KR830002686A - 아실화 나프틸아민 식물용 살균제의 제조방법 - Google Patents

아실화 나프틸아민 식물용 살균제의 제조방법

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KR830002686A
KR830002686A KR1019800001519A KR800001519A KR830002686A KR 830002686 A KR830002686 A KR 830002686A KR 1019800001519 A KR1019800001519 A KR 1019800001519A KR 800001519 A KR800001519 A KR 800001519A KR 830002686 A KR830002686 A KR 830002686A
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methylnaphthyl
alanine
alkyl
formula
ester
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KR850000337B1 (ko
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모제트 한스
에크하르트 볼프강
쿤즈 월터
후벨레 아돌프
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아놀드자일러
시바-가이기 에이지
언스트알테르
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    • C07D307/18—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having no double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D307/24—Carbon atoms having three bonds to hetero atoms with at the most one bond to halogen
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    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
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    • C07D307/56—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D307/68—Carbon atoms having three bonds to hetero atoms with at the most one bond to halogen

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Abstract

내용 없음

Description

아실화 나프틸아민 식물용 살균제의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (61)

  1. 구조식 Ⅰ의 아실화 나프틸아민
  3. 상기의 구조식에서 R2는 수소 또는 메틸 : R3는-CH(CH3)COOR
  4. 또는
  6. 이며 R4는 할로겐 또는 C1-C2-알콕시에 의해 치환되지 않은 C1-C4-알킬, C2-C4-알케닐, C3-C4-알키닐 또는 C3-C7-사이클로알킬이며, R5는 수소 또는 메틸임 : R6는 할로겐으로 치환되거나 치환되지 않은 2-퍼릴 또는 2-테트라히드로퍼릴이거나 β-(C1-C4)-알콕시 에틸 또는 CH2Z기인데, Z는 아래의 그룹중 하나이다. ㄱ)-X-R7ㄴ)-NH-N(R8)(R9), ㄷ)-OSO2R10, ㄹ)-O(CO)R11, ㅁ) 1,2-피라졸, ㅂ)1,2,4-트리아졸(1), 또는 이들의 염이나 금속염들, X는 산소 또는 황이고, R7은 C1-C2-알콕시로 치환된 C1-C6-알킬기, C3-C4-알케닐 또는 C3-C4-알키닐이고, R8은 수소 또는 C1-C3-알킬이며 R9은 C1-C3-알킬 또는 페닐이고, R10은 C1-C4알킬 또는 모노-, 디-(C1-C3)-알킬아민이고, R11은 C1-C2알콕시로 치환되거나 치환되지 않은 C1-C3-알킬임 : R3가-CH(CH3) C00R4일 경우, 치환분 R7은 C1-C6-알킬이 될 수도 있다.
  7. 청구범위 Ⅰ에 따르는 아실화 나프틸 아민. 여기에서 R2는 수소 또는 메틸,
  8. R3는-CH(CH3)COOR4또는
  10. R4는 C1-C2-알콕시로 치환되거나 치환되지 않은 C1-C3-알킬, 또는 C2-C4-알케닐, C3-C4-알키닐.
  11. R6는 수소 또는 메틸.
  12. R6는 2-퍼릴, 2-테트라히드로퍼릴, 또는 CH2Z이며 Z는 하기의 그룹중 하나임,
  13. ㄱ) -X-R7, X는 수소 또는 황,
  14. ㄴ) -NH-N(R8)(R9)
  15. ㄷ) -OSO2R10
  16. ㄹ) 1,2,4-트리아졸(1)과 염 또는 이들의 금속염들, R7은, R3가 락톤인 경우, 알릴 또는 프로파길, R3가 -CH(CH3)COOR4인 경우, 알릴, 프로파길 또는 C1-C3-알킬.
  17. R8과 R9은 각기 C1-C2-알킬,
  18. R10은 C1-C2-알킬 또는 모노메틸아민이다.
  19. 청구범위 1에 따르는 구조식 Ⅰ의 아실화 나프틸아민, 여기에서
  20. R2는 수소 또는 메틸,
  21. R3는 -CH(CH3)-COOR4또는
  23. R4는 C1-C3-알킬,
  24. R6는 2-퍼릴, 2-테트라히드로퍼릴 또는 CH2Z, Z는 R3가 -CH(CH3)COOR4인 경우
  25. ㄱ) -OR7, R7은 C1-C2-알킬,
  26. ㄴ) -OSO2R10R10,R10은 C1-C2-알킬 또는 모노메틸아민
  27. ㄷ) 1,2,4-트리아졸
  28. R3가 락톤인 경우 ㄴ) 또는 e)의 하나를 지닌다.
  29. 구조식 N-(2-프로핀-1-일옥시아세틸-N-(2-메틸나프틸)-N-(2-옥소-테트라히드로푸란-3-일)-아민, 또는
  30. N-(2-프로펜-1-일옥시아세틸)-N-(2-메틸 나프틸)-N-(2-옥소테트라 히드로 푸란-3-일)-아민중의 어떤 한가지 화합물.
  31. 구조식 N-(2-메틸나프틸)-N-메톡시아세틸-알라닌-2-메톡시에틸 에스테르, N-(2-메틸나프틸)-N-(이소프로폭시아세틸)-알라닌메틸 에스테르, N-(2-메틸나프틸)-N-메톡시아세틸-알라닌-2-이소프로필에스테르, N-(2,3-디메틸나프틸-N-메톡시아세틸-알라닌메틸에스테르, N-(2,3-디메틸나프틸)-N-(3-메톡시프로피오닐)-알라닌-메틸 에스테르중의 어떤 한가지 화합물.
  32. 구조식 N-(2-메틸나프틸)-N-메틸설포닐옥시아세틸-알라닌 메틸 에스테르, N-(2-메틸나프틸)-N-(N'-메틸설파모일옥시 아세틸)-알라닌-메틸 에스테르, N-(2-메틸나프틸)-N-메틸설포닐옥시아세틸-알라닌-이소프로필 에스테르, -(2,3-디메틸나프틸)-N-(N'-메틸설파모일 옥시아세틸)-N-(2-메틸나프틸)-N-(2-옥소테트라히드로 푸란-3-일)-아민, N-(N'-메틸설파모일옥시아세틸)-N-(2-메틸나프틸-N-(2-옥소 테트라히드로푸란-3-일)-아민, N-(2,3-디메틸나프틸-N-(N'메틸설파모일 옥시아세틸)-(2-옥소-테트라히드로푸란-3-일)-아민, N-(2,3-디메틸나프틸)-N-(메틸설포닐 옥시아세틸)-N-(2-옥소-테트라 히드로 푸란-3-일)아민 중의 어떤 한가지 화합물.
  33. 구조식 N-(2-메틸나프틸)-N-[1,2,4-트리아조릴 (1)-아세틸]-알라닌-메틸에스테르,
  34. N-(2-메틸나프틸)-N-[1,2,4-트리아조릴 (1)-아세틸]-알라닌-2-메톡시에틸 에스테르,
  35. N-(2-메톡시나프틸)-N-[1,2,4-트리아조릴 (1)-아세틸]-알라닌-2-이소프로필 에스테르,
  36. N-(2,3-디메틸나프틸)-N-[1,2,4-트리아조릴 (1)-아세틸]-알라닌 메틸 에스테르,
  37. N-(2-메틸나프틸)-N-(2-옥소-5-메틸-테트라히드로푸란-3-일(-N-[1,2,4-트리아조릴 (1)-아세틸-아민,
  38. N-(2,3-디메틸나프틸)-N-(2-옥소-테트라히드로푸란-3-일)-N-[1,2,4-트리아조릴 (1)-아세틸]-아민 중의 어떤 한가지 화합물.
  39. 구조식 N-(2-메틸나프틸)-N-(2-옥소-테트라히드로푸란-3-일)-N-테트라 히드로 푸란-3-일)-N[테트라 히드로 푸라노일 (2)]-아민,
  40. N-(2,3-디메틸나프틸)-N-(2-옥소-테트라 히드로 푸란-3-일)-N-[테트라 히드로 푸라노일(2)]-아민, -(2-메틸나프틸)-N-[테트라히드로푸라노일(2)]-알라닌-메틸 에스테르,
  41. N-(2-메틸나프틸 0)-N-[테트라히드로 푸라노일(2)]-알라닌-2-메톡시에틸 에스테르,
  42. N-(2-메틸나프틸)-N-[푸라노일(2)]-알라닌-2-메톡시-에틸 에스테르,
  43. N-(2-메틸나프틸)-N-[테트라히드로 푸라노일(2)]-알라닌-이소프로필 에스테르,
  44. N-(2,3-디메틸나프틸)-N-[푸라노일 (2)]-알라닌-메틸 에스테르,
  45. N-(2,3-디메틸나프틸)-N-[테트라히드로푸란 노일(2)]-알라닌-메틸 에스테르중의 어떤 한가지 화합물.
  46. 구조식 N-(2-메틸나프탈렌-N-(N'-2-펜닐히드라지노아세틸)-알라닌-메틸 에스테르,
  47. N-(2-메틸나프틸)-N-(N',N'-2-디메틸히드라지노아세틸)-알라닌메틸 에스테르,
  48. N-(2,3-디메틸나프틸)-N-(N',N'-2-디메틸 히드라지노아세틸)-알라닌메틸 에스테르 중의 어떤 한가지 화합물.
  49. 하기의 과정으로 구성된, 청구범위 1에 따라 구조식 Ⅰ의 아실화 나프틸아민을 생산하는 공정.
  50. 가. 구조식 Ⅲ의 카르복실 산을 지녔거나 할로겐 산 또는 이들의 산 무수물을 지닌 구조식 Ⅱ화합물을 아실화시킴.
  52. 나. 구조식 Ⅳ 또는 이들의 염을 구조식 Ⅴ Ⅵ 또는 Ⅶ 화합물과 반응시킴 :
  54. 다. 구조식 Ⅹ화합물을 구조식 XI, XⅡ, XⅢ 또는 XⅢa와 반응시킴
  56. 상기식에서 치환분 R2,R3,R6,R11,X는 구조식 Ⅰ에서 정의된 것과 동일하며, "Hal"은 염소 또는 브롬등 할로겐이고, "M"은 수소 또는 알카리 금속 양이온 또는 알카리에서 유래된 금속 양이온 이며, "Azole"은 1,2-피라졸 또는 1,2,4-트리아졸임.
  57. 최소한 한가지 활성 물질로서, 적절한 매개물 또는 계면-활성첨가제와 함께, 구조식 Ⅰ의 물질을 함유한 청구범위 1에 따른 조화물.
  58. 청구범위 2에서 9를 포괄한 어느 한가지에 따른 구조식Ⅰ의 활성물질을 함유한 청구범위 Ⅱ에 따른 조합물.
  59. 청구범위 1의 구조식Ⅰ의 세균에 활성인 화합물에 의해 보호를 받도록 처리된 위치에 적용시킨 식물의 세균 오염을 방지하거나 퇴치시키는 공정.
  60. 청구범위 2에서 9를 포괄한 어떠한 한가지에 따라 화합물을 사용한 청구범위 13에 따른 공정.
  61. ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019800001519A 1979-04-10 1980-04-10 아실화 나프틸아민의 제조방법 KR850000337B1 (ko)

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DE2948704A1 (de) * 1979-12-04 1981-06-11 Basf Ag, 6700 Ludwigshafen N-substituierte 2-methylnaphthylamide, verfahren zu ihrer herstellung und diese enthaltende fungizide
AU8314482A (en) * 1981-05-19 1982-11-25 Imperial Chemical Industries Plc 3-triazolyl(imidazolyl)-2,2 bis phenyl-propionamides
DE3126082A1 (de) * 1981-07-02 1983-01-20 Basf Ag, 6700 Ludwigshafen Glykoletheressigsaeurenaphthylamide, verfahren zu ihrer herstellung und diese enthaltende fungizide
DE3126083A1 (de) * 1981-07-02 1983-01-20 Basf Ag, 6700 Ludwigshafen N-substituierte 2-methylnaphthylamide, verfahren zu ihrer herstellung und diese enthaltende fungizide
DE3135239A1 (de) * 1981-09-05 1983-03-17 Basf Ag, 6700 Ludwigshafen N-substituierte brenztraubensaeureamide, verfahren zu ihrer herstellung und diese enthaltende fungizide
DE3135670A1 (de) * 1981-09-09 1983-03-24 Basf Ag, 6700 Ludwigshafen Oxalamide, verfahren zu ihrer herstellung und diese enthaltende fungizide
DE3144951A1 (de) * 1981-11-12 1983-05-19 Basf Ag, 6700 Ludwigshafen Isoxazol-carbonsaeure-amide, ihre herstellung und ihre verwendung als fungizide
CA2024971A1 (en) * 1989-09-14 1991-03-15 Atsuo Hazato Naphthalene derivative and preparation method thereof
DE10029077A1 (de) * 2000-06-13 2001-12-20 Bayer Ag Thiazolylsubstituierte Heterocyclen
CN106243053B (zh) * 2016-09-12 2018-09-28 三峡大学 一种三唑酰胺酮类杀菌剂，合成方法及其应用

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DE1003221B (de) * 1953-06-24 1957-02-28 Cassella Farbwerke Mainkur Ag Verfahren zur Herstellung neuer anaesthetisch wirkender Aminocarbonsaeureamide
OA04979A (fr) * 1974-04-09 1980-11-30 Ciba Geigy Nouveaux dérivés de l'aniline utiles comme agents microbicides et leur procédé de préparation.
US4151299A (en) * 1974-04-09 1979-04-24 Ciba-Geigy Corporation Certain aniline derivatives as microbicidal agents
IL52928A0 (en) * 1976-09-17 1977-11-30 Ciba Geigy Ag New aniline derivatives their preparation and pesticidal compositions containing them
US4147792A (en) * 1977-02-04 1979-04-03 Ciba-Geigy Corporation Fungicidal compositions
GB1601453A (en) * 1977-05-05 1981-10-28 Ici Ltd Triazole and imidazole derivatives useful in agriculture
DE2724785A1 (de) * 1977-05-27 1978-12-14 Schering Ag Furancarbonsaeureanilide, fungizide mittel enthaltend diese verbindungen sowie verfahren zu ihrer herstellung
DE2845454A1 (de) * 1977-11-01 1979-05-10 Chevron Res 3-(n-acyl-n-arylamino)- gamma -butyrolactone und - gamma -butyrothiolactone sowie fungizide mittel
US4310463A (en) * 1979-02-22 1982-01-12 Chevron Research 3-(N-Arylamino)-gamma-butyrolactones, butyrolactams and thiobutyrolactones are intermediates for compounds having fungicidal activity
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MX160628A (es) 1990-03-29
DK160296C (da) 1991-07-29
EP0018510B1 (de) 1983-12-21
BG35461A3 (en) 1984-04-15
IL59787A (en) 1983-03-31
CA1152081A (en) 1983-08-16
DE3065932D1 (en) 1984-01-26
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GR68192B (ko) 1981-11-10
HU188127B (en) 1986-03-28
US4916157A (en) 1990-04-10
NZ193371A (en) 1982-12-21
MY8700202A (en) 1987-12-31
AU5726180A (en) 1980-10-16
DK160296B (da) 1991-02-25
DK152380A (da) 1980-10-11
IE800708L (en) 1980-10-10
JPH0234939B2 (ko) 1990-08-07
DD151403A5 (de) 1981-10-21
AR225761A1 (es) 1982-04-30
IE49669B1 (en) 1985-11-13
EP0018510A1 (de) 1980-11-12
EG14292A (en) 1983-09-30
CS219274B2 (en) 1983-03-25
JPS55143943A (en) 1980-11-10
ATE5653T1 (de) 1984-01-15
KR850000338B1 (ko) 1985-03-21
ZA802106B (en) 1981-04-29
MX6018E (es) 1984-09-24
PL223324A1 (ko) 1981-02-13
IL59787A0 (en) 1980-06-30
AU532779B2 (en) 1983-10-13
KR850000337B1 (ko) 1985-03-21
OA06510A (fr) 1981-07-31
PL122677B1 (en) 1982-08-31
US5128371A (en) 1992-07-07
PT71075A (en) 1980-05-01

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