KR830009027A - 2-피리딜 옥시아세트아닐리드의 제조방법 - Google Patents
2-피리딜 옥시아세트아닐리드의 제조방법 Download PDFInfo
- Publication number
- KR830009027A KR830009027A KR1019820000332A KR820000332A KR830009027A KR 830009027 A KR830009027 A KR 830009027A KR 1019820000332 A KR1019820000332 A KR 1019820000332A KR 820000332 A KR820000332 A KR 820000332A KR 830009027 A KR830009027 A KR 830009027A
- Authority
- KR
- South Korea
- Prior art keywords
- formula
- reaction
- alkali metal
- carried out
- alkyl
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims 10
- RWOFNOHFTLAOPE-UHFFFAOYSA-N n-phenyl-2-pyridin-2-yloxyacetamide Chemical compound C=1C=CC=CC=1NC(=O)COC1=CC=CC=N1 RWOFNOHFTLAOPE-UHFFFAOYSA-N 0.000 title 1
- 229910052783 alkali metal Chemical group 0.000 claims 3
- AEMRFAOFKBGASW-UHFFFAOYSA-N Glycolic acid Chemical compound OCC(O)=O AEMRFAOFKBGASW-UHFFFAOYSA-N 0.000 claims 2
- 239000002253 acid Substances 0.000 claims 2
- 150000001340 alkali metals Chemical group 0.000 claims 2
- 239000011230 binding agent Substances 0.000 claims 2
- 239000003085 diluting agent Substances 0.000 claims 2
- 229910052736 halogen Inorganic materials 0.000 claims 2
- 150000002367 halogens Chemical group 0.000 claims 2
- 229910052739 hydrogen Inorganic materials 0.000 claims 2
- 239000001257 hydrogen Substances 0.000 claims 2
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims 2
- GKNOMEOXEUNEKT-UHFFFAOYSA-N 1h-pyridin-2-one;sodium Chemical compound [Na].OC1=CC=CC=N1 GKNOMEOXEUNEKT-UHFFFAOYSA-N 0.000 claims 1
- FNRMMDCDHWCQTH-UHFFFAOYSA-N 2-chloropyridine;3-chloropyridine;4-chloropyridine Chemical compound ClC1=CC=NC=C1.ClC1=CC=CN=C1.ClC1=CC=CC=N1 FNRMMDCDHWCQTH-UHFFFAOYSA-N 0.000 claims 1
- -1 alkali metal bicarbonates Chemical class 0.000 claims 1
- 229910000288 alkali metal carbonate Inorganic materials 0.000 claims 1
- 150000008041 alkali metal carbonates Chemical class 0.000 claims 1
- 150000008044 alkali metal hydroxides Chemical group 0.000 claims 1
- 150000003931 anilides Chemical class 0.000 claims 1
- 238000009835 boiling Methods 0.000 claims 1
- 239000003960 organic solvent Substances 0.000 claims 1
- 239000000376 reactant Substances 0.000 claims 1
- 239000011541 reaction mixture Substances 0.000 claims 1
- 125000001424 substituent group Chemical group 0.000 claims 1
- 150000003512 tertiary amines Chemical class 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/62—Oxygen or sulfur atoms
- C07D213/63—One oxygen atom
- C07D213/64—One oxygen atom attached in position 2 or 6
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
Landscapes
- Organic Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Plant Pathology (AREA)
- Pest Control & Pesticides (AREA)
- Health & Medical Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Pyridine Compounds (AREA)
- Cephalosporin Compounds (AREA)
- Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Plural Heterocyclic Compounds (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (9)
- a) 다음 일반식(II)의 클로로피리딘을 다음 일반식(III)의 글리콜산 N-알킬아닐리드와 반응시키거나,b) 다음 일반식(IV)의 2-피리디놀나트륨염을 다음 일반식(V)의 클로로아세토-N-알킬아닐리드와 반응시킴을 특징으로 하여 다음 일반식(I)의 2-피리딜옥시아세트아닐리드를 제조하는 방법.상기 일반식에서X는 수소, 할로겐, C1, C4알킬 또는 C1-C4할로게노알킬이고,R은 C1-C4알킬이고Y는 할로겐, C1-C4알킬, C1-C4알콕시 또는 C1-C4할로게노알킬이고,n은 0,1,2, 또는 3이며 n이 2 또는 3일 경우 치환체 Y는 독립적으로 선택되고M은 수소 또는 알칼리금속이다.
- 제1(a)항에 있어서 반응을 산결합제 존재하에 수행하는 방법.
- 제2항에 있어서, 산결합제가 알칼리금속 수산화물, 알칼리금속 카보네이트, 알칼리금속 비카보네이트, 알칼리금속 알콜레이트 및 3급 아민중에서 선택된 것인 방법.
- 제1,2 또는 3항에 있어서, 반응을 희석제 존재하에 수행하는 방법.
- 제4항에 있어서, 반응을 희석제로서 물 및/또는 하나 이상의 불활성 유기 용매 존재하에 수행하는 방법.
- 제1 내지 5항에 있어서, 반응을 -20℃ 내지 반응혼합물의 비점에서 수행하는 방법.
- 제6항에 있어서, 반응을 0˚내지 100℃에서 수행하는 방법.
- 제1 내지 7항에 있어서, 반응물이 상술한 바와 같이 특정한 것인 방법.
- 제1항에 있어서, 실시예 1 내지 19에 기술된 방법으로 제조하는 방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP56-10110 | 1981-01-28 | ||
| JP56010110A JPS57126473A (en) | 1981-01-28 | 1981-01-28 | 2-pyridyloxyacetic anilide and its preparation application |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| KR830009027A true KR830009027A (ko) | 1983-12-17 |
Family
ID=11741169
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1019820000332A KR830009027A (ko) | 1981-01-28 | 1982-01-27 | 2-피리딜 옥시아세트아닐리드의 제조방법 |
Country Status (19)
| Country | Link |
|---|---|
| US (1) | US4391629A (ko) |
| EP (1) | EP0057367B1 (ko) |
| JP (1) | JPS57126473A (ko) |
| KR (1) | KR830009027A (ko) |
| AT (1) | ATE5720T1 (ko) |
| AU (1) | AU7960882A (ko) |
| BR (1) | BR8200443A (ko) |
| CS (1) | CS228914B2 (ko) |
| DD (1) | DD219362A5 (ko) |
| DE (1) | DE3260023D1 (ko) |
| DK (1) | DK37582A (ko) |
| ES (1) | ES8301922A1 (ko) |
| GR (1) | GR75166B (ko) |
| IL (1) | IL64857A0 (ko) |
| PH (1) | PH17658A (ko) |
| PL (1) | PL129394B1 (ko) |
| PT (1) | PT74305B (ko) |
| TR (1) | TR21412A (ko) |
| ZA (1) | ZA82521B (ko) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS57149268A (en) * | 1981-03-12 | 1982-09-14 | Nippon Tokushu Noyaku Seizo Kk | 2-pyridyloxyacetanilide compound, its preparation and herbicide |
| US4544661A (en) * | 1983-09-23 | 1985-10-01 | Chevron Research Company | Fungicidal N-pyridyloxy alkyl amines |
| CA2822296A1 (en) | 2010-12-21 | 2012-06-28 | Bayer Cropscience Lp | Sandpaper mutants of bacillus and methods of their use to enhance plant growth, promote plant health and control diseases and pests |
| EP2755485A1 (en) | 2011-09-12 | 2014-07-23 | Bayer Cropscience LP | Methods of enhancing health and/or promoting growth of a plant and/or of improving fruit ripening |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4110104A (en) * | 1973-03-19 | 1978-08-29 | The Dow Chemical Company | Herbicidal use of aminohalopyridyloxy acids and derivatives thereof |
| IN139196B (ko) * | 1974-04-11 | 1976-05-22 | Dow Chemical Co | |
| CH625940A5 (en) * | 1975-08-25 | 1981-10-30 | Ciba Geigy Ag | A composition for regulating the growth of plants containing, as active ingredient, 3-pyridinol compounds |
| US4067725A (en) * | 1975-08-25 | 1978-01-10 | Ciba-Geigy Corporation | 3-Pyridyl-oxy-alkanecarboxylic acid amides |
-
1981
- 1981-01-28 JP JP56010110A patent/JPS57126473A/ja active Pending
-
1982
- 1982-01-15 GR GR67119A patent/GR75166B/el unknown
- 1982-01-18 DE DE8282100318T patent/DE3260023D1/de not_active Expired
- 1982-01-18 AT AT82100318T patent/ATE5720T1/de not_active IP Right Cessation
- 1982-01-18 EP EP82100318A patent/EP0057367B1/de not_active Expired
- 1982-01-19 AU AU79608/82A patent/AU7960882A/en not_active Abandoned
- 1982-01-19 PT PT74305A patent/PT74305B/pt unknown
- 1982-01-20 DD DD82236879A patent/DD219362A5/de unknown
- 1982-01-21 TR TR21412A patent/TR21412A/xx unknown
- 1982-01-21 US US06/341,379 patent/US4391629A/en not_active Expired - Fee Related
- 1982-01-25 PH PH26787A patent/PH17658A/en unknown
- 1982-01-25 IL IL64857A patent/IL64857A0/xx unknown
- 1982-01-27 KR KR1019820000332A patent/KR830009027A/ko unknown
- 1982-01-27 BR BR8200443A patent/BR8200443A/pt unknown
- 1982-01-27 PL PL1982234847A patent/PL129394B1/pl unknown
- 1982-01-27 DK DK37582A patent/DK37582A/da not_active Application Discontinuation
- 1982-01-27 ZA ZA82521A patent/ZA82521B/xx unknown
- 1982-01-27 ES ES509099A patent/ES8301922A1/es not_active Expired
- 1982-01-28 CS CS82601A patent/CS228914B2/cs unknown
Also Published As
| Publication number | Publication date |
|---|---|
| JPS57126473A (en) | 1982-08-06 |
| PT74305B (en) | 1983-07-06 |
| BR8200443A (pt) | 1982-11-30 |
| ATE5720T1 (de) | 1984-01-15 |
| AU7960882A (en) | 1982-08-05 |
| DD219362A5 (de) | 1985-03-06 |
| EP0057367B1 (de) | 1983-12-28 |
| EP0057367A1 (de) | 1982-08-11 |
| US4391629A (en) | 1983-07-05 |
| GR75166B (ko) | 1984-07-13 |
| TR21412A (tr) | 1984-05-29 |
| ES509099A0 (es) | 1983-01-01 |
| PL234847A1 (en) | 1983-03-14 |
| PL129394B1 (en) | 1984-05-31 |
| PH17658A (en) | 1984-10-25 |
| ES8301922A1 (es) | 1983-01-01 |
| IL64857A0 (en) | 1982-03-31 |
| ZA82521B (en) | 1982-12-29 |
| DK37582A (da) | 1982-07-29 |
| CS228914B2 (en) | 1984-05-14 |
| DE3260023D1 (en) | 1984-02-02 |
| PT74305A (en) | 1982-02-01 |
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