KR20220014119A - Pimple care cosmetic composition of containing jade powder and purified water using jade powder, and manufacturing method thereof - Google Patents

Abstract

The present invention relates to a cosmetic composition having an effect of alleviating acne containing jade powder and jade purified water, and a method for manufacturing the same. The method comprise the following steps: (a) preparing jade powder and jade purified water; (b) with respect to 100 parts by weight of purified water, mixing 0.1 to 3 parts by weight of jade powder, 5 to 30 parts by weight of jade purified water, and 0.1 to 0.5 part by weight of a fragrance to manufacture a crude cosmetic material; (c) storing the crude cosmetic material at a low temperature of 5 to 10℃ for 60 to 90 days, so that there is an effect of mass-producing the cosmetic composition having the effect of alleviating acne using mineral jade powder harmless to the human body and having a skin soothing effect, and jade purified water without skin troubles.

Description

A cosmetic composition having an acne improvement effect containing jade powder and okjeong water, and a manufacturing method thereof {Pimple care cosmetic composition of containing jade powder and purified water using jade powder, and manufacturing method thereof}

The present invention relates to a cosmetic composition having an acne-improving effect containing jade powder and jade water, and a method for preparing the same.

Korean Patent Laid-Open Patent No. 10-2017-0099762 (published date: September 1, 2017, title of invention: composition for improving acne comprising black ginger extract) contains black ginger (kaempferia parviflora) extract as an active ingredient, but Disclosed is a cosmetic composition for improving or preventing acne, characterized in that it has antibacterial activity against Onibacterium acnes or Staphylococcus aureus.

This prior art contains black ginger extract having excellent antibacterial activity against acne bacteria Propionibacterium acnes and Staphylococcus aureus as an active ingredient. Because of this, there was a disadvantage that could cause trouble on sensitive skin.

In addition, Republic of Korea Patent No. 0803941 (registration date: February 11, 2008, title of invention: cosmetic composition containing jade powder) is a cross-linked silicone polymer as a main material, cyclomethicone, non-henoxy dimethicone , Stearoxydimethicone, Lauryldimethicone Polyolloy alone or a mixture of silicones and water emulsified silicone emulsion as a main component, a cosmetic composition containing a surface-treated jade powder containing the cosmetic composition is disclosed.

In this prior art, the cosmetic composition has excellent moisturizing effect and skin roughness relieving effect, and improves brightness and saturation to brighten skin color. , it claims that it has the effect of improving product quality and reliability by improving adhesion and preventing powder agglomeration as well as providing sebum control effect, but the disadvantage is that it is difficult to mass-produce because the manufacturing method of jade powder is not clear. there was.

An object of the present invention, which was created to solve the above problems, is to provide a cosmetic composition having an acne improvement effect using jade powder of a mineral component that is harmless to the human body and has a skin soothing effect and okjeong water without skin troubles, and a method for manufacturing the same there is

This object of the present invention, (a) preparing jade powder and jade water; (b) with respect to 100 parts by weight of purified water, 0.1 to 3 parts by weight of jade powder, 5 to 30 parts by weight of okjeongsu, and 0.1 to 0.5 parts by weight of fragrance to prepare a rough cosmetic by mixing; (c) it can be achieved by a cosmetic composition manufacturing method having an acne improvement effect containing jade powder and okjeong water comprising the step of storing the raw cosmetic at 5 to 10 ° C. at a low temperature for 60 to 90 days.

Preferably, the jade powder of step (a) of the present invention, (A) remove impurities by heating 0.1 to 10 mm diameter jade in a furnace of 180 to 230 ° C. for 5 to 6 hours and then furnace cooling step of; (B) directly burning a flame of 1,150 to 1,250° C. for 1 to 5 minutes on the surface of the jade; (C) With respect to 100 parts by weight of Geumgangsa (金剛砂), 50 to 75 parts by weight of the jade are mixed, and then, using a planetary ball mill, the jade is pulverized to 30 to 50㎛ or less, and then the rough jade powder is selected using a mesh screen. step of; (D) with respect to 100 parts by weight of the raw jade powder, 30 parts by weight of light oil and 5 to 5 parts by weight of paint thinner are mixed and ignited, and then after 10 to 13 hours, washing and drying the raw jade powder 1 to 5 times; ; (E) consists of a step of repeatedly inputting the dried rough jade powder into a heating roller press to finally produce jade powder of 10 μm or less, and the okjeong water of step (a) is, with respect to 100 parts by weight of purified water, a diameter of 10 15-20 parts by weight of ~150 mm nephrite beads are mixed, heated at 80 ~ 95 ℃ for 24 ~ 26 hours, cooled to 20 ~ 25 ℃, then 0.1 ~ 0.3 parts by weight of rose oil, 0.1 ~ 3 parts by weight of citric acid and vitamin C It is characterized in that it is prepared by further adding 0.1 to 1.5 parts by weight.

Preferably, the fragrance of step (b) of the present invention is frankincense essence oil, bergamot essence oil, sweet orange essence oil, lavender essence oil, neroli essence oil, green mandarin essence oil, clary sage essence oil, ylang ylang It is characterized in that at least one of an essence oil, Roman chamomile essence oil, chrysage essence oil, marjoram essence oil, and Swiss basil essence oil is mixed.

Preferably, the method further comprises step (d) between step (b) and step (c) of the present invention, wherein step (d) is 0.5 to 1.0 weight of fermented horseradish extract based on 100 parts by weight of Okjeong water. It consists of adding more parts by weight, 0.5 to 1.0 parts by weight of soothing fermented extract, and 0.5 to 1.0 parts by weight of fermented Wonchuri extract, wherein the fermented wasabi extract is 100 to 150 parts by weight of sugar and 10 to 15 parts by weight of licorice, based on 100 parts by weight of wasabi. It is prepared by filling parts by weight in an airtight container, fermenting for 6 to 9 months, and then centrifuging to separate the supernatant, and the fermented extract is 100 to 150 parts by weight of sugar, 10 to 15 parts by weight of brewed vinegar, based on 100 parts by weight of sedum gugun. Part and 10-15 parts by weight of licorice are filled in an airtight container, fermented for 6-9 months, and then centrifuged to separate supernatant water, and the fermented wonky root extract contains 10-15 parts by weight of sugar, and It is characterized in that it is prepared by filling 10 to 15 parts by weight of licorice in an airtight container, fermenting it for 6 to 9 months, and then centrifuging to separate the supernatant.

In addition, another object of the present invention can be achieved by a cosmetic composition having an acne improvement effect containing jade powder and jade water produced by any one of the above methods.

As described above, the present invention has the effect of mass-producing a cosmetic composition having an acne improvement effect using jade powder of mineral components that is harmless to the human body and has a skin soothing effect and jade water without skin troubles.

Hereinafter, it will be described with reference to the embodiment of the present invention.

1. Making Jade Powder

Jade powder as a cosmetic raw material is known to improve transparency, spreadability, and adhesion when manufacturing cosmetics, as mentioned in Patent Registration No. 0803941 above. In addition, in a paper on 'Effect of jade powder on cytotoxicity and oxidative stress induced by heavy metals' of Daebong LS of Korea [2018, IFSCC presentation in Munich, Germany], Chuncheon white jade was used Experiment contents and results showing that 99% of the tenants are crushed to 15㎛ or less and managed to a size that does not feel a foreign body feeling on the skin, but hydrophobic particles are completed using silicone surface treatment technology, which helps to purify the skin and relieve stress from external stimuli. is disclosed.

However, the invention of Registered Patent No. 0803941 has the disadvantage that mass production is difficult because the manufacturing method of the jade powder is not clear, and the technology of Daebong LS is a technology that goes against the trend of reducing or not using silicone as a cosmetic raw material. .

(A) Selection of raw materials

The raw material of jade in this embodiment uses a mixture of nephrite (軟玉) and corundum (Corundum).

Here, nephrite is mined from the white jade mine in Wolgok-ri, Dong-myeon, Chuncheon-si, Gangwon-do, and corundum is a mineral produced in hexagonal or columnar crystals, with a hardness of 9 and specific gravity of 3.9-4, making it the second hardest after diamond. In particular, corundum is colorless and transparent when pure without impurities, but depending on the type or amount of impurity elements, red (ruby), blue (sapphire), yellow (oriental topaz), green (oriental emerald), purple (oriental amethyst) , blackish brown, etc., and the name of the gem is given accordingly.

(B) Processing raw material

1. After heating jade with a diameter of 0.1 to 10 mm in a furnace at 180 to 230°C for 5 to 6 hours, it is cooled in the furnace to remove impurities. Here, the impurities are wood-based or oil components that are extinguished by high heat.

2. Directly irradiate the surface of the jade with a flame of 1,150 ~ 1,250℃ for 1 ~ 5 minutes. Here, the flame is provided by using a torch using butane gas or a mixed gas of acetylene and oxygen, and is intended to remove metal impurities such as lead, copper, zinc, etc. that are buried on the surface of nephrite and corundum.

3. With respect to 100 parts by weight of Geumgangsa (金剛砂), 50 to 75 parts by weight of jade are mixed, and then the jade is pulverized to 30-50 μm or less using a planetary ball mill, and then rough jade using a mesh screen. Select the powder. Here, Kumgangsa is provided to disperse heat generated during the ball milling process and to facilitate pulverization, and the sieve number (Sieve No.) of the mesh screen is #200. In addition, since Geumgangsa is not pulverized to less than 100㎛ during the ball milling process, rough jade powder can be selected using a mesh screen.

In addition, the jade of this embodiment is preferably nephrite mined in Chuncheon, and puts out in advance that 3 to 7 parts by weight of corundum may be mixed with 100 parts by weight of nephrite.

4. With respect to 100 parts by weight of the rough jade powder, 30 parts by weight of light oil and 5 to 5 parts by weight of paint thinner are mixed and ignited. After 10 to 13 hours, the rough jade powder is washed 1 to 5 times and dried. . Here, the reason why the rough jade powder is mixed with light oil and paint thinner to ignite is to induce fine cracks in the powder due to high heat.

5. The dried rough jade powder is repeatedly put into a heating roller press to finally produce jade powder of 10 μm or less. Here, the pressure and working temperature of the heating roller press are 5 ~ 100 MPa and 250 ~ 280 ℃.

2. Making Okjeong Water

Ock purified water is mixed with 15 to 20 parts by weight of nephrite beads with a diameter of 10 to 150 mm with respect to 100 parts by weight of purified water, heated at 80 to 95 ° C for 24 to 26 hours, cooled to 20 to 25 ° C, and then rose oil 0.1 to 0.3 weight It is prepared by adding more parts. Here, rose oil is used as a fragrance used in general lotion or cosmetics.

In addition, 0.1 to 3 parts by weight of citric acid may be further added with respect to 100 parts by weight of okjeongsu.

In addition, 0.1 to 1.5 parts by weight of vitamin C may be further added based on 100 parts by weight of okjeongsu.

3. Preparation of a primer cosmetic composition

The rough cosmetic composition is prepared by mixing 0.1 to 3 parts by weight of jade powder, 5 to 30 parts by weight of okjeongsu, and 0.1 to 0.5 parts by weight of fragrance based on 100 parts by weight of purified water.

Here, the fragrance is frankincense essence oil, bergamot essence oil, sweet orange essence oil, lavender essence oil, neroli essence oil, green mandarin essence oil, clary sage essence oil, ylang ylang essence oil, Roman chamomile essence oil, clisage essence. It is a mixture of at least one of oil, marjoram essential oil, and swwi basil essential oil.

4. Mixing fermented wild greens extract

This embodiment may be prepared by further adding 0.5 to 1.0 parts by weight of fermented horseradish extract, 0.5 to 1.0 parts by weight of soothing fermented extract, and 0.5 to 1.0 parts by weight of fermented Wonchuri extract with respect to 100 parts by weight of Okjeongsu.

Here, it has been reported that the fermented wild greens extracts of this example all use domestic wild greens that can be consumed for food, and have good effects on gynecological diseases and contain a large amount of anticancer components.

Watercress is excellent for relieving hangover and restoring liver function, and in China's 'Shinnongbonchogyeong', it is written that it prevents fatty liver. In addition, wasabi is effective for cirrhosis, diabetes, high blood pressure, loss of energy, frigidity, peritonitis, fever, eye irritation, headache, detoxification, and postpartum hemorrhage. ', the effect of preventing arteriosclerosis and relieving constipation is described.

Fermented wasabi extract is prepared by filling 100 to 150 parts by weight of sugar and 10 to 15 parts by weight of licorice in an airtight container based on 100 parts by weight of wasabi, fermenting for 6 to 9 months, and then centrifuging to separate the supernatant.

As a soothing perennial bulbous plant in the family Liliaceae, 'Donguibogam' acts on the spleen and kidneys to aid digestion, and the efficacy is described as being good for Tosagwak eggs. In addition, it is effective in soothing gastrointestinal diseases, menstrual irregularities, and nerve stabilization, and it is reported to contain a large amount of antipruritic performance while preventing heart disease by improving the flow of coronary arteries into Allium together with garlic.

For the soothing fermented extract, 100 to 150 parts by weight of sugar, 10 to 15 parts by weight of brewed vinegar, and 10 to 15 parts by weight of licorice, based on 100 parts by weight of Dalai Gugun, are filled in an airtight container, fermented for 6 to 9 months, and then centrifuged to obtain supernatant water. manufactured separately. Here, only soothing bulbs are used, and the reason for adding brewed vinegar during fermentation is to facilitate the extraction of beta-carotene, the main component of soothing.

Wonchuli is also called Hwoncho, Mangwoocho, Geumchimchae, and Hwanghwachae, and is known to have medicinal effects on pulmonary tuberculosis, tumors, ulcers, and jaundice. In addition, the root of Wonchuri is known to be good for gynecological diseases such as stones, dropsy, insomnia, irregular menstruation, lobster, constipation, etc.

Fermented Wonchul extract is prepared by filling 10-15 parts by weight of sugar and 10-15 parts by weight of licorice in an airtight container with respect to 100 parts by weight of Wonchul root, fermenting for 6-9 months, and then centrifuging to separate the supernatant. Here, the reason for using only Wonchul root is that important pharmacological components are concentrated in the root, such as menstrual irregularities and lobster in this example, and the reason for using as little as 10 to 15 parts by weight of sugar is that Wonchuri itself contains 4.4% of sugar. Because it contains a lot of sugar, it is not necessary.

5. Preparing the final cosmetic composition

The final cosmetic composition is prepared by storing the initial cosmetic composition at 5 to 10° C. at a low temperature for 60 to 90 days.

4. Making cosmetics (cream formulation)

This cosmetic composition is described by limiting it to manufacturing general cosmetics of a cream formulation as shown in Table 1 below, but it is not limited thereto, and it is possible to transform it into a spray formulation, a liquid formulation, etc., as well as soap, shampoo, rinse, It should be noted in advance that it can be widely applied to detergents, etc.

Here, the components of No. 1 to No. 9 are the composition of a general cosmetic of a cream formulation as described above, and the unit is weight %, and the units of jade powder and okjeongsu are parts by weight with respect to 100 parts by weight of the cosmetic of Comparative Example 1. In addition, component 10 is a cosmetic composition prepared according to this example.

Referring to Table 1, women in their teens and 20s with acne on the face were asked to use the creams of Comparative Examples and Examples 3 times a day for 3 months, and then a questionnaire was conducted on skin moisturizing, skin soothing effect and satisfaction. As a result, it was confirmed that the skin moisturizing and skin soothing effects were high in all of the Examples, unlike the Comparative Examples, which are cosmetic products of a general cream formulation, thereby improving acne.

Although the present invention as described above is limited to one embodiment, it is clear that all embodiments modified based on the technical idea of the present invention are not limited thereto and fall within the scope of the present invention.

Claims (4)

(a) preparing jade powder and jade water;
(b) with respect to 100 parts by weight of purified water, 0.1 to 3 parts by weight of jade powder, 5 to 30 parts by weight of okjeongsu, and 0.1 to 0.5 parts by weight of fragrance to prepare a rough cosmetic by mixing;
(c) the step of storing the raw cosmetic at a low temperature of 5 to 10 ℃ for 60 to 90 days,
The jade powder of step (a) is,
(A) removing impurities by heating the jade having a diameter of 0.1 to 10 mm in a furnace at 180 to 230° C. for 5 to 6 hours and then furnace cooling;
(B) directly burning a flame of 1,150 to 1,250° C. for 1 to 5 minutes on the surface of the jade;
(C) With respect to 100 parts by weight of Geumgangsa (金剛砂), 50 to 75 parts by weight of the jade are mixed, and then the jade is pulverized to 30-50 μm or less using a planetary ball mill, and then the rough jade powder is selected using a mesh screen. step of;
(D) with respect to 100 parts by weight of the raw jade powder, 30 parts by weight of light oil and 5 to 5 parts by weight of paint thinner are mixed and ignited, and then after 10 to 13 hours, washing and drying the raw jade powder 1 to 5 times; ;
(E) repeatedly inputting the dried rough jade powder into a heating roller press to finally produce jade powder of 10 μm or less,
The okjeong water of step (a) is,
With respect to 100 parts by weight of purified water, 15 to 20 parts by weight of nephrite beads with a diameter of 10 to 150 mm are mixed, heated at 80 to 95 ℃ for 24 to 26 hours, cooled to 20 to 25 ℃, and then 0.1 to 0.3 parts by weight of rose oil; A method for producing a cosmetic composition having an acne improvement effect containing jade powder and okjeongsu, characterized in that it is prepared by further adding 0.1 to 3 parts by weight of citric acid and 0.1 to 1.5 parts by weight of vitamin C.
The method of claim 1,
The fragrance of step (b) is frankincense essence oil, bergamot essence oil, sweet orange essence oil, lavender essence oil, neroli essence oil, green mandarin essence oil, clary sage essence oil, ylang ylang essence oil, Roman chamomile essence oil , A method for producing a cosmetic composition having an acne improvement effect containing jade powder and okjeongsu, characterized in that at least one of clisage essence oil, marjoram essence oil, and swiwe basil essence oil is mixed.
The method of claim 1,
Further comprising step (d) between step (b) and step (c),
The step (d) is based on 100 parts by weight of the okjeong water, 0.5 to 1.0 parts by weight of the fermented horseradish extract, 0.5 to 1.0 parts by weight of the soothing fermented extract, and 0.5 to 1.0 parts by weight of the fermented Wonchuri extract.
The fermented wasabi extract is prepared by filling 100 to 150 parts by weight of sugar and 10 to 15 parts by weight of licorice in an airtight container with respect to 100 parts by weight of wasabi, fermenting for 6 to 9 months, and then centrifuging to separate the supernatant,
The soothing fermented extract is filled in an airtight container with 100 to 150 parts by weight of sugar, 10 to 15 parts by weight of brewed vinegar and 10 to 15 parts by weight of licorice, based on 100 parts by weight of soothing gugun, fermented for 6 to 9 months, and then centrifuged to supernatant water. is prepared by separating
The fermented Wonchu-ri extract is prepared by separating the supernatant by centrifuging after fermenting for 6-9 months by filling 10-15 parts by weight of sugar and 10-15 parts by weight of licorice in an airtight container with respect to 100 parts by weight of the Wonki root. A method for manufacturing a cosmetic composition having an acne improvement effect containing jade powder and okjeongsu.
A cosmetic composition having an acne improvement effect containing jade powder and jade water produced by any one of claims 1 to 3.