KR20220065183A - Composition for hair treatment comprising Hordeum vulgare L. extract - Google Patents

Abstract

The present invention relates to a hair treatment composition containing a white glutinous barley extract, and more specifically, to a hair treatment composition which contains vegetable extracts in harmony with white glutinous barley extract to make hair shine, flexible, and elastic and have an excellent hair protection function by making hairstyle last long and reducing the appearance of thinning hair. The hair treatment composition, according to the present invention, effectively treats thin, frizzy, and weak hair which has been physically and chemically damaged as a result of excessive hair cosmetic procedures such as perm, hair dryer, and hair dyeing, thereby making the hair shine, flexible and elastic, and proving an excellent hair protection function by making hairstyle last long and reducing the appearance of thinning hair.

Description

Hair treatment composition comprising white glutinous rice barley extract {Composition for hair treatment comprising Hordeum vulgare L. extract}

The present invention relates to a hair treatment composition comprising a white glutinous rice barley extract, and more particularly, to a hair treatment composition comprising a plant extract in harmony with a white glutinous rice barley extract to provide shine, flexibility and elasticity to the hair, and to improve hair style. It relates to a hair treatment composition having an excellent hair protection function by improving the durability and symptoms of hair thinning.

In general, as a product that changes the shape of hair, there is a composition for perm divided into a first agent reducing agent and a second agent neutralizing agent.

Depending on the method of treatment, they are called permanent waving agents and straight perming agents. Generally, thioglycolic acid or its salts, cysteine or its salts are used as the main ingredient in the first reducing agent, and these reduce and break the cysteine bond in the hair, where hydrogen peroxide Waves and straights are formed by oxidative recombination by treatment with a second neutralizing agent using water or sodium bromate as a main component. Waves and straight styles formed in this way show excellent durability, such as lasting more than 3 months, but there is a strong odor due to the main ingredients used during the procedure, and the residual odor remains after the procedure. The disadvantage is that it causes serious chemical damage to the hair due to the chemical reaction. In addition, there is a inconvenience of using the first and second agents sequentially.

Therefore, research to solve the above problems is continuously being conducted, and as a result of these studies, various hair cosmetics are specialized and subdivided, and products having various functions and effects have been proposed.

As such a technique, Korean Patent Publication No. 2013-0134505 discloses a composition for improving damaged hair and protecting hair containing supercritical carbon dioxide kelp/wheat extract. This technology uses supercritical or subcritical liquefied carbon dioxide as the main solvent for extraction, but contains as a raw material any one or a mixture of two or more selected from seaweed or its processed or by-products, crustaceans or their processed or by-products, vegetables or their processed or by-products. and rice bran or its processed product or by-product, wheat germ or its processed product or by-product, rice bran or its processed product or by-product, rice bran or its processed product or by-product, or a mixture of two or more selected from rice bran or its processed product or by-product as an auxiliary material.

In addition, in the Republic of Korea Patent Publication No. 2013-0081003, a composition for hair treatment applied to or sprayed on the hair in order to prevent damage and supply nutrition to the hair and scalp before perming or dyeing treatment or after perming or dyeing treatment, , arginine, hyaluronic acid, licorice extract, vitamin C, collagen, keratin, cell membrane complex (Cell Membrane Complex) and a composition for hair treatment comprising purified water is disclosed.

In addition, Korean Patent Registration No. 10-1476955 discloses a technology for manufacturing a hair treatment by mixing a fermented liquid obtained by fermenting general tea leaves and mugwort, plant extracts, emulsifiers, and natural preservatives.

However, these technologies are products for hair care treatment that use natural substances rather than synthetic raw materials as raw materials, and although these products are judged to have some effect on hair protection, etc. There is a demand for a product that can maintain shiny and soft hair for a long time.

Korea Registration No. 10-1970503 (April 15, 2019) Korean Publication No. 10-2008-0047102 (May 28, 2008)

As a result of the present inventor's intensive research to develop functional substances for various natural products based on long experience with natural products, the hair treatment composition prepared using the white glutinous rice barley extract has no side effects, as will be described later. When applied to hair, compared to conventional hair treatment products, it gives the hair gloss, flexibility and elasticity, and improves the continuity of the hair style and the symptoms of hair thinning. reached

Therefore, it is an object of the present invention to effectively treat thin, brittle, and powerless hair that has been physically and chemically damaged as a result of excessive hair cosmetic procedures such as perms, hair dryers, and hair dyeing to improve the shine, flexibility and elasticity of the hair. An object of the present invention is to provide a hair treatment composition having an excellent hair protection function by improving the durability of the hair style and the symptoms of hair thinning.

The above object of the present invention can be achieved by a hair treatment composition comprising a solvent extract of white glutinous rice barley as a main component.

The hair treatment composition according to the present invention effectively treats thin, brittle, and powerless hair that has been physically and chemically damaged as a result of excessive hair cosmetic procedures such as perms, hair dryers, and hair dyes to improve hair shine, flexibility and It has excellent hair protection function by giving elasticity and improving the continuity of hair style and hair thinning symptoms.

1 is a manufacturing process diagram of a hair treatment composition of the present invention.

The present invention, in one aspect,

It provides a hair treatment composition comprising a solvent extract of white glutinous rice barley as a main component.

The present invention, in a further aspect,

Based on 100 parts by weight of the total composition, 15-25 parts by weight of white glutinous rice barley extract, 5-15 parts by weight of seaweed extract, 3-7 parts by weight of mugwort extract, 3-7 parts by weight of Seoritae extract, 3-7 parts by weight of licorice extract , provides a hair treatment composition comprising 3 to 7 parts by weight of ginseng extract, 3 to 7 parts by weight of green tea extract, 3 to 7 parts by weight of vegetable oil and the remainder of purified water.

The present invention, in another further aspect,

The extract provides a hair treatment composition, characterized in that at least one extract selected from the group consisting of water, an organic solvent, and mixtures thereof.

The present invention, in another further aspect,

The composition provides a hair treatment composition, characterized in that it is used as a shampoo, colorant or hair care agent.

The present invention harmoniously blends white glutinous rice barley extract and harmonious plant extract to give shine, flexibility and elasticity to physically and chemically damaged hair that has become thin, brittle, and powerless, and maintains hair style and improves hair There is a technical feature in providing a hair treatment composition having an excellent hair protection function by improving the symptoms of thinning, and the composition ratio of the composition according to the present invention is the result of a long study in consideration of the effective dose and side effects of each component. It is set by , and if it is out of the range of the ratio, it may not exhibit a desirable synergistic effect with other components, and there is a fear that the functionality and effect may be deteriorated.

As used herein, "hair treatment composition" refers to a composition that can effectively protect hair and improve damaged hair, and such a composition can be used alone, as well as shampoos, conditioners, hair dyes, and other well-known compositions. It can also be applied to various hair care formulations.

Hereinafter, each individual component is demonstrated.

In the hair treatment composition of the present invention, white glutinous rice barley ( Hordeum vulgare L. ), which is the main ingredient, is a variety bred by artificial crossbreeding between Bangsa No. 6 and the Cheolseong variety Yojaza and Mochi in 1981. As a cultivar that was decided as an encouraging variety and named white barley, the characteristic characteristic of white barley is that it has green leaves, and the leaf width and leaf length are similar to those of the standard variety, and the stem color and thickness are similar to those of the standard variety. The stalks are green and short in length, and the ears are hexagonal like glutinous barley, smuggled and upright.

The disaster-resistance characteristics of white barley are very strong cold resistance and wear resistance, and it is stronger than barley barley for streaks and has stronger resistance to barley escort disease than barley barley. The quality characteristics of white rice barley are similar to those of sticky rice barley, and the protein content is similar to that of sticky rice barley, and the grain whiteness is slightly higher than that of sticky rice barley, but it is very high compared to regular rice barley.

The white glutinous rice barley extract is adopted as the main ingredient to protect the hair, and it gives elasticity to damaged hair and shows the main function of improving the symptoms of hair thinning, and 15 to 25 parts by weight based on 100 parts by weight of the total composition. It may be desirable to be included, and if it is out of this, it is difficult to harmonize with other ingredients, and there is a fear that the functionality may be reduced.

Seaweed is an annual seaweed belonging to the Carpus family of brown algae. It contains inorganic and physiologically active ingredients such as calcium, potassium, iron, and iodine. In particular, mucilage and polysaccharides are effective in adsorbing and excreting heavy metals in food contaminated with pesticides. Arginic acid, an important component of brown algae cell membrane, is a hybrid polymer of D-mannuronic acid and L-glucuronic acid.

The seaweed is in harmony with the white glutinous rice barley extract and is a component that prevents hair damage, strengthens hair, and helps prevent hair loss. It may be preferable to include 5 to 15 parts by weight based on 100 parts by weight of the total composition. there is.

Mugwort is one of the perennial plants belonging to the Asteraceae family. In addition to mugwort, mugwort (A montana), wormwood (A lavandulaefolia), and mugwort (A rubripes) are commonly called mugwort. You can feel the spring by boiling and eating young shoots that appear in early spring, or making and eating rice cakes. Mugwort is also called medicinal mugwort. The stems and leaves are harvested before and after Dano and dried in the shade. It is called yakae (藥艾) and is used for abdominal pain, vomiting, and hemostasis. also do Dried leaves are called aeyeop (艾葉), and the juice of the leaves is sometimes applied to minor wounds. It grows on sunny roadsides, grasslands, mountains and fields throughout Korea.

Seoritae is also called black bean, and it has been handed down as a medicinal bean in folklore since ancient times. Seoritae, like soybeans, contains isoflavones such as genistein and daizein, which have antioxidant effects by removing harmful reactive oxygen species, and cancer cells are attacked by the immune system. It is known to exhibit anticancer action against breast, rectal and prostate cancer by inhibiting the production of stress proteins such as HSP (heat shook protein) and GRPs (glucose-related proten), which help to survive It has been reported that daizein suppresses the rapid rise in blood alcohol concentration after drinking by delaying the rate of alcohol excretion from the stomach.

In addition, there are reports that the soya saponins of Seoritae are closely related to antioxidant properties, serum cholesterol lowering, selective toxicity to cancer cells, and immune effects. There is also a report that the darker the black color compared to soybeans, the stronger the antioxidant effect.

Licorice is a perennial herb in the legume family, and it has a woody, vine-like underground stem and long, deep-rooted roots. The parts used are the three-year-old root and the underground stem, and the weakness is moderate and the taste is sweet. In addition, licorice is widely used as medicine, tobacco, and food. It has antibacterial, antiviral, bile promotion, antipyretic, antitussive, muscle relief, liver protection and anticancer action, anti-allergic, antibacterial, anti-inflammatory, anti-convulsant, soothing, anti-allergic, antibacterial, anti-viral, anti-inflammatory, anti-inflammatory, etc. , hepatitis, liver and kidney cirrhosis, menstrual pain, Addison's disease (adrenal insufficiency), eczema and herpes simplex, cholesterol, trichomoniasis infection, drug or food poisoning, fatigue, fever, heart palpitations, etc. Of course, it is one of the most used herbs because it is often used for flavoring when preparing other medicines.

Ginseng ( Panax ginseng CA Meyer ) is a plant belonging to the genus Ginseng, and the extract extracted from ginseng is known to have various medical effects, including immunity, anticancer, antioxidant, and antidiabetic activity. These effects are mainly ginseng saponin. It is caused by triterpenoid glucoside called ginsenoside. Ginsenoside is a specially named saponin component of ginseng among various saponins present in plants. It has been reported to have anti-diabetic, anti-stress, respiratory disease improvement, digestive system improvement, blood sugar lowering, immunity enhancement, antioxidant and anti-aging effects.

In the composition of the present invention, ginseng can be used without limitation on its type and year, and either dried or undried ginseng can be used. In addition, ginseng can be used without limitation on the site, and in particular, it may be preferable to use the root of ginseng.

Green tea (Green-tea, Camellia teaceac ) is a non-alcoholic favorite beverage that contains caffeine along with coffee, cocoa, and black tea. Green tea is known to have the function of supplying vitamins and minerals nutrients and satisfying the taste and aroma, and in 100 mg of whole dried green tea leaves, 13 mg of carotene, 654 mg of vitamin E, and It has been reported that 106 mg of dietary fiber is contained, and minerals such as Ca, Fe and K are also abundantly contained. Among these green teas, the main component of the astringent taste is catechin, a polyphenol component. Depending on the derivative, catechin is epicatechin, epigallocatechin, epicatechin gallate, and epigallo. It can be classified as catechin gallate (Epigallocatechin gallate) and the like. The content of catechin reaches about 8-20% of that of dried green tea, and it is soluble in water and eluted into water when boiled with water. The bitter taste of green tea is mainly due to caffeine, which is known to have arousal, diuretic, and fatigue recovery action. It accounts for about half and contains about 20 kinds of amino acids.

In addition, green tea used in the present invention can be used without limitation on its kind and cultivation days, and both dried or undried green tea can be used. In addition, in the present invention, green tea can be used without limitation on the site, and in particular, green tea leaves can be preferably used.

As the vegetable oil, camellia oil, olive oil, eucalyptus oil and tea tree oil may be preferably used.

The vegetable oil is obtained by pressing leaves, fruits, or fruits, or by adding an extraction solvent to the raw material in a weight ratio of 1:2 to 1:20, putting it in a reflux condenser, heating and distilling for 2-3 hours, and then cooling After filtration, the cooled extract is filtered for 5 to 7 hours, and an extract prepared individually can be preferably used.

Alternatively, the vegetable oil may be used by extracting leaves, fruits, or fruits by a conventional rectification method. For example, after selecting seeds, leaves, or pulp well, washing and drying, and pressing at 70 to 150° C., the milked oil may be collected through filtration and oil collection processes.

The mugwort extract, seoritae extract, licorice extract, ginseng extract, green tea extract, and vegetable oil are in harmony with the main ingredient, white glutinous rice barley, by forming the composition as described above, and are physically and chemically damaged to become thin, crumbly and weak. It is possible to provide a hair treatment composition having an excellent hair protection function by imparting gloss, flexibility and elasticity to the hair, and improving the continuity of the hair style and the symptoms of thinning hair.

In addition, the hair treatment composition according to the present invention includes, in addition to the above substances, a hair treatment solution, shampoo, dye, hair tonic, which can give a synergistic effect on hair function, preferably within a range that does not impair the hair functional effect. It may further include known active ingredients used in hair nourishing lotion, scalp treatment, hair conditioner, hair lotion and hair care formulation.

In addition, the hair treatment composition according to the present invention further contains a moisturizing agent, emulsion, suspension, dispersing agent, thickener, emollient, ultraviolet absorber, preservative, bactericide, antioxidant, pH adjuster, organic and inorganic pigment, fragrance, cooling agent or limiting agent. may include

The blending amount of the component can be easily selected by those skilled in the art within the range that does not impair the purpose and effect of the present invention, and the blending amount may be 0.01 to 5 parts by weight, specifically 0.01 to 3 parts by weight, based on the total weight of the composition.

1 is a manufacturing process diagram of a hair treatment composition of the present invention. The white glutinous rice barley, seaweed extract, mugwort extract, seoritae extract, licorice extract, ginseng extract and green tea extract, the above-mentioned raw plant extracts can be extracted as follows.

First, in a1) pretreatment step, raw materials are washed with clean water such as purified water to remove foreign substances, and then washed to remove foreign substances and pre-treated. The washing operation is preferably hand-washed individually, and it is also possible to wash by spraying washing water, washing in flowing purified water, or washing the material by immersing it in purified water and then repeatedly taking it out.

a2) Then, put the vegetable material, which has been pretreated, such as removing foreign substances, into the extractor, add 10 to 25 times the extraction solvent based on the weight, and then put it in an autoclaved pot at a temperature of 65 to 125° C. for 2 to 24 hours, preferably It is extracted by heating it for 5 hours. Alternatively, extraction can also be carried out by brewing for 6 to 72 hours at a pressure of 0.5 to 0.6 atmosphere and a medium temperature of 70 ° C to 95 ° C.

The extraction solvent may be extracted using water, an organic solvent, or a mixed solvent thereof, and specifically, water, methylol, ethanol, propanol, butanol, glycerin, acetone, ethyl acetate, hexane, 1,3-butylene glycol Alternatively, extraction may be performed using a mixed solvent thereof.

When extracting, you can mix and extract all the ingredients you want to extract, or you can use the optimally mixed ingredients extracted individually.

Then, in the filtration step a3), for example, using a filtration membrane, paper filter paper, non-woven fabric or cotton, etc. to filter out solid foreign substances and particles, or ultrafiltration, freezing filtration, centrifugal separation, etc. It can be filtered. In addition, filtration may be performed by first filtering using gauze, and then performing secondary filtering using Whatman paper.

On the other hand, the vegetable oil is separately prepared by the compression method or the rectification method as described above.

a4) In the dilution step, the extracted plants as above are in a undiluted state and mixed with other ingredients at a certain ratio, and then diluted or appropriately diluted ones are blended at a certain ratio.

a5) In the additive mixing step, the extracted plant extract and the extract and separately treated vegetable oil are mixed in an appropriate ratio as described above to prepare a blending solution, and then, if necessary, by adding additives such as a dispersing agent It can be applied to one bar of product.

a6) In the packaging step, the manufactured hair treatment products are packaged and stored in a certain unit.

a7) In addition, if necessary, the packaged product may be sterilized for long-term storage and distribution.

As the step of sterilizing the packaged product, various sterilization methods can be selected and carried out depending on the dosage form and packaging type, but conventional UV sterilization, retort sterilization or steam sterilization methods are used, and these conditions are finely modified as necessary. It is more preferable to perform

<Example>

Hereinafter, the present invention will be described in more detail through examples. These examples are only for illustrating the present invention in more detail, and it will be apparent to those of ordinary skill in the art that the scope of the present invention is not limited by these examples according to the gist of the present invention. .

Preparation Example 1: Preparation of plant extract

Each commercially purchased material (white glutinous rice barley, seaweed giraffe, mugwort, seoritae, licorice, ginseng, green tea) is pretreated to remove foreign substances, put the material into the extractor, add 20 times water by weight, and then add 0.6 After extraction by brewing at atmospheric pressure and medium temperature of 75° C. for 8 hours, foreign substances were filtered from the obtained extract to obtain individual extracts.

Preparation Example 2: Preparation of vegetable oil

After adding purified water 20 times by weight to the leaves and stems of the tea tree tree, put it in a reflux condenser, and after heating and distilling for 3 hours to cool, the cooled extract is filtered for 6 hours to obtain tea tree oil, A camellia oil undiluted solution was prepared by pressing the camellia fruit.

Examples 1 to 5 and Comparative Examples: Preparation of spray formulations

After diluting the extracts of Example 1 10-fold, as shown in Table 1 below, after mixing with additives based on weight (g), a small amount of dispersant was added, and 200 ml of each was dispensed into a spray container to prepare a spray formulation. .

item Example 1 Example 2 Example 3 Example 4 Example 5 comparative example White glutinous rice barley extract 15 20 20 20 25 Barley Extract 25 seaweed extract 10 5 7 12 15 - mugwort extract 7 5 5 3 3 10 Seoritae Extract 5 3 7 3 3 10 Licorice Extract 5 7 3 4 3 10 Ginseng Extract 5 6 3 3 7 - green tea extract 3 5 5 7 3 - Vegetable oil (tea tree: camellia oil = 1:1 weight ratio) 5 3 3.5 3 7 - Additive (cetyl alcohol) - One 1.5 - - - Dispersant (carboxymethyl cellulose) a very small amount - a very small amount - - - Purified water 45 45 45 45 34 45 Sum 100 100 100 100 100 100

Experimental Example 1: Satisfaction evaluation

After use of the hair treatment products of Examples 1 to 5 and Comparative Example 1, hair elasticity, gloss, flexibility, thickness improvement, hair style durability, and overall satisfaction were evaluated through a panel of 50 experts. The evaluation scale of the results for the degree of improvement in each item is a 7-point scale (7 points: very good, 6 points: good, 5 points: slightly good, 4 points: moderate, 3 points: slightly bad, 2 points: poor, 1 point: very bad), which was aggregated as an average and shown in Table 2 below.

item Example 1 Example 2 Example 3 Example 4 Example 5 Comparative Example 1 elasticity of hair 6.21±0.75 6.25±0.38 6.37±0.25 6.01±0.71 6.07±0.72 4.37±0.56 hair shine 6.46±0.25 6.22±0.52 6.35±0.71 6.21±0.35 6.25±0.43 4.68±0.34 hair flexibility 6.52±0.36 6.47±0.16 6.36±0.25 5.97±0.03 6.23±0.26 4.42±0.39 improvement of hair thickness 6.43±0.11 6.53±0.55 6.42±0.65 6.23±0.59 6.33±0.74 4.07±0.56 hair style continuity 6.31±0.56 6.42±0.76 6.31±0.11 6.23±0.52 6.28±0.58 4.72±0.78 overall satisfaction 6.37±0.61 6.41±0.48 6.36±0.52 6.25±0.56 6.26±0.33 4.35±0.26

From the results in Table 2, the spray products according to Examples 1 to 5 of the present invention have increased hair elasticity, gloss, and flexibility, improved style durability and hair thinning symptoms, and improved style durability compared to the comparative example products. and overall satisfaction was also confirmed to be excellent.

As described above, preferred embodiments of the present invention have been described, but those of ordinary skill in the art to which the present invention pertains can understand that the present invention may be embodied in other specific forms without changing the technical spirit or essential features. There will be. Therefore, it should be understood that the embodiment described above is illustrative in all respects and not restrictive.

Claims (4)

A hair treatment composition comprising a solvent extract of white glutinous rice barley as a main component. The method according to claim 1,
Based on 100 parts by weight of the total composition, 15-25 parts by weight of white glutinous rice barley extract, 5-15 parts by weight of seaweed extract, 3-7 parts by weight of mugwort extract, 3-7 parts by weight of Seoritae extract, 3-7 parts by weight of licorice extract , 3-7 parts by weight of ginseng extract, 3-7 parts by weight of green tea extract, 3-7 parts by weight of vegetable oil, and a hair treatment composition comprising the remaining amount of purified water. The method according to claim 1,
The extract is a hair treatment composition, characterized in that at least one extract selected from the group consisting of water, an organic solvent, and mixtures thereof. The method according to claim 1,
The composition is a hair treatment composition, characterized in that used as a shampoo, dye or hair care formulation.

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