KR20160142114A - The composition of foot dip disinfectant for livestock quarantine and method for manufacturing thereof - Google Patents
The composition of foot dip disinfectant for livestock quarantine and method for manufacturing thereof Download PDFInfo
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- KR20160142114A KR20160142114A KR1020150078054A KR20150078054A KR20160142114A KR 20160142114 A KR20160142114 A KR 20160142114A KR 1020150078054 A KR1020150078054 A KR 1020150078054A KR 20150078054 A KR20150078054 A KR 20150078054A KR 20160142114 A KR20160142114 A KR 20160142114A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
- A01N33/02—Amines; Quaternary ammonium compounds
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
- A01N31/02—Acyclic compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2/00—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor
- A61L2/16—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor using chemical substances
- A61L2/18—Liquid substances or solutions comprising solids or dissolved gases
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Environmental Sciences (AREA)
- Plant Pathology (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- Pest Control & Pesticides (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Agronomy & Crop Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Epidemiology (AREA)
- Animal Behavior & Ethology (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
Description
The present invention relates to a composite composition for scaffold disinfection chemicals for preventing livestock epidemic diseases such as foot-and-mouth disease and avian influenza, and more particularly, to a composition for preventing livestock diseases which does not freeze in winter and is stable at high temperatures and sunlight, And a method of manufacturing the same.
Recently, foot and mouth disease and Avian influenza have been continuing to develop in Korea, causing serious economic and social damage.
The foot-and-mouth disease is acute viral disease of hoofed animals such as cattle, pigs, and deer, characterized by formation of vesicles mainly on hoofs, oral mucous membranes and papillae and is very infectious. It is designated as the first livestock infectious disease in the country and managed. Although foot-and-mouth disease viruses do not spread to humans, the transmission rate between animals is very fast and the mortality rate is up to 50%. Recently, foot-and-mouth disease virus ("FMD") has been reported to spread to remote farms mainly through people or vehicles, especially when contaminated by human shoes or wheels.
On the other hand, avian influenza is an acute respiratory disease that is infected with avian influenza, which is called avian influenza. Avian influenza, especially avian influenza, can be transmitted from animals to humans, so it is a very important disease in public health. In Korea, because of the disposal policy for the avian influenza, the economic damage caused by the disposal is not only large but also the growth of the industry related to the poultry industry is hindered because of the decrease in consumption of the products and the prohibition of export. The avian influenza virus has been reported to be caused by contaminated feces of infected migratory birds in human shoes.
Therefore, the government of Korea is also investing huge amount of manpower and budget for the prevention of foot-and-mouth disease and avian influenza, so as to prevent and block the disease. As part of this, the disinfection drug for foot-and- mouth disease and avian influenza is purchased and supplied to livestock farmers and related organizations free of charge .
Disinfection drugs for foot-and-mouth disease and avian influenza are used for disinfection of domestic animals, disinfection of domestic animals, disinfection of footbaths, disinfection of vehicles and wheels, disinfection of vehicles, disinfection of animals inside the vehicle to prevent influenza virus and avian influenza virus from entering the farm, Disinfecting chemicals used to disinfect polluted areas such as disinfecting people and roads and migratory birds. It is desirable that such disinfectant drugs are developed and supplied to be suitable for disinfection.
For example, domestic disinfectants must be manufactured from ingredients that do not cause skin and respiratory disturbance of livestock because domestic animals are kept in the house, and disinfectants for roads and migratory birds are harmful to nearby plants, streams, lakes and soils. It should be manufactured with no ingredients. Since the disinfection tank is provided outdoors such as a farm entrance, a housing entrance such as a farm entrance, a building entrance such as a government office where a lot of livestock related personnel go by, a door entrance of a migratory bird, etc., the disinfection of the footbath disinfectant should not be frozen in the winter season and should be stable to sunlight and high temperature. The lowering of the disinfection power by the water should be small. In some advanced countries, such as Germany and the UK, disinfectants suitable for the disinfection target have been developed and marketed in various fields, but they are still in the early stage of research in Korea.
In particular, the outbreak of foot-and-mouth disease and avian influenza viruses spread rapidly through people's shoes or vehicle wheels, and it is emphasized the importance of disinfection of pedestal shoes that can disinfect people's shoes or wheels. Has been demanded.
At present, there is no special disinfectant for disinfection of foot-and-mouth disease for the prevention of foot-and-mouth disease and avian influenza in Korea. However, phenolic compounds, aldehyde compounds, surfactants, halogen compounds and acid disinfectants have been recommended as substitutes for footing disinfectants. Since these disinfecting chemicals are not exclusive disinfectants for footing, they have various problems as follows.
Phenol compound disinfectant is the main component of the disinfectant of phenolic compound. When used as a foot disinfectant, the effect of the disinfectant decreases rapidly in sunlight. It has low penetration power in organic matter, strong smell, high shoe corrosion and low freezing point.
Aldehyde compound disinfectant is mainly composed of glutaraldehyde, and when it is used as a footing disinfectant drug, the disinfectant liquid is frozen in the winter when it is cold and has strong irritation, and it is toxic such as cancer when it is exposed to the respiratory tract.
Surfactants are mainly quaternary ammonium salts, and when used as a footing disinfectant, the disinfecting power is reduced when exposed to sunlight and high temperature, and the disinfectant solution is frozen in the cold of winter.
Halogenated compounds are chlorine-based, and they are a disinfectant for footing, and when exposed to the sunlight or when the temperature rises, the disinfection power drops rapidly and the disinfectant solution is frozen in the cold of winter.
The acidic preparation is mainly composed of citric acid and lactic acid, and is a disinfectant for scaffolds. When used as a scaffold, it has insufficient disinfecting power and penetration ability in organic matter, and disinfectant solution is frozen in winter.
Due to the weaknesses of the conventional chemicals used in footing disinfection, disinfection effect is not so much compared with the input cost and labor, and it is urgent to prepare countermeasures.
DISCLOSURE OF THE INVENTION Accordingly, the present invention has been made to solve the above-mentioned problems of the conventional disinfectant for animal husbandry, and it is a disinfectant for disinfecting foot care for effectively preventing livestock infectious diseases such as foot-and-mouth disease and avian influenza, The present invention has been made to provide a composite composition for disinfectant for disinfection of footbath and a method of manufacturing the same, which can greatly improve the efficiency and economical efficiency of disinfection.
Technical Solution In order to achieve the above object, the technical means of the present invention is a method for purifying a quaternary ammonium compound, which comprises reacting Lactic acid, Glycerin, Polysorbate 80 and Ethanol with a quaternary ammonium compound, Wherein the composite composition comprises 0.01 to 0.2% by weight of quaternary ammonium, 0.002 to 0.05% by weight of lactic acid, 20 to 60% by weight of glycerin, 0.01 to 1% by weight of polysorbate 80, 5 to 20% And 18.75 to 74.978% by weight of purified water.
An appropriate amount of purified water was added to a warming stirrer and lactic acid, glycerin, and polysorbate 80 were added in order while stirring at a speed of 20 rpm. The stirring speed was increased at a speed of 35 rpm, the temperature of the stirring tank was gradually increased, Quaternary ammonium was added to the intermediate preparation which had been cooled to room temperature and then stirred at a speed of 10 rpm for 6 to 12 hours. Then, ethanol and the remaining amount of purified water were added to the mixture to adjust the composition to 100 wt% Are mixed with each other.
The present invention relates to a footing disinfecting drug composition comprising Quaternary ammonium compound, Lactic acid, Glycerin, Polysorbate 80 and Ethanol, It is not frozen even in cold weather in winter, and disinfection power is not greatly reduced by temperature, sunlight and organic matter. Therefore, effective disinfection can be performed when a livestock infectious disease such as foot-and-mouth disease or avian influenza occurs and the efficiency and economical efficiency of sterilization can be greatly improved have.
Hereinafter, the present invention will be described in detail.
The disinfectant composition for livestock poultry disinfection according to the present invention is composed of quaternary ammonium as a disinfecting ingredient and glycerin, polysorbate 80 and ethanol as a stabilizer in lactic acid and is mixed with purified water. In the winter, when the disinfectant is freezing, In addition, the present invention solves the problem that the disinfectant is quickly decomposed by sunlight, high temperature, and organic matter, and the disinfecting power is reduced, thereby enabling effective disinfection of footplate.
The quaternary ammonium compound, which is a disinfecting component, is preferably 0.01 to 0.2% by weight based on the total composition. At this time, if quaternary ammonium is less than 0.01 wt%, the disinfecting power is insufficient, and when it is more than 0.2 wt%, it is not preferable because of excessive use.
The quaternary ammonium may be benzalkonium chloride or Didecyl dimethyl ammonium chloride.
The composition of the present invention is preferably an organic acid produced from lactic acid by a lactic acid bacterium in an amount of 0.002 to 0.05% by weight of the total composition. When the amount of lactic acid is 0.002% by weight or less in the present invention, If the improvement effect is insufficient and 0.05 wt% or more, it is not preferable because of excessive use.
Glycerin used in the present invention has a side effect, and it is used for relieving the irritation of the diluted solution, softening the locality, protecting the local drug, locust, alleviating external stimuli and preventing intrusion of harmful substances It is preferable to use 20 to 60% by weight of the total composition. When the amount of glycerin in the present invention is 20% by weight or less, the effect of improving the resistance to frost formation and stability is insufficient and the disinfecting power is decreased .
Among the compositions of the present invention, Polysorbate 80 is a surface active agent used for dispersing vitality, hormones, procaine penicillin and the like in a water solution, and is preferably 0.01 to 1% by weight in the total composition When the content is less than 0.01% by weight, the effect of improving the stability against sunlight, temperature and organic matters is low, and when it is 1% by weight or more, it is not preferable due to an increase in production cost.
Ethanol used in the present invention is preferably used in an amount of 5 to 20% by weight of the total composition. When the amount is less than 5% by weight, the effect of improving disinfecting power and resistance to frost formation is insufficient. When the amount is more than 20% by weight, It may cause a problem in safety, which is not preferable.
The purified water of the scaffold disinfecting drug composition according to the present invention is used as an excipient so that the total weight percentage of the scouring disinfectant composition is 100% by weight based on the sum of disinfection components and stabilizing component weight percentages used.
The method for manufacturing the scaffold disinfecting drug composite composition for livestock protection according to the present invention comprises the steps of preparing an intermediate preparation liquid and preparing a composite composition.
In the intermediate preparation step, 40 wt% of purified water was added to a warming stirrer, and 0.01 wt% of lactic acid, 40 wt% of glycerin and 0.1 wt% of polysorbate 80 were sequentially added thereto while stirring at 20 rpm, Is stirred at 35 rpm, the temperature of the stirring tank is gradually raised to 65 DEG C, stirred for 30 minutes, and cooled to room temperature to prepare an intermediate preparation liquid.
0.05 part by weight of quaternary ammonium was added to the intermediate preparation solution and stirred slowly at a rate of 10 rpm for 6 to 12 hours. Then, purified water was added to the mixture in an amount of 10% by weight of ethanol and 100% At a rate of 30 minutes to finally prepare a composite composition for disinfection of footpad for livestock, and quaternary ammonium reaction time is most preferably 9 hours.
The present invention can be understood more specifically by the following examples and experimental examples, and it is to be understood that the following examples are merely illustrative of the present invention and are not intended to limit the scope of the present invention.
A plurality of raw materials are mixed as shown in Table 1 to prepare a composite composition.
The process for preparing the composite composition of Example 1 is as follows.
40 wt% of purified water was put into a stirrer for warming, lactic acid, glycerin and polysorbate 80 were sequentially added thereto while stirring at a speed of 20 rpm, the stirring speed was raised to 35 rpm, the temperature of the stirring tank was gradually raised, After stirring the mixture for a minute, the mixture was cooled to room temperature, added with benzalkonium chloride, stirred slowly at a speed of 10 rpm for 9 hours, mixed with ethanol and the remaining amount of purified water, and mixed at 35 rpm for 30 minutes.
A plurality of raw materials are mixed as shown in Table 2 to prepare a composite composition.
The process for preparing the composite composition of Example 2 is as follows.
40% by weight of purified water was put into a stirrer for warming, and glycerin and polysorbate 80 were sequentially added thereto while stirring at a speed of 20 rpm, the stirring speed was increased to 35 rpm, the temperature of the stirring tank was gradually raised, The mixture was cooled to room temperature, added with benzalkonium chloride, stirred slowly at a speed of 10 rpm for 9 hours, mixed with ethanol and the remaining amount of purified water, and mixed at 35 rpm for 30 minutes.
A plurality of raw materials are mixed as shown in Table 3 to prepare a composite composition.
The process for preparing the composite composition of Example 3 is as follows.
40 wt% of purified water was put into a stirrer for warming, lactic acid, glycerin and polysorbate 80 were sequentially added thereto while stirring at a speed of 20 rpm, the stirring speed was raised to 35 rpm, the temperature of the stirring tank was gradually raised, The mixture was stirred for a minute, cooled to room temperature, mixed with ethanol and the remaining amount of purified water, and mixed at a speed of 35 rpm for 30 minutes.
A plurality of raw materials are mixed as shown in Table 4 to prepare a composite composition.
The process for preparing the composite composition of Example 4 is as follows.
40% by weight of purified water was put into a stirrer for warming, lactic acid and polysorbate 80 were sequentially added while stirring at a speed of 20 rpm, the stirring speed was raised to 35 rpm, the temperature of the stirring tank was gradually raised, and the mixture was stirred at 65 캜 for 30 minutes The mixture was cooled to room temperature, added with benzalkonium chloride, stirred slowly at a speed of 10 rpm for 9 hours, mixed with ethanol and the remaining amount of purified water, and mixed at 35 rpm for 30 minutes.
A plurality of raw materials are mixed as shown in Table 5 to prepare a composite composition.
The process for preparing the composite composition of Example 5 is as follows.
40% by weight of purified water was added to the stirrer for warming, and lactic acid and glycerin were added in this order while stirring at a speed of 20 rpm, the stirring speed was increased to 35 rpm, the temperature of the stirring tank was gradually raised, stirring was continued for 30 minutes at 65 ° C, And the mixture was stirred at 10 rpm for 9 hours. Then, ethanol and the remaining amount of purified water were added and mixed at a speed of 35 rpm for 30 minutes.
A plurality of raw materials are mixed as shown in Table 6 to prepare a composite composition.
The process for preparing the composite composition of Example 6 is as follows.
After adding benzalkonium chloride, lactic acid, ethanol and purified water to the agitator in order, the mixture was mixed at a speed of 35 rpm for 30 minutes and subdivided by a predetermined amount.
A plurality of raw materials are mixed as shown in Table 7 to prepare a composite composition.
The process for preparing the composite composition of Example 7 is as follows.
Benzalkonium chloride, ethanol and purified water were sequentially added to the agitator, and the mixture was mixed at a speed of 35 rpm for 30 minutes and subdivided by a predetermined amount.
A plurality of raw materials are mixed as shown in Table 8 to prepare a composite composition.
The process for preparing the composite composition of Example 8 is as follows.
Lactic acid, ethanol, and purified water are sequentially added to the agitator, and the mixture is mixed at a rate of 35 rpm for 30 minutes and subdivided by a predetermined amount.
The raw materials for forming the composite compositions of Examples 1 to 8 above are summarized in Table 9 below.
≪ Experimental Example 1 >
1. Experimental Method
In order to carry out the cross-linking test of the composite compositions formed in Examples 1 to 8, each composition was weighed in a 500 ml beaker in an amount of 400 ml and allowed to stand at 5 ° C, 10 ° C, 15 ° C and 20 ° C for 24 hours, Respectively.
2. Experimental results
Table 10 shows the results of the cross-linking test of the composite composition according to each example.
<Experimental Example 2> Test for stability against sunlight
1. Experimental Method
Determination of stability against sunlight of the composite composition formed by Examples 1 to 8 Each composition was filled in a 100 ml beaker in an amount of 50 ml each for 48 hours in a room free of sunshine and outdoors exposed to sunlight and then quaternary ammonium salt And lactic acid were measured.
2. Experimental results
The results of the stability test on the sunlight of the composite composition according to each example are shown in Table 11.
≪ Experimental Example 3 >
1. Experimental Method
Each composition was filled into a 100 ml beaker in an amount of 50 ml, placed in a constant-temperature and humidity chamber, and allowed to stand at 30 ° C and 50 ° C for 48 hours. The content of quaternary ammonium salt and lactic acid Were measured.
2. Experimental results
The results of the stability test for the temperature of the composite composition according to each example are shown in Table 12.
<Experimental Example 4> Disinfection test in the presence of organic substances
1. Experimental Method
The composite compositions formed according to Examples 1 to 8 were comparatively evaluated using the MIC measurement method to investigate the degree of degradation of disinfection ability in the presence of organic matter. 0.2 mL of E. coli ATCC 25922 was inoculated into 100 mL of nutrition agar and cultured for 24 hours. Then, a test piece having a diameter of 8 mm and a thickness of 1.5 mm was placed on the culture medium. Yeast extract was added to each composition of the above Example as test solution The 5% organic matter diluent prepared was added to each test specimen in an amount of 50 쨉 m. After incubation for 24 hours, the average diameter of the bacterial growth inhibition rings was measured.
2. Experimental results
The results of the sanitization test in the presence of the organic compound of the composite composition according to each Example are shown in Table 13 below.
As described above, the scaffold disinfecting chemical composition for livestock defense according to the present invention and the method for producing the same have remarkably improved the efficiency of sterilization due to excellent stability against frost formation, sunlight stability, and temperature, And it is an extremely highly industrially applicable invention that considers economical aspects by reducing the cost of disinfection.
The embodiments of the pedicure disinfecting drug composite composition for livestock defense of the present invention described above and the method of manufacturing the same are merely illustrative and those skilled in the art will appreciate that various modifications and equivalent It will be appreciated that other embodiments are possible. Therefore, it is to be understood that the present invention is not limited to the above-described embodiments. Accordingly, the true scope of the present invention should be determined by the technical idea of the appended claims.
It is also to be understood that the invention includes all modifications, equivalents, and alternatives falling within the spirit and scope of the invention as defined by the appended claims.
Claims (4)
Wherein the quaternary ammonium is any one selected from the group consisting of benzalkonium chloride and Didecyl dimethyl ammonium chloride.
0.05 part by weight of quaternary ammonium was added to the intermediate preparation solution and stirred slowly at a speed of 10 rpm for 6 to 12 hours. Then, purified water was added thereto so that the total weight of the composite composition was 10% by weight of ethanol and 100% Thereby producing a scaffold antifouling drug composite composition for animal control.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20200041494A (en) * | 2018-10-12 | 2020-04-22 | 농업회사법인 주식회사 과농 | Sterilization and cleansing agent of antifreezing for cattle shed |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20210098650A (en) | 2020-02-03 | 2021-08-11 | 최형규 | The composition of disinfectant for veterinary usage containing thymol |
| KR102602886B1 (en) | 2021-06-30 | 2023-11-17 | 명전바이오 주식회사 | Environment-friendly disinfectant composition for preventing spread of infectious disease having excellent antibacterial and deodorizing function with liquid sodium silicate and environment-friendly disinfectant for preventing spread of infectious disease with the same |
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- 2015-06-02 KR KR1020150078054A patent/KR101687337B1/en active IP Right Grant
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| KR20070102487A (en) * | 2004-12-14 | 2007-10-18 | 더 퀴글리 코포레이션 | Compositions and methods for reducing the transmissivity of illnesses |
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