KR20210135041A - Manufacturing method of emulsion water using minerals and pine needles - Google Patents

Abstract

The present invention relates to a method of preparing emulsion water using minerals and pine needles. More particularly, the method comprises: a mineral extract preparing step of preparing a mineral extract; a pine needle extract preparing step of preparing a pine needle extract; a raw material mixing step of mixing 150 to 250 parts by weight of the pine needle extract prepared through the pine needle extract preparing step with 100 parts by weight of the mineral extract prepared through the mineral extract preparing step; a cypress extract mixing step of mixing a cypress extract with the mixture prepared through the raw material mixing step; and a precipitation aging step of precipitating and aging the mixture containing the cypress extract through the cypress extract mixing step. The emulsion water produced through the above process contains the mineral extract and the pine needle extract, and thus has excellent skin whitening, skin moisturizing, skin soothing, skin regenerating and wrinkle alleviating effects, has excellent anti-inflammatory and antibacterial performances, and exhibits excellent preservability without using separate preservatives.

Description

Manufacturing method of lotion using minerals and pine needles {MANUFACTURING METHOD OF EMULSION WATER USING MINERALS AND PINE NEEDLES}

The present invention relates to a method for manufacturing a lotion using minerals and pine needles, and more particularly, it has excellent skin whitening, skin moisturizing, skin soothing, skin regeneration and wrinkle improvement effects, and excellent anti-inflammatory and antibacterial performance, It relates to a method for manufacturing a lotion using a mineral and pine needles that provides a lotion exhibiting excellent preservability without adding a preservative.

Most of the conventional lotions contain moisturizing agents such as polyhydric alcohols, proteins, amino acids and mucopolysaccharides, solubilizers such as polyoxyethylene oleyl ether, thickeners, preservatives, and fragrances.

Polyhydric alcohols, which are conventionally used as moisturizers in lotions made of the above ingredients, are cheap and have an excellent moisturizing effect, but when used in excess, they can cause skin problems by promoting percutaneous absorption, and are natural moisturizing ingredients. Amino acids, proteins, mucopolysaccharides, etc. do not have a very large moisturizing effect, and there is a risk that the product may be spoiled by microorganisms.

In addition, in order to improve the moisturizing effect of skin care cosmetics containing lotion, a method is known that can reduce the sticky feeling even under high humidity by adding protease peptone together with a moisturizing agent, which is less toxic to the skin and is cosmetic. In order to obtain the effect, an astringent lotion for facial cleansing containing extracts of apricot seed, green tea, gold and placenta has been disclosed, and a lotion containing herbal ingredients of sangbaekpi, oyster root, ginseng, and licorice has been commercialized, but the products listed above are not products. It contains stabilizers such as preservatives and preservatives for the stability of the skin, and not only adversely affects the skin, but also has a problem in that it is not excellent in moisturizing properties.

On the other hand, pine (Pinus densiflora Seibold et Zuccarini) is an evergreen coniferous tree that is wild in the mountains of Korea, and mainly red pine (land pine) that grows a lot in inland areas, pine pine, Rigida pine, gom pine, white pine. etc.

Pine needles, the leaves of pine trees, have been used for medicinal or health food in oriental medicine or folk remedies since ancient times. According to Donguibogam, pine needles are known to be effective in treating gastrointestinal diseases, stroke, hypertension, neuralgia, and asthma.

These pharmacological actions of pine needles are functional substances such as essential oil, protein, vitamin A, vitamin C, vitamin K, vitamin P (rutin), phosphorus, iron, enzymes, tannins, chlorophyll, bitter substances, and flavonoids contained in pine needles. made by In particular, vitamin P (rutin) has an excellent effect in promoting blood circulation and preventing high blood pressure and aging. In addition, the volatile essential oil of pine needles plays a role in relieving fatigue during forest bathing.

Korean Patent Registration No. 10-1180412 (2012.08.31) Korean Patent Registration No. 10-1571792 (2015.11.19)

An object of the present invention is a mineral and To provide a method for manufacturing a lotion using pine needles.

An object of the present invention is a mineral extract manufacturing step for preparing a mineral extract, a pine needle extract manufacturing step for preparing a pine needle extract, 100 parts by weight of a mineral extract prepared through the mineral extract manufacturing step pine needles prepared through the pine needle extract manufacturing step The raw material mixing step of mixing 150 to 250 parts by weight of the extract, the cypress extract mixing step of mixing the cypress extract with the mixture prepared through the raw material mixing step, and the cypress extract mixing step Precipitating and aging the mixture containing the cypress extract It is achieved by providing a method for manufacturing a lotion using minerals and pine needles, characterized in that it consists of a precipitation aging step.

According to a preferred feature of the present invention, in the step of preparing the pine needle extract, the pine needles are washed and dried, dried in the shade for 24 to 48 hours, crushed to a size of 50 to 200 mesh, dissolved in water, and then by steam distillation. It is supposed to be made in the process of removing moisture.

According to a more preferred feature of the present invention, between the cypress extract mixing step and the precipitation ripening step, 10 to 30 parts by weight of an additive is further contained relative to 100 parts by weight of the mixture prepared through the cypress extract mixing step, and the additive is ginuari It shall consist of at least one selected from the group consisting of extract, sacha inchi oil, amethyst extract, mineral salt extract, pearl extract, aloes root extract, and ginseng extract.

According to a more preferred feature of the present invention, the additive is a ginseng extract, and the ginseng extract is prepared by mixing ginseng powder with an extraction solvent, cooling and filtering.

According to an even more preferred feature of the present invention, the ginseng extract is prepared by mixing 100 parts by weight of ginseng powder with 800 to 1200 parts by weight of an extraction solvent, cooling it for 2 to 4 days, and then filtering it.

According to an even more preferred feature of the present invention, the mineral extract manufacturing step is a mineral mixing step of mixing the mineral powder, the mineral mixture prepared through the mineral mixing step is mixed with purified water and 5 to 7 at a temperature of 45 to 80 ° C. A stirring step of stirring for a period of time, a mineral supernatant recovery step of recovering supernatant water by leaving the mineral mixture stirred through the stirring step, an aging step of aging the supernatant recovered through the mineral supernatant recovery step, and aging through the aging step It shall consist of a filtration step of filtering the supernatant.

According to an even more preferred feature of the present invention, between the cypress extract mixing step and the precipitation aging step, a basalt treatment step of mixing 3 to 5 parts by weight of basalt powder to 100 parts by weight of the mixture prepared through the cypress extract mixing step is further performed. to be in progress.

According to an even more preferred feature of the present invention, the step of mixing the cypress extract is made by mixing 5 to 10 parts by weight of the cypress extract in 100 parts by weight of the mixture prepared through the raw material mixing step.

According to an even more preferred feature of the present invention, the cypress extract is made by mixing 100 to 400 parts by weight of purified water with 100 parts by weight of cypress leaves and putting it in an essential oil extraction pressure machine at a temperature of 105 to 150° C. for 3 to 9 hours. .

According to an even more preferred feature of the present invention, the cypress extract is made by mixing 250 parts by weight of purified water with 100 parts by weight of cypress leaf and putting it in an essential oil extraction pressure machine at a temperature of 130° C. for 6 hours.

The method for manufacturing a lotion using minerals and pine needles according to the present invention is excellent in skin whitening, skin moisturizing, skin soothing, skin regeneration and wrinkle improvement effects, and excellent anti-inflammatory and antibacterial performance, and excellent without adding a separate preservative. It has an excellent effect of providing a lotion showing preservation, and in particular, it has the advantage of providing effects such as controlling sebum secretion, shrinking pores, moisturizing the skin, cleaning the skin and improving blood circulation by far-infrared radiation by the basalt treatment step.

1 is a flowchart illustrating a method for manufacturing a lotion using minerals and pine needles according to an embodiment of the present invention.
2 is a flowchart illustrating a method for manufacturing a lotion using minerals and pine needles according to another embodiment of the present invention.
3 is a flowchart illustrating a method for manufacturing a lotion using minerals and pine needles according to another embodiment of the present invention.
4 is a flowchart illustrating a method for manufacturing a lotion using minerals and pine needles according to another embodiment of the present invention.

Hereinafter, a preferred embodiment of the present invention and the physical properties of each component will be described in detail, which is intended to describe in detail enough that a person of ordinary skill in the art to which the present invention pertains can easily carry out the invention, This does not mean that the technical spirit and scope of the present invention is limited.

The method for manufacturing a lotion using minerals and pine needles according to the present invention includes a mineral extract manufacturing step (S101) of preparing a mineral extract, a pine needle extract manufacturing step (S101-1) of preparing a pine needle extract, and the mineral extract manufacturing step (S101) A raw material mixing step (S103) of mixing 150 to 250 parts by weight of the pine needle extract prepared through the pine needle extract manufacturing step (S101-1) to 100 parts by weight of the mineral extract prepared through the raw material mixing step (S103), the raw material mixing step (S103) It consists of a precipitation aging step (S107) of precipitating and aging the mixture containing the cypress extract through the cypress extract mixing step (S105) and the cypress extract mixing step (S105).

The mineral extract manufacturing step (S101) is a step of extracting the active ingredient contained in the mineral powder mixture consisting of loess, illite, zeolite, elvan, bentonite, diatomaceous earth, jade, germanium and limestone, and mixing the mineral powders listed above. Mineral mixing step, a stirring step of mixing and stirring the mineral mixture prepared through the mineral mixing step with purified water, a mineral phase recovery step of recovering supernatant by leaving the stirred mineral mixture through the stirring step, the mineral phase recovery recovery It consists of an aging step of aging the supernatant water recovered through the step and a filtration step of filtering the supernatant water aged through the aging step.

The mineral mixing step is a step of mixing ocher, illite, zeolite, elvan, bentonite, diatomaceous earth, calcium, jade, germanium and limestone, 100 parts by weight of loess, 80 to 90 parts by weight of illite, 40 to 60 parts by weight of zeolite , 25 to 35 parts by weight of elvan, 10 to 15 parts by weight of bentonite, 8 to 15 parts by weight of diatomaceous earth, 30 to 80 parts by weight of jade, 20 to 40 parts by weight of germanium and 20 to 40 parts by weight of limestone. It is preferred that the listed minerals exhibit a particle size of 300 to 350 mesh.

If the particle size of the mineral mixture is less than 300 mesh, the extraction efficiency of the active ingredient contained in the mineral mixture is reduced, and when the particle size of the mineral mixture exceeds 350 mesh, the mineral mixture is easily scattered because the particle size is too small. This contaminates the workplace and lowers the efficiency of the lotion manufacturing process.

The loess has an excellent effect of controlling humidity, and when the humidity is high, it absorbs moisture, and when the humidity is low, it discharges moisture to maintain a constant humidity. In addition, ocher contains enzymes that inhibit the growth of bacteria and fungi, and because it has an excellent detoxification action, it removes toxic substances from the human body, and improves skin elasticity due to its excellent self-cleaning ability and waste removal effect. , which relieves inflammation in the skin.

In addition, the Illite delivers negative ions and heat deep into the skin and maintains smooth and elastic skin, and discharges skin wastes and maintains healthy skin through the interaction of negative ions and far-infrared radiation. to maintain moist skin with skin cell regeneration, excellent whitening effect, and removal of sebum and acne from the skin Not only does it play a role in purifying the lotion by causing precipitation, but it also emits 93% of far-infrared rays at a temperature of 40℃, has a bacteriostatic action against bacteria and mold, and adsorbs various heavy metals, organic substances and toxic substances remaining on the skin. and decomposition, and has good elasticity and does not form lumps, thereby suppressing the occurrence of sediment in the lotion.

In addition, the zeolite is dissolved in hydrochloric acid and often becomes a glue, but a few types are insoluble in hydrochloric acid. The main types include bantamite, fisheye, chabazite, soda zeolite, hewlandite, stilbite, lomontite, and inesite.

It is produced in hollows or fissures of basic igneous rocks such as basalt and pyroclastic tuff, and sometimes exists as a secondary mineral in granite and gneiss.

The elvan stone is ^{composed of more than 30,000 multi-layered porous materials per 1 cm 2} , exhibits metal adsorption and harmful substances adsorption effects in the body, and contains more than 40 minerals. The necessary minerals are eluted. In addition, it promotes metabolism, adjusts water to be slightly alkaline when mixed with water, emits far-infrared rays and shows heat effect, and the far-infrared rays emitted from elvan can relieve headaches, dizziness, chronic fatigue, insomnia, cold hands and feet, and abnormal sweating. shows an improvement effect.

The bentonite contains about 66 kinds of natural minerals, and has excellent cation exchange ability to exchange cations with sebum and wastes in the skin to clean the skin.

In addition, the bentonite is made of components such as silicon, aluminum, magnesium and iron, and in particular, silicon, the main component of bentonite, shows excellent adsorption power and penetrates deep into pores. .

In addition, the diatomaceous earth contains various micronutrients from phytoplankton and deep-sea mineral components to promote skin health, and because it is light and has good absorption, it can be used in various technical fields. It is adsorbed to purify the skin, and it can be applied to atopy or sensitive skin. In addition, the jade contains a large amount of minerals (M, Ca, Fe, Al) essential for the human body, especially magnesium (38%). Silver works to promote mutual resonance with the components that make up the cells of our body, and the bioenergy from jade is used to maintain health through tissue revitalization, blood circulation improvement, weak alkalinity of blood, and excretion of harmful substances from the body. effective.

In addition, the germanium absolutely needs nutrients and oxygen for human cells to continuously and repeatedly perform metabolism, and when oxygen is insufficient, chronic carbon monoxide poisoning, anemia, vascular disorders, heart disorders, hypotension, cellular aging, mental disorders, etc. disease occurs. According to recent experiments by medical scientists, since germanium acts as an oxygen catalyst that helps the efficient use of oxygen, it supplies oxygen to the skin and shows a skin improvement effect. plays a role in making

The stirring step is a step of mixing and stirring the mineral mixture prepared through the mineral mixing step with purified water, 100 parts by weight of purified water and 3 to 5 parts by weight of the mineral mixture are mixed in a stirrer equipped with a heating device, and the speed of 100 to 200 rpm And it is preferably made by stirring at a temperature of 45 to 80 ℃ for 5 to 7 hours.

When the temperature of the stirring step (S101-3) shows 45 to 80° C., the amount of far-infrared rays emitted from illite, etc. contained in the mineral mixture increases to have a bacteriostatic action against bacteria or fungi, so a separate preservative is added It is possible to manufacture a lotion with excellent preservation properties without doing so.

In addition, if the stirring time is less than 5 hours, the mineral mixture is not evenly mixed in the purified water, the elution amount of the active ingredient contained in the mineral mixture is reduced, and when the stirring time exceeds 7 hours, most of the active ingredients contained in the mineral mixture are eluted It is undesirable because the stirring process is continuously carried out even though it is possible.

The mineral supernatant recovery step is a step of separating and recovering supernatant water using a device such as a pump, after allowing the mineral mixture stirred through the stirring step to stand for 18 to 24 hours to precipitate solids. At this time, the recovered supernatant is in a state in which the solid content is removed, and the active ingredient of the mineral is eluted.

The aging step is a step of aging the supernatant water recovered through the mineral supernatant recovery step at a temperature of 50 to 80° C. for 48 to 70 hours. Since it is fused and stabilized after the active ingredients are mixed evenly, it is prepared with supernatant water showing uniform efficacy.

The filtration step is a step of filtering the supernatant water aged through the aging step using one or more filters selected from the group consisting of a sediment filter, a fra carbon filter, a hollow fiber membrane filter, a post carbon filter, and a reverse osmosis filter. Mention filter, plastic carbon filter, hollow fiber membrane filter, post carbon filter and reverse osmosis filter may be used alone, but it is preferable to remove foreign substances contained in the supernatant by sequentially applying the filters listed above.

The pine needle extract manufacturing step (S101-1) is a step of preparing a pine needle extract, after washing and drying red pine pine needles, which are raw materials, dried in the shade for 24 to 48 hours, crushed to a size of 50 to 200 mesh, and , after dissolving in water to remove moisture by steam distillation, the steam distillation is preferably performed at 95° C. or higher for 3 to 5 hours. When the distillation temperature and time are insufficient, the active ingredients of pine needles, such as karen, limonene and terpinolene, are not sufficiently eluted into water.

The resulting residue is concentrated and separated under reduced pressure, and the resultant residue is sufficiently dissolved in water, and then water is removed by steam redstillation again. It is preferable that the steam re-distillation is performed at 95° C. or higher for about 8 hours. Here too, if the distillation temperature and time are insufficient, the active ingredient contained in the pine needles is not sufficiently eluted into the water, and if it is boiled too much, the water evaporates too much, which is not preferable. The eluted liquid of the residue containing the active ingredient is the state in which water has been evaporated. The component from which the water is evaporated is aged again for about 15 to 30 days in a drying chamber at room temperature. As a result, a liquid composition of an organic component having little moisture was obtained. In this case, as the drying agent used for drying, anhydrous magnesium sulfate, anhydrous calcium sulfate, or anhydrous silica gel widely used in the art is used, and anhydrous magnesium sulfate is most preferable.

Karen, limonene, and terpinolene, which are major components of the pine needle extract, all have chemical formulas of C ₁₀ H ₁₆ and molecular weights of 136.24. First, as a major component of pine needles, Karen, also called delta-3-carene, is a double-ringed single terpene that exists as a natural component of turpentine. Karen is insoluble in water but soluble in fats and oils. It has a density of 0.867 (20°C) and a boiling point of 168-169°C.

Limonene is a type of hydrocarbon belonging to the terpenes class, and is also called 1,8-p-mentadiene. The boiling point is 178℃, the melting point is -96.9℃, and the specific gravity is 0.8411 (20℃).

Terpinolene is a single ring monoterpene that is soluble in alcohol and ether glycol, but insoluble in water. The boiling point is 184°C.

The pine needles emit phytoncide, a common term for various sterilizing substances that plants emit to defend themselves from other microorganisms, more than 10 times more than other plants. These phytoncides kill bacteria and fungi in the air, and prevent pests and weeds from invading plants. In addition, it also eliminates pathogens harmful to humans, and the pine needle extract produced through the above process suppresses skin troubles caused by bacteria, etc. do.

The raw material mixing step (S103) is a step of mixing the pine needle extract prepared through the pine needle extract manufacturing step (S101-1) with the mineral extract prepared through the mineral extract manufacturing step (S101), the mineral extract manufacturing step It is preferable to mix 150 to 250 parts by weight of the pine needle extract prepared through the pine needle extract preparation step (S101-1) with 100 parts by weight of the mineral extract prepared through (S101).

When the pine needle extract is contained in the mineral extract, the proliferation of bacteria or fungi in the air is suppressed in the lotion, and the occurrence of skin troubles such as inflammation is suppressed by sterilizing the bacteria remaining on the skin, thereby providing a lotion with excellent skin soothing effect. can provide

If the content of the pine needle extract is less than 150 parts by weight, the above effect is insignificant, and when the content of the pine needle extract exceeds 250 parts by weight, the effect is not significantly improved and the content of the mineral extract is relatively reduced, resulting in skin whitening, Skin moisturizing, skin soothing, skin regeneration and wrinkle improvement effects may be reduced.

The cypress extract mixing step (S105) is a step of mixing the cypress extract with the mixture prepared through the raw material mixing step (S103), and 5 to 100 parts by weight of the mixture prepared through the raw material mixing step (S103) It is made by mixing 10 parts by weight.

The cypress extract is prepared by mixing 100 to 400 parts by weight of purified water with 100 parts by weight of cypress leaf, and extracting it at a temperature of 105 to 150° C. for 3 to 9 hours after input to an essential oil extraction pressure machine, and 100 parts by weight of cypress leaf Most preferably, it is prepared by mixing 250 parts by weight of purified water and extracting it at a temperature of 130° C. for 6 hours after input to an essential oil extraction pressure machine.

Cypress extract prepared through the above process contains a large amount of terpene flavor and phytoncide, so it relieves stress, strong antibacterial action, anti-corruption action, deodorant action, neutralizing harmful substances, sedative action, allergy and skin disease improvement work, and immune function enhancement. and so forth.

When the content of the cypress extract is less than 5 parts by weight, the above effects are insignificant, and when the content of the cypress extract exceeds 10 parts by weight, the above effects are not significantly improved and the skin whitening, skin moisturizing, skin soothing, Skin regeneration and wrinkle improvement effects may be reduced.

The precipitation and aging step (S107) is a step of precipitating and aging the mixture containing the cypress extract through the cypress extract mixing step (S105), and the mixture containing the cypress extract 20 through the cypress extract mixing step (S105) After leaving for 30 hours to precipitate the precipitate, and recovering the supernatant, stirring for 30 minutes at a speed of 100 to 200 rpm at a temperature of 20 to 25 ° C and aging for 45 to 50 hours.

The mixture that has undergone the precipitation and aging step (S107) consisting of the above process can be commercialized through a process of filtration through a reverse osmosis filter, etc. , a lotion showing homogeneous physical properties is provided.

In addition, between the cypress extract mixing step (S105) and the precipitation and aging step (S107), 10 to 30 parts by weight of the additive compared to 100 parts by weight of the mixture prepared through the cypress extract mixing step (S105) is mixed in an additive input step (S106) ) can be further proceeded, and the additive is preferably made of one or more selected from the group consisting of Jinuari extract, sacha inchi oil, amethyst extract, mineral salt extract, pearl extract, aloes extract and ginseng extract, and consists of ginseng extract. it is most preferable

The ginuari extract has excellent moisturizing effect and serves to further improve the moisturizing effect of the cosmetic composition according to the present invention. , glycerin, acetone, ethyl acetate, chloroform, butyl acetate, diethyl ether, dichloromethane, solvent extraction method of extraction with an extraction solvent selected from the group consisting of nucleic acids and mixtures thereof, supercritical extraction method, ultrasonic extraction method and microorganisms It can be prepared by an extraction method selected from the group consisting of fermentation extraction method.

In addition, the Sacha Inchi Oil exhibits moisturizing power and excellent moisture retention power. It is an oil obtained by pressing the seeds of African walnut (Plukenetia Volubilis), and various called by nickname. Sacha Inchi Oil contains omega-3 (48%), omega-6 (36%), and omega-9 (9%), and is rich in iodine and vitamins A and E. Omega 3 and vitamin E show excellent effects on skin regeneration.

In addition, the amethyst extract is produced by extracting from amethyst (紫水晶, Amethyst), and the amethyst is produced in pegmatite rocks as magma (lava) cools during a volcanic eruption, usually determined by hydrothermal water for 60 million years. As a weak mineral, it is also called magnetite (紫石英). The amethyst is harmless to the human body because its composition is determined as 99% silicon, and as the mystical power of far-infrared radiation, negative ions, and other waves and biological waves and the mysterious power of the hexagonal system is known, it is used as a bio raw material for various health new materials such as cosmetic raw materials and paint raw materials. is being applied

In addition, the mineral salt extract (Mineral Salt or Sea Salt Extract) is prepared by extracting from mineral salt, the mineral salt is a mineral belonging to the equiaxed crystal system having the same crystal structure as diamond, and the chemical composition is sodium chloride (NaCl). The mineral salt is mostly colorless and transparent, but sometimes has yellow, red, blue, and purple colors, and the streak color is white. Sodium chloride constituting the mineral salt is physiologically essential for animals and is included in body fluids to control the osmotic pressure of body fluids, and sodium, a component of sodium chloride, binds with phosphoric acid to maintain acid-base balance of body fluids as a buffer material. . The mineral salt exerts a positive effect on the human body when applied to the skin as well as ingested, and has been reported to have superior skin moisturizing power than urea, which is a natural moisturizing factor of the skin. ), it is known to be effective in removing skin waste and dead skin cells, acne, wrinkles, and atopy.

In addition, the pearl extract is prepared by extracting from pearl, and the pearl is a gem obtained from shellfish, which is an aquatic organism. includes Most of the organic matter is conchiolin, known as a skeletal protein, and conchiolin is a natural protein composed of 7 to 14 amino acids. is a substance The pearl is known to be useful as a herbal medicine, and when the pearl is ingested, it is known to strengthen bones, lower blood pressure, and promote digestion and stomach action. In addition, the pearl is also known to be useful as a treatment for burns or a hair growth promoting agent when applied to the face and skin.

In addition, the olivine extract is extracted from olivine, and the olivine has an excellent far-infrared radiation effect, and the far-infrared radiation emitted from the olivine penetrates up to 40 mm into the skin and expands the capillaries of the human body, thereby expanding blood circulation. It can help the excretion of toxins by making it smooth and promoting metabolism. The olivine suppresses the activity of free radicals in the body through anions and has an antioxidant action to prevent aging, and it can have the effect of discharging waste products and increasing immunity by more active blood circulation and metabolism.

In addition, the ginseng extract is prepared by mixing ginseng powder with an extraction solvent, cooling and filtration, mixing 100 parts by weight of ginseng powder with 800 to 1200 parts by weight of an extraction solvent, cooling for 2 to 4 days, and then filtering it is preferable

At this time, the extraction solvent is water, methanol, ethanol, propyl alcohol, C ₁ to C ₄ lower alcohols such as butyl alcohol, polyhydric alcohols such as glycerin, butylene glycol, propylene glycol and methyl acetate, ethyl acetate, acetone, benzene , hexane, diethyl ether, dichloromethane, or a mixture thereof may be used, or a mixture thereof, preferably water, lower alcohol, 1,3-butylene glycol, ethyl acetate alone or a mixture of two or more can be used by

Samchil (三七) The root and rhizome of Panax notoginseng FH Chen (Araliaceae) is a perennial herb that is collected in autumn and used as a medicine. It can be named as Jeonchil, Jeonsaengchil, and Ginsengsamchil.

The ginseng extract prepared through the above process serves to provide a lotion with excellent moisturizing effect by increasing the moisturizing power by maintaining the skin's own natural defense function.

In addition, between the cypress extract mixing step (S105) and the precipitation aging step (S107), a basalt treatment step of mixing 3 to 5 parts by weight of basalt powder in 100 parts by weight of the mixture prepared through the cypress extract mixing step (A105) ( S106-1) may further proceed.

At this time, both the additive input step (S106) and the basalt treatment step (S106-1) may proceed between the cypress extract mixing step (S105) and the precipitation and aging step (S107), in this case, the additive input step ( It is preferable to proceed with the basalt treatment step (S106-1) after S106).

The basalt powder has a particle size of 400 to 1200 mesh, and serves to provide a lotion showing efficacy such as sebum secretion control, pore reduction, skin moisture, skin cleansing and improvement of blood circulation by far-infrared radiation.

Here, having a particle size within the range of 400 mesh or more means the size that passes through a sieve of 400 mesh or more, and having a particle size within the range of less than 1250 mesh means a sieve with a number smaller than 1250 mesh. The smaller the number, the larger the sieve). Therefore, having a particle size within the range of 400 mesh or more and less than 1250 mesh refers to the particle size that passes through a 400 mesh sieve but takes on a 1250 mesh sieve.

In addition, if the particle size of the basalt powder is less than the above range, the particle size is too small, causing self-aggregation of the particles, difficult handling and storage, and may aggravate difficulties such as scattering during product manufacturing. .

If the content of the basalt powder is less than 3 parts by weight, the above effect is insignificant, and when the content of the basalt powder exceeds 5 parts by weight, the above effect is not significantly improved and formulation is difficult, product usability decreases, skin irritation increases side effects may occur.

Hereinafter, the method for manufacturing a lotion using minerals and pine needles according to the present invention and the physical properties of the lotion prepared through the manufacturing method will be described with reference to examples.

<Preparation Example 1> Preparation of mineral extract

Particle size is 320 parts by weight of purified water, 100 parts by weight of loess, 85 parts by weight of illite, 50 parts by weight of zeolite, 30 parts by weight of elvan, 12 parts by weight of bentonite, diatomaceous earth, 12 parts by weight, 55 parts by weight of jade, germanium 4 parts by weight of a mineral powder consisting of 30 parts by weight and 30 parts by weight of limestone was put into a stirrer equipped with a heating device, stirred at 150 rpm and 60° C. for 6 hours, and the stirred mixture was left for 21 hours to precipitate solid content. After drying, the supernatant water is recovered using a pump, and the recovered supernatant water is aged at a temperature of 60° C. for 60 hours, and then the aged supernatant water is subjected to a sediment filter, a plastic carbon filter, a hollow fiber membrane filter, a post carbon filter, and reverse osmosis pressure. The mineral extract was prepared by sequential filtration with a filter.

<Preparation Example 2> Preparation of pine needle extract

After washing and drying red pine pine needles as raw materials, dried in the shade for 36 hours, crushed to a size of 120 mesh, dissolved in water, and then water was removed by steam distillation at 95° C. for 4 hours to prepare a pine needle extract .

<Preparation Example 3> Preparation of cypress extract

A cypress extract was prepared by mixing 250 parts by weight of purified water with 100 parts by weight of cypress leaf, adding it to an essential oil extraction press, and extracting it at a temperature of 130° C. for 6 hours.

<Example 1>

After mixing 200 parts by weight of the pine needle extract prepared in Preparation Example 2 to 100 parts by weight of the mineral extract prepared in Preparation Example 1, and stirring at a speed of 200 rpm for 30 minutes, 100 parts by weight of the mixture cypress extract 8 After mixing parts by weight, leaving the mixture for 24 hours to set the precipitate and recovering the supernatant, the recovered supernatant water was stirred at a temperature of 22° C. at a speed of 150 rpm for 30 minutes and aged for 48 hours to obtain minerals and pine needles. The used lotion was prepared.

<Example 2>

In the same manner as in Example 1, 100 parts by weight of the mineral extract prepared in Preparation Example 1 was mixed with 150 parts by weight of the herbal extract prepared in Preparation Example 2 to prepare a lotion using minerals and pine needles.

<Example 3>

In the same manner as in Example 1, 250 parts by weight of the pine needle extract prepared in Preparation Example 2 was mixed with 100 parts by weight of the mineral extract prepared in Preparation Example 1 to prepare a lotion using minerals and pine needles.

<Comparative Example 1>

M's lotion.

<Comparative Example 2>

Company A's lotion (essence skin)

The skin moisturizing power, skin whitening, skin soothing and wrinkle improvement effects of the lotion prepared in Examples 1 to 3 and Comparative Examples 1 to 2 were measured and shown in Table 1 below.

(However, the skin moisturizing power, skin whitening, skin soothing and wrinkle improvement effects are for 50 women in their 20s to 50s, but 10 people per group apply the lotion of Examples 1 to 3 and Comparative Examples 1 and 2 2 per day. After applying for two months by applying 5 g each to the face, satisfaction was surveyed using a 5-point scale and expressed as an average value, 5 points: very good, 4 points: excellent, 3 points: average, 2 points: poor, 1 point. : Very bad.)

<Table 1>

As shown in Table 1, it can be seen that the lotion using the mineral and pine needles prepared in Examples 1 to 3 of the present invention has excellent effects such as skin moisturizing power, skin whitening, skin soothing and wrinkle improvement.

Therefore, the method for manufacturing a lotion using minerals and pine needles according to the present invention has excellent skin whitening, skin moisturizing, skin soothing, skin regeneration and wrinkle improvement effects, and excellent anti-inflammatory and antibacterial performance, and does not add a separate preservative. To provide a lotion with excellent preservability without

S101; Mineral Extract Manufacturing Stage
S101-1; Pine leaf extract manufacturing step
S103; Raw material mixing stage
S105 ; Cypress Extract Mixing Step
S106 ; Additive input step
S106-1; Basalt Treatment Stage
S107; Precipitation maturation stage

Claims (10)

Mineral extract manufacturing step of preparing a mineral extract;
A pine needle extract preparation step of preparing a pine needle extract;
A raw material mixing step of mixing 150 to 250 parts by weight of the pine needle extract prepared through the pine needle extract manufacturing step to 100 parts by weight of the mineral extract prepared through the mineral extract manufacturing step;
a cypress extract mixing step of mixing the cypress extract with the mixture prepared through the raw material mixing step; and
A method for producing a lotion using minerals and pine needles, characterized in that it comprises; a precipitation aging step of precipitating and aging the mixture containing the cypress extract through the cypress extract mixing step.
The method according to claim 1,
The pine needle extract manufacturing step is a process of washing and drying pine needles, drying them in the shade for 24 to 48 hours, crushing them to a size of 50 to 200 mesh, dissolving them in water, and then removing moisture by steam distillation. A method for manufacturing a lotion using minerals and pine needles, characterized in that
The method according to claim 1,
Between the cypress extract mixing step and the precipitation ripening step, an additive input step of mixing 10 to 30 parts by weight of an additive relative to 100 parts by weight of the mixture prepared through the cypress extract mixing step is further performed,
The additive is a method for producing a lotion using minerals and pine needles, characterized in that it consists of at least one selected from the group consisting of Jinuari extract, sacha inchi oil, amethyst extract, mineral salt extract, pearl extract, aloes root extract and ginseng extract.
4. The method according to claim 3,
The additive consists of ginseng extract,
The ginseng extract is a method for preparing a lotion using minerals and pine needles, characterized in that it is prepared by mixing ginseng powder with an extraction solvent, cooling and filtering.
5. The method according to claim 4,
The method for preparing a lotion using minerals and pine needles, characterized in that the ginseng extract is prepared by mixing 100 parts by weight of ginseng powder with 800 to 1200 parts by weight of an extraction solvent, cooling it for 2 to 4 days, and then filtering it.
The method according to claim 1,
The mineral extract manufacturing step is a mineral mixing step of mixing the mineral powder;
A stirring step of mixing the mineral mixture prepared through the mineral mixing step with purified water and stirring at a temperature of 45 to 80° C. for 5 to 7 hours;
a mineral phase recovery step of recovering supernatant water by leaving the stirred mineral mixture through the stirring step;
Aging step of aging the supernatant recovered through the mineral supernatant recovery step; and
A method for producing a lotion using minerals and pine needles, characterized in that it comprises; a filtration step of filtering the supernatant water aged through the aging step.
6. The method of claim 5,
Between the cypress extract mixing step and the precipitation aging step, a basalt treatment step of mixing 3 to 5 parts by weight of basalt powder to 100 parts by weight of the mixture prepared through the cypress extract mixing step is further performed. Mineral and pine needles A method for preparing a lotion using
The method according to claim 1,
The method of manufacturing a lotion using minerals and pine needles, characterized in that the step of mixing the cypress extract comprises mixing 5 to 10 parts by weight of the cypress extract in 100 parts by weight of the mixture prepared through the raw material mixing step.
9. The method of claim 1 or 8,
The cypress extract is prepared by mixing 100 to 400 parts by weight of purified water with 100 parts by weight of the cypress leaf, putting it in an essential oil extraction pressure machine, and extracting it at a temperature of 105 to 150° C. for 3 to 9 hours. Mineral and pine needles A method for manufacturing a lotion using
10. The method of claim 9,
The method for producing a lotion using minerals and pine needles, characterized in that the cypress extract is prepared by mixing 250 parts by weight of purified water with 100 parts by weight of cypress leaf, and extracting it at a temperature of 130° C. for 6 hours after inputting it into an essential oil extraction press. .

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