870001272A
- Authority
- KR
- South Korea
- Prior art keywords
- excess nitrite
- adjustment
- sulfamic acid
- remove excess
- nitrite
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0096—Purification; Precipitation; Filtration
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N27/00—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
- G01N27/26—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating electrochemical variables; by using electrolysis or electrophoresis
- G01N27/416—Systems
- G01N27/4166—Systems measuring a particular property of an electrolyte
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Biochemistry (AREA)
- Immunology (AREA)
- Physics & Mathematics (AREA)
- Analytical Chemistry (AREA)
- Molecular Biology (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Electrochemistry (AREA)
- Pathology (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
- Removal Of Specific Substances (AREA)
Abstract
내용 없음.
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
제1도는 디아조화 용액중 과량의 아질산염 연속식 제거장치
Claims (6)
- 전기화학적 조절 변수(variable)에 의해 아질산염 이온 제거용 시약의 첨가를 조절함을 특징으로 하는 방향족 아민 디아조화 용액중 과량의 아질산 염의 자동조절 연속식 제거방법.
- 제1항에 있어서, 조절용으로 사용하는 조절변수가 전위차계, 전압계 또는 폴라그라피 방법으로 측정한 값인 방법.
- 제2항에 있어서, 전위차계 방법으로 조절을 수행하고, 디아조화의 산화환원 전위를 조절 변수로서 사용하는 방법.
- 제1항 내지 제3항중 어느 하나에 있어서, 과량의 아질산염을 설팜산, 우레아 또는 4-니트로아닐린으로 제거하는 방법.
- 제4항에 있어서, 과량의 아질산 염을 설팜산으로 제거하는 방법.
- 제4항에 있어서, 설팜산을 일정한 첨가속도로 단속적으로 가하는 방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CH3052/85-8 | 1985-07-15 | ||
CH305285 | 1985-07-15 |
Publications (1)
Publication Number | Publication Date |
---|---|
KR870001272A true KR870001272A (ko) | 1987-03-12 |
Family
ID=4247532
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019860005676A KR870001272A (ko) | 1985-07-15 | 1986-07-14 | 디아조화 용액중 과량의 아질산염 제거방법 |
Country Status (6)
Country | Link |
---|---|
US (1) | US4845638A (ko) |
EP (1) | EP0209492A3 (ko) |
JP (1) | JPS6215261A (ko) |
KR (1) | KR870001272A (ko) |
BR (1) | BR8603339A (ko) |
ES (1) | ES2000664A6 (ko) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4918168A (en) * | 1987-11-24 | 1990-04-17 | Mallinckrodt Inc. | Process for the continuous diazotization of amines in a multi-stage reactor |
DK374889D0 (da) * | 1989-07-28 | 1989-07-28 | Koege Kemisk Vaerk | Fremgangsmaade til procesovervaagning |
DE4405469C2 (de) * | 1994-02-21 | 1996-11-07 | Ciba Geigy Ag | Verfahren zur Herstellung von Azofarbstoffen |
NL2018826B1 (en) | 2017-05-02 | 2018-11-09 | Spgprints B V | One-pot synthesis of reactive deep black |
Family Cites Families (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3800288A (en) * | 1972-02-24 | 1974-03-26 | Foxboro Co | Computer-directed process control system with crt display |
US4159264A (en) * | 1975-08-09 | 1979-06-26 | Ciba-Geigy Corporation | Automatic control of azo coupling processes in the manufacture of azo pigments |
GB1547760A (en) * | 1975-08-12 | 1979-06-27 | Ciba Geigy Ag | Control of continuos diazotisation of aromatic amines |
DE2741925A1 (de) * | 1977-09-17 | 1979-03-29 | Bayer Ag | Verfahren zur kontinuierlichen indirekten diazotierung von aromatischen aminen |
US4246171A (en) * | 1978-09-07 | 1981-01-20 | Ciba-Geigy Corporation | Continuous diazotization process, wherein the rate of addition of inorganic nitrite is automatically controlled by polarovoltric means |
DE2843873A1 (de) * | 1978-10-07 | 1980-04-17 | Basf Ag | Azoverbindungen |
DE2903588A1 (de) * | 1979-01-31 | 1980-08-14 | Basf Ag | Polyazofarbstoffe |
DD144118A1 (de) * | 1979-06-05 | 1980-09-24 | Kallweit Hans Juergen | Verfahren und vorrichtung zur bestimmung von nitrit sowie nitrosen gasen |
US4294755A (en) * | 1979-10-10 | 1981-10-13 | Basf Aktiengesellschaft | Pigments containing pyrazolo quinazolone radicals |
US4387422A (en) * | 1980-06-03 | 1983-06-07 | Steutermann Edward M | Control system process controller |
EP0071988B1 (en) * | 1981-08-05 | 1988-05-11 | Sumitomo Rubber Industries Limited | Apparatus for automatically measuring and controlling chemical reaction amount |
US4633413A (en) * | 1983-07-28 | 1986-12-30 | Cavro Scientific Instruments | Digital dilution apparatus and method |
US4737240A (en) * | 1985-05-02 | 1988-04-12 | Ciba-Geigy Corporation | Trisazo black dyes from 2-(4'-aminophenylazo)-7-amino-1-naphthol-3-sulfonic acid |
-
1986
- 1986-07-08 US US06/883,213 patent/US4845638A/en not_active Expired - Fee Related
- 1986-07-09 EP EP86810303A patent/EP0209492A3/de not_active Withdrawn
- 1986-07-14 ES ES8600277A patent/ES2000664A6/es not_active Expired
- 1986-07-14 KR KR1019860005676A patent/KR870001272A/ko not_active Application Discontinuation
- 1986-07-15 JP JP61164859A patent/JPS6215261A/ja active Pending
- 1986-07-15 BR BR8603339A patent/BR8603339A/pt unknown
Also Published As
Publication number | Publication date |
---|---|
ES2000664A6 (es) | 1988-03-16 |
EP0209492A2 (de) | 1987-01-21 |
EP0209492A3 (de) | 1989-11-02 |
JPS6215261A (ja) | 1987-01-23 |
BR8603339A (pt) | 1987-02-24 |
US4845638A (en) | 1989-07-04 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
WITN | Application deemed withdrawn, e.g. because no request for examination was filed or no examination fee was paid |