KR830003571A - 슈크로오스 에스테르를 함유하는 계면활성제의 제법 - Google Patents
슈크로오스 에스테르를 함유하는 계면활성제의 제법 Download PDFInfo
- Publication number
- KR830003571A KR830003571A KR1019800003743A KR800003743A KR830003571A KR 830003571 A KR830003571 A KR 830003571A KR 1019800003743 A KR1019800003743 A KR 1019800003743A KR 800003743 A KR800003743 A KR 800003743A KR 830003571 A KR830003571 A KR 830003571A
- Authority
- KR
- South Korea
- Prior art keywords
- starting
- sucrose
- soap
- mixture
- weight
- Prior art date
Links
- 229930006000 Sucrose Natural products 0.000 title claims description 10
- 239000005720 sucrose Substances 0.000 title claims description 10
- 239000004094 surface-active agent Substances 0.000 title claims 2
- -1 sucrose ester Chemical class 0.000 title description 4
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims description 6
- 239000000344 soap Substances 0.000 claims description 6
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims 4
- 230000007704 transition Effects 0.000 claims 3
- 239000003054 catalyst Substances 0.000 claims 2
- 235000014113 dietary fatty acids Nutrition 0.000 claims 2
- 230000032050 esterification Effects 0.000 claims 2
- 238000005886 esterification reaction Methods 0.000 claims 2
- 229930195729 fatty acid Natural products 0.000 claims 2
- 239000000194 fatty acid Substances 0.000 claims 2
- 150000004665 fatty acids Chemical class 0.000 claims 2
- 239000007787 solid Substances 0.000 claims 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical group [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims 1
- OGBUMNBNEWYMNJ-UHFFFAOYSA-N batilol Chemical class CCCCCCCCCCCCCCCCCCOCC(O)CO OGBUMNBNEWYMNJ-UHFFFAOYSA-N 0.000 claims 1
- 125000004432 carbon atom Chemical group C* 0.000 claims 1
- 150000005690 diesters Chemical class 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 229910052700 potassium Inorganic materials 0.000 claims 1
- 239000011591 potassium Substances 0.000 claims 1
- 239000002904 solvent Substances 0.000 claims 1
- 239000007858 starting material Substances 0.000 claims 1
- UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 claims 1
- 230000008018 melting Effects 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 150000003445 sucroses Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
- C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
- C07H13/04—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals attached to acyclic carbon atoms
- C07H13/06—Fatty acids
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S516/00—Colloid systems and wetting agents; subcombinations thereof; processes of
- Y10S516/01—Wetting, emulsifying, dispersing, or stabilizing agents
Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
제 1 도, 3 도, 5 도 및 7 도는 각각 기간에 대한 슈크로오스 에스테르 및 기타 반응 성분의 농도를 표시한 것이다.
제 2 도는 개시 비누 성분에 대한 슈크로오스 에스테르 수준이 20%에 도달하는 기간을 표시한 것이다.
제 4 도는 개시 비누 성분에 대한 슈크로오스 에스테르 수준을 표시한 것이다.
제 6 도는 개시 하이드록실 값에 대한 슈크로오스 에스테르 수준을 표시한 것이다.
제 8 도는 개시 슈크로오스 농도에 대한 반응성분을 표시한 것이다.
제 9 도는 개시 슈크로오스 농도에 대한 생성물의 융점을 표시한 것이다.
제10도는 개시 슈크로오스 농도에 대한 생성물의 HLB 값을 표시한 것이다.
Claims (1)
- 본문에 상술하고 도면에 도시한 바와같이, 출발 혼합물이, 출발 혼합물의 500 mg KOH/100g 보다 큰 하이드록실 값을 제공하기 위한 량으로 디-및/또는 모노-글리세리드를 함유하고, 최소한 비누의 50중량%가 칼륨 비누인 염기성 전이 에스테르화 촉매와 또한 지방산 비누의 최소한 10중량 %를 함유하며, 슈크로오스의 최소한 25%를 함유(비누 함량이 20중량% 이하일 때) 함을 특징으로 하는, 용매없이 대기압하에 110-140℃의 온도에서 고체의 미세한 슈크로오스를 포함하는 출발 물질을 최소한 8개 탄소원자를 갖는 지방산의 최소한 하나의 트리글리세리드 : 및 염기성 전이 에스테르화 촉매와 출발 혼합물을 반응시킴으로서 슈크로오스 모노-및 디-에스테르를 함유하는 계면활성제 혼합물을 제조하는 방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB43,762 | 1979-12-19 | ||
GB7943762 | 1979-12-19 | ||
GB14,370 | 1980-05-01 | ||
GB8014370 | 1980-05-01 |
Publications (1)
Publication Number | Publication Date |
---|---|
KR830003571A true KR830003571A (ko) | 1983-06-21 |
Family
ID=26273922
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019800003743A KR830003571A (ko) | 1979-12-19 | 1980-09-25 | 슈크로오스 에스테르를 함유하는 계면활성제의 제법 |
Country Status (19)
Country | Link |
---|---|
US (1) | US4298730A (ko) |
EP (1) | EP0031191B1 (ko) |
KR (1) | KR830003571A (ko) |
AR (1) | AR222567A1 (ko) |
AU (1) | AU534287B2 (ko) |
BR (1) | BR8005556A (ko) |
CA (1) | CA1153945A (ko) |
CU (1) | CU35315A (ko) |
DE (1) | DE3060918D1 (ko) |
DK (1) | DK370880A (ko) |
ES (1) | ES494692A0 (ko) |
GR (1) | GR69950B (ko) |
IE (1) | IE50028B1 (ko) |
IL (1) | IL60716A0 (ko) |
NO (1) | NO802549L (ko) |
NZ (1) | NZ194465A (ko) |
OA (1) | OA06636A (ko) |
PT (1) | PT71737B (ko) |
YU (1) | YU216380A (ko) |
Families Citing this family (34)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS6115893A (ja) * | 1984-06-29 | 1986-01-23 | Dai Ichi Kogyo Seiyaku Co Ltd | シヨ糖脂肪酸エステルの精製法 |
GB8514975D0 (en) * | 1985-06-13 | 1985-07-17 | Sempernova Plc | Compositions |
NL8601904A (nl) * | 1986-07-23 | 1988-02-16 | Unilever Nv | Werkwijze voor de bereiding van polyol-vetzuurpolyesters. |
GB8800087D0 (en) * | 1988-01-05 | 1988-02-10 | Unilever Plc | Process for synthesis of polyol fatty acid polyesters |
JPH0667955B2 (ja) * | 1989-05-09 | 1994-08-31 | 第一工業製薬株式会社 | 粉末状高hlbショ糖脂肪酸エステルの製造法 |
DK0550526T3 (da) * | 1990-09-11 | 1997-06-02 | Procter & Gamble | Polyolpolyestersyntese |
ATE117310T1 (de) | 1990-09-11 | 1995-02-15 | Procter & Gamble | Verfahren zum erhalten hochgradig veresterter polyolfettsäurepolyester mit verringertem gehalt an di-höheralkylketonen und beta-ketoestern. |
WO1992018591A2 (en) * | 1991-04-12 | 1992-10-29 | The Procter & Gamble Company | Process for improving oxidative stability of polyol fatty acid polyesters |
US5872245A (en) * | 1992-09-30 | 1999-02-16 | Optima Technologies Group | Continuous process for the synthesis of sucrose fatty acid esters |
US5681948A (en) * | 1995-03-06 | 1997-10-28 | Kraft Foods, Inc. | Two-stage method for preparing polyol fatty acid polyesters |
US5596085A (en) * | 1995-04-11 | 1997-01-21 | Kraft Foods, Inc. | Method for preparing polyol fatty acid polyesters by transesterification |
US5705147A (en) * | 1995-09-18 | 1998-01-06 | Stepan Company | Methods and compositions for conditioning skin and hair |
US5968566A (en) * | 1996-05-14 | 1999-10-19 | Mlp Operating Company | Refrigerated yeast-raised pizza dough |
US5767257A (en) * | 1996-07-19 | 1998-06-16 | The Procter & Gamble Company | Methods for producing polyol fatty acid polyesters using atmospheric or superatmospheric pressure |
US5945529A (en) * | 1996-07-19 | 1999-08-31 | The Procter & Gamble Company | Synthesis of polyol fatty acid polyesters using column with inert gas stripping |
CZ36499A3 (cs) * | 1996-08-08 | 1999-07-14 | The Procter & Gamble Company | Syntéza polyolových polyesterů |
US6121440A (en) * | 1998-01-29 | 2000-09-19 | The Procter & Gamble Company | Process for synthesis of polyol fatty acid polyesters |
DE69908104T2 (de) * | 1998-03-23 | 2004-04-01 | The Procter & Gamble Company, Cincinnati | Herstellung von hochveresterten polyol-fettsäurepolyestern |
US7098352B2 (en) * | 2001-11-16 | 2006-08-29 | Virtus Nutrition Llc | Calcium salt saponification of polyunsaturated oils |
US20030130348A1 (en) * | 2001-11-16 | 2003-07-10 | Strohmaier George K. | Polyunsaturated oil saponification |
MXPA06013990A (es) * | 2004-04-30 | 2007-08-14 | Virtus Nutrition Llc | Sintesis de sal de metal monovalente y divalente de acido graso polinsaturado. |
GB0423972D0 (en) * | 2004-10-28 | 2004-12-01 | Vincent Processes Ltd | Process for the production of esters of sugars and sugar derivatives |
GB0608512D0 (en) * | 2006-04-28 | 2006-06-07 | Vincent Processes Ltd | Process for the production of esters of sugars and sugar derivatives |
ES2564518T3 (es) | 2006-09-14 | 2016-03-23 | Bahram Memarzadeh | Monolaurato de sucralosa y monomiristato de sucralosa, formulaciones farmacéuticas, estuches de diagnóstico y métodos de tratamiento |
MX2009007100A (es) * | 2006-12-29 | 2009-07-09 | Sherwin Williams Co | Sistema de pretratamiento y tincion. |
CN102093438A (zh) * | 2010-11-22 | 2011-06-15 | 柳州爱格富食品科技股份有限公司 | 利用旋转薄膜酯交换连续反应器合成蔗糖多酯的工艺 |
CN102533454B (zh) * | 2011-12-31 | 2013-04-10 | 柳州高通食品化工有限公司 | 一种蔗糖酯的生产方法及其在调制油脂专用抗氧化剂中的应用 |
EP2819987B1 (en) | 2012-02-28 | 2020-12-23 | Petroliam Nasional Berhad | Lubricant composition of matter and methods of preparation |
CN104321302A (zh) | 2012-02-28 | 2015-01-28 | 马来西亚国家石油公司 | 用于聚氨酯应用的物质多元醇的组合物 |
SG11201405261TA (en) | 2012-02-28 | 2014-09-26 | Petroliam Nasional Berhad | Bio-polyols for bio-lubricant and bio-polymer and methods for the preparation thereof |
DK2820112T3 (en) | 2012-02-28 | 2017-09-11 | Petroliam Nasional Berhad | PROCEDURE FOR PREPARING POLYOLS AND APPLICATIONS THEREOF |
SG11201405265QA (en) | 2012-02-28 | 2014-09-26 | Petroliam Nasional Berhad | Method for the production of esters and uses thereof |
CN102850413A (zh) * | 2012-05-29 | 2013-01-02 | 常州大学 | 一种制备蔗糖脂肪酸酯的方法 |
MY169226A (en) | 2013-02-28 | 2019-03-19 | Petroliam Nasional Berhad | Preparation of biopolyol esters for lubricant application |
Family Cites Families (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2970962A (en) * | 1958-02-11 | 1961-02-07 | Sugar Res Foundation Inc | Novel detergent compositions |
DE1200276B (de) * | 1959-10-08 | 1965-09-09 | Bayer Ag | Verfahren zum Herstellen von Carbonsaeureestern nichtreduzierender Zucker |
NL145278B (nl) * | 1966-04-06 | 1975-03-17 | Nebraska State | Werkwijze ter uitvoering van een heresteringsreactie tussen een vloeibare polyhydrische alcohol en een hydrofobe ester van een vetzuur met lange keten. |
DE1643795A1 (de) * | 1967-08-04 | 1971-07-01 | Cassella Farbwerke Mainkur Ag | Verfahren zur Herstellung von Zuckerestern |
US3714144A (en) * | 1969-05-29 | 1973-01-30 | Us Agriculture | Process for the production of sucrose esters of fatty acids |
BE757846A (fr) * | 1969-10-23 | 1971-04-01 | Dai Ichi Kogyo Seiyaku Cy Ltd | Procede de synthese d'esters de saccharose d'acides gras |
GB1399927A (en) * | 1971-09-11 | 1975-07-02 | Dai Ichi Kogyo Seiyaku Co Ltd | Detergent compositions |
GB1399053A (en) * | 1973-03-16 | 1975-06-25 | Tate & Lyle Ltd | Process for the production of surface active agents comprising sucrose esters |
US3963699A (en) * | 1974-01-10 | 1976-06-15 | The Procter & Gamble Company | Synthesis of higher polyol fatty acid polyesters |
GB1499989A (en) * | 1974-10-17 | 1978-02-01 | Tate & Lyle Ltd | Production of a surface active material containing sucrose esters |
NO142306C (no) * | 1975-04-18 | 1980-07-30 | Tate & Lyle Ltd | Fremgangsmaate til rensing av et fast stoff i form av et omestringsprodukt frembrakt ved reaksjon mellom sukrose og minst ett fettsyretriglycerid |
-
1980
- 1980-07-24 IE IE1546/80A patent/IE50028B1/en unknown
- 1980-07-25 CA CA000356985A patent/CA1153945A/en not_active Expired
- 1980-07-28 NZ NZ194465A patent/NZ194465A/xx unknown
- 1980-07-31 US US06/174,277 patent/US4298730A/en not_active Expired - Lifetime
- 1980-07-31 IL IL60716A patent/IL60716A0/xx unknown
- 1980-08-01 AU AU60988/80A patent/AU534287B2/en not_active Ceased
- 1980-08-13 DE DE8080302785T patent/DE3060918D1/de not_active Expired
- 1980-08-13 EP EP80302785A patent/EP0031191B1/en not_active Expired
- 1980-08-15 AR AR282186A patent/AR222567A1/es active
- 1980-08-25 PT PT71737A patent/PT71737B/pt unknown
- 1980-08-29 YU YU02163/80A patent/YU216380A/xx unknown
- 1980-08-29 DK DK370880A patent/DK370880A/da not_active Application Discontinuation
- 1980-08-29 NO NO802549A patent/NO802549L/no unknown
- 1980-08-30 GR GR62774A patent/GR69950B/el unknown
- 1980-09-01 ES ES494692A patent/ES494692A0/es active Granted
- 1980-09-01 BR BR8005556A patent/BR8005556A/pt unknown
- 1980-09-05 CU CU8035315A patent/CU35315A/es unknown
- 1980-09-25 KR KR1019800003743A patent/KR830003571A/ko unknown
- 1980-10-07 OA OA57230A patent/OA06636A/xx unknown
Also Published As
Publication number | Publication date |
---|---|
NO802549L (no) | 1981-06-22 |
IE801546L (en) | 1981-06-19 |
US4298730A (en) | 1981-11-03 |
DE3060918D1 (en) | 1982-11-11 |
BR8005556A (pt) | 1981-06-23 |
DK370880A (da) | 1981-06-20 |
PT71737B (en) | 1981-06-15 |
YU216380A (en) | 1983-10-31 |
PT71737A (en) | 1980-09-01 |
IL60716A0 (en) | 1980-09-16 |
NZ194465A (en) | 1982-12-21 |
CA1153945A (en) | 1983-09-20 |
GR69950B (ko) | 1982-07-22 |
EP0031191B1 (en) | 1982-10-06 |
IE50028B1 (en) | 1986-02-05 |
AU6098880A (en) | 1981-06-25 |
OA06636A (fr) | 1981-08-31 |
CU35315A (en) | 1982-03-28 |
ES8106538A1 (es) | 1981-07-16 |
EP0031191A1 (en) | 1981-07-01 |
AR222567A1 (es) | 1981-05-29 |
AU534287B2 (en) | 1984-01-19 |
ES494692A0 (es) | 1981-07-16 |
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