KR102106921B1 - The composition of livestock disinfectant which improved pest repellent effect - Google Patents
The composition of livestock disinfectant which improved pest repellent effect Download PDFInfo
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- KR102106921B1 KR102106921B1 KR1020180027263A KR20180027263A KR102106921B1 KR 102106921 B1 KR102106921 B1 KR 102106921B1 KR 1020180027263 A KR1020180027263 A KR 1020180027263A KR 20180027263 A KR20180027263 A KR 20180027263A KR 102106921 B1 KR102106921 B1 KR 102106921B1
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- repellent effect
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- 239000000203 mixture Substances 0.000 title claims abstract description 82
- 230000000249 desinfective Effects 0.000 title claims abstract description 65
- 244000144972 livestock Species 0.000 title claims abstract description 52
- 230000000694 effects Effects 0.000 title abstract description 45
- 241000607479 Yersinia pestis Species 0.000 title abstract description 40
- 239000005871 repellent Substances 0.000 title abstract description 34
- 230000002940 repellent Effects 0.000 title abstract description 34
- 239000002131 composite material Substances 0.000 claims abstract description 40
- 239000000077 insect repellent Substances 0.000 claims abstract description 26
- NBIIXXVUZAFLBC-UHFFFAOYSA-N phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 46
- DNIAPMSPPWPWGF-UHFFFAOYSA-N propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 34
- 239000008213 purified water Substances 0.000 claims description 33
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 33
- 229960000686 Benzalkonium Chloride Drugs 0.000 claims description 28
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 23
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 claims description 21
- 235000019270 ammonium chloride Nutrition 0.000 claims description 21
- QDHHCQZDFGDHMP-UHFFFAOYSA-N monochloramine Chemical compound ClN QDHHCQZDFGDHMP-UHFFFAOYSA-N 0.000 claims description 21
- 241000723347 Cinnamomum Species 0.000 claims description 15
- 235000004310 Cinnamomum zeylanicum Nutrition 0.000 claims description 15
- 235000017803 cinnamon Nutrition 0.000 claims description 15
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 15
- 239000000645 desinfectant Substances 0.000 claims description 6
- OOCCDEMITAIZTP-QPJJXVBHSA-N Cinnamyl alcohol Natural products OC\C=C\C1=CC=CC=C1 OOCCDEMITAIZTP-QPJJXVBHSA-N 0.000 claims description 5
- 230000001846 repelling Effects 0.000 abstract description 12
- 241000287828 Gallus gallus Species 0.000 description 10
- 239000004615 ingredient Substances 0.000 description 10
- 235000013601 eggs Nutrition 0.000 description 9
- 239000007788 liquid Substances 0.000 description 9
- 238000004519 manufacturing process Methods 0.000 description 9
- 238000000034 method Methods 0.000 description 9
- 239000002994 raw material Substances 0.000 description 9
- 239000010630 cinnamon oil Substances 0.000 description 8
- 238000003860 storage Methods 0.000 description 8
- 239000000575 pesticide Substances 0.000 description 6
- 244000144977 poultry Species 0.000 description 6
- 239000008399 tap water Substances 0.000 description 5
- 235000020679 tap water Nutrition 0.000 description 5
- 241000238631 Hexapoda Species 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
- 201000010099 disease Diseases 0.000 description 4
- 210000004369 Blood Anatomy 0.000 description 3
- 239000008280 blood Substances 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 230000000749 insecticidal Effects 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 238000004659 sterilization and disinfection Methods 0.000 description 3
- WBYWAXJHAXSJNI-VOTSOKGWSA-M .beta-Phenylacrylic acid Natural products [O-]C(=O)\C=C\C1=CC=CC=C1 WBYWAXJHAXSJNI-VOTSOKGWSA-M 0.000 description 2
- 241001481695 Dermanyssus gallinae Species 0.000 description 2
- 239000005899 Fipronil Substances 0.000 description 2
- ZOCSXAVNDGMNBV-UHFFFAOYSA-N Fipronil Chemical compound NC1=C(S(=O)C(F)(F)F)C(C#N)=NN1C1=C(Cl)C=C(C(F)(F)F)C=C1Cl ZOCSXAVNDGMNBV-UHFFFAOYSA-N 0.000 description 2
- KJPRLNWUNMBNBZ-QPJJXVBHSA-N cinnamic aldehyde Natural products O=C\C=C\C1=CC=CC=C1 KJPRLNWUNMBNBZ-QPJJXVBHSA-N 0.000 description 2
- 235000020230 cinnamon extract Nutrition 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 229940079593 drugs Drugs 0.000 description 2
- 229940013764 fipronil Drugs 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 239000002917 insecticide Substances 0.000 description 2
- 239000003381 stabilizer Substances 0.000 description 2
- 239000012085 test solution Substances 0.000 description 2
- 230000002588 toxic Effects 0.000 description 2
- 231100000331 toxic Toxicity 0.000 description 2
- 241000239223 Arachnida Species 0.000 description 1
- 210000003746 Feathers Anatomy 0.000 description 1
- 210000002751 Lymph Anatomy 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- QVLTXCYWHPZMCA-UHFFFAOYSA-N PO4-PO4 Chemical compound OP(O)(O)=O.OP(O)(O)=O QVLTXCYWHPZMCA-UHFFFAOYSA-N 0.000 description 1
- 210000003491 Skin Anatomy 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K [O-]P([O-])([O-])=O Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 230000001058 adult Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- KXDHJXZQYSOELW-UHFFFAOYSA-M carbamate Chemical compound NC([O-])=O KXDHJXZQYSOELW-UHFFFAOYSA-M 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 229930016911 cinnamic acid Natural products 0.000 description 1
- 235000013985 cinnamic acid Nutrition 0.000 description 1
- 229940117916 cinnamic aldehyde Drugs 0.000 description 1
- 244000078703 ectoparasites Species 0.000 description 1
- 239000003623 enhancer Substances 0.000 description 1
- 230000002708 enhancing Effects 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 235000021393 food security Nutrition 0.000 description 1
- 238000005755 formation reaction Methods 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 230000000422 nocturnal Effects 0.000 description 1
- 239000003002 pH adjusting agent Substances 0.000 description 1
- 230000002688 persistence Effects 0.000 description 1
- 239000000447 pesticide residue Substances 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- 230000036633 rest Effects 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000003892 spreading Methods 0.000 description 1
- 230000001954 sterilising Effects 0.000 description 1
- 230000002195 synergetic Effects 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 201000008297 typhoid fever Diseases 0.000 description 1
Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION, OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS, OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS, OR SURGICAL ARTICLES
- A61L2/00—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor
- A61L2/16—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor using chemical substances
- A61L2/18—Liquid substances or solutions comprising solids or dissolved gases
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/24—Lauraceae [Laurel family], e.g. laurel, avocado, sassafras, cinnamon or camphor
Abstract
본 발명은 해충 기피효과가 개선된 축사용 소독제 복합조성물에 관한 것으로 축사를 소독하기 위하여 사용되는 축사용 소독제에 해충 기피제를 복합조성하여 소독효과와 더불어 해충 기피효과가 우수한 소독제를 제공함으로써 기존 제품의 문제점인 소독력 저하 및 미흡한 해충 기피효과를 개선시킬 수 있다.The present invention relates to a composite composition of a livestock disinfectant with improved insect repellent effect, and provides a disinfectant having a good insect repellent effect as well as a disinfecting effect by compounding a pest repellent in a livestock disinfectant used to disinfect the house. It can improve the disinfecting power, which is a problem, and the repelling effect of insufficient pests.
Description
본 발명은 해충 기피효과가 개선된 축사용 소독제 복합조성물에 관한 것으로, 보다 상세하게는 축사를 소독하기 위하여 사용되는 축사용 소독제에 해충 기피제를 복합조성하여 소독효과와 더불어 해충 기피효과가 우수한 소독제를 제공함으로써 기존 제품의 문제점인 소독력 저하 및 미흡한 해충 기피효과를 개선시킬 수 있도록 한 해충 기피효과가 개선된 축사용 소독제 복합조성물에 관한 것이다.
The present invention relates to a composite composition of a livestock disinfectant with improved pest repellent effect, and more specifically, to provide a disinfectant excellent in pest repelling effect together with a disinfecting effect by compounding a pest repellent compound in a livestock disinfectant used to disinfect a house. The present invention relates to a composite composition for a livestock disinfectant with improved pest repelling effect, so as to improve the repellent effect and insufficient repelling effect, which is a problem of existing products.
최근 유럽뿐만 아니라 우리나라에서도 살충제 계란으로 인하여 엄청난 사회적 경제적 파장을 일으킨바 있다. 최초로 살충제가 잔류된 계란이 확인된 네덜란드는 식품 및 계란산업이 초토화 되었으며 세계 각국의 식량 안보에 대한 위협으로 대두되고 있다. 우리나라에서도 2017년 8월 경기도 남양주에 소재한 친환경 인증을 받은 양계장에서 생산된 계란에서 맹독성 살충제인 피프로닐이 검출되면서 전국 산란계농장 전수검사 결과 다수의 양계장에서 살충제가 잔류된 계란이 확인되어 커다란 사회적 문제가 대두된바 있다.Recently, not only in Europe, but also in Korea, pesticide eggs have caused tremendous social and economic impact. In the Netherlands, where the first pesticide-retaining eggs were identified, the food and egg industry was devastated and is emerging as a threat to food security worldwide. In Korea, in August 2017, when fipronil, a highly toxic insecticide, was detected in eggs produced in an environmentally-certified poultry farm located in Namyangju, Gyeonggi-do, as a result of the nationwide spawning farm inspection, eggs with pesticide residues were identified in a number of poultry farms. Has emerged.
닭 와구모는 닭 진드기라고도 부르며, 닭 등 가금류에 기생하는 거미강 진드기목의 외부기생충으로서 성충이 흡혈 후 피를 소화한 다음 4-8개의 알을 낳고 알이 부화하여 2-3일 후 유충이 되고 유충이 성장하여 흡혈이 가능한 약충이 되고 약충이 성장하여 흡혈 능력이 왕성한 성충이 되는 생활환을 가지고 있다.Chicken wagumo, also called chicken mite, is an ectoparasite of the arachnid mite that parasitizes poultry such as chickens. After the adult has digested the blood, it digests the blood, lays 4-8 eggs, hatches the egg, becomes a larva after 2-3 days. It has a life cycle where larvae grow and become vampires capable of vampire, and nymphs grow and become vigorous adults.
특히, 닭 와구모는 야행성으로 햇빛이 있는 주간에는 바닥이나 벽면 틈새 등 어두운 곳에서 쉬다가 밤이 되면 닭 피부 및 깃털로 이동하여 혈액이나 림프를 빨아먹고 살아간다. 라이프사이클은 6-9일이며 한 마리가 2달 후에는 1억마리 이상으로 증식하여 가금티푸스 등 질병을 전파하며 흡혈 스트레스로 산란율 및 계란품질 저하, 사료효율 감소 및 수명단축 등 막대한 경제적 피해를 유발한다. 농림축산식품부 발표에 의하면 국내 산란계 농장의 94%가 닭 와구모에 감염되어 있으며 이로 인해 경제적으로 엄청난 피해를 입고 있지만 마땅한 대책이나 구제제가 없어 안타까운 실정이다.In particular, chicken wagumo is nocturnal, and in the daylight when there is sunlight, it rests in a dark place such as a gap in the floor or wall, and at night, it moves to the chicken skin and feathers, sucking blood or lymph and living. The life cycle is 6-9 days, and after 2 months, one multiplies to more than 100 million, spreading diseases such as poultry typhoid and causing enormous economic damage such as spawning rate and egg quality deterioration, reduced feed efficiency and shortened lifespan due to vampire stress. do. According to the Ministry of Food, Agriculture, Forestry and Rural Affairs, 94% of domestic spawning farms are infected with chicken wagmo, which is causing great economic damage, but it is unfortunate because there are no proper measures or remedies.
현재 국내에는 닭 와구모를 구제하기 위하여 동물약품으로 허가된 카바메이트계, 유기인계 또는 유기염소계 살충제가 있지만 독성이 강하여 빈 계사에만 사용을 허가하고 닭에는 사용을 금지하고 있으며 이마저도 내성이 생겨 효과가 미흡하기 때문에 대부분의 농장주들은 닭에 감염된 와구모를 구제하기 위하여 살충력이 강력한 피닐피라졸계 화합물인 피프로닐(fipronil)등 양계장 및 닭에 사용하여서는 안 될 살충제 농약을 불법적으로 사용하여 사회적인 문제를 일으킨바 있다.Currently, there are carbamate, organophosphorus, or organochlorine pesticides that are approved as animal drugs in order to relieve chicken wagumo, but since they are highly toxic, they are only allowed to be used in empty cages, and are prohibited for use in chickens. Most farm owners have caused social problems by illegally using pesticide pesticides that should not be used in poultry farms and chickens, such as fipronil, which is a powerful insecticidal pinylpyrazole-based compound in order to remedy coccyx infected with chickens. .
특허출원 제10-2011-0001048(축사 및 양계 소독용 살충제 조성물 및 이의 제조방법)에서는 닭에 직접 살포하더라도 안전하고 살충성분의 지속력이 뛰어난 닭 진드기 구충용 살충제 조성물을 게시하고 있으나 정부에서는 살충성분의 독성으로 말미암아 가축이 없는 빈 축사에만 사용하도록 허가하고 있어 현실적으로 가축이 들어 있는 축사에 사용하는 것은 불가능하다.Patent application No. 10-2011-0001048 (Pesticide composition for disinfecting livestock and poultry and its manufacturing method) discloses a pesticide composition for insect repellent for chicken mite that is safe and has excellent persistence of insecticide even when sprayed directly on chicken, but the government Due to its toxicity, it is permitted to be used only for empty houses without livestock, so it is practically impossible to use for livestock houses.
따라서, 많은 축산농가에서 축사 소독제와 해충 기피제를 따로 따로 사용하고 있으나 빈번한 사용으로 인해 불편을 호소하고 있으며 일부농가에서는 해충 기피제가 복합된 소독제를 사용하고 있으나 소독성분의 안정성 저하로 소독효력이 감소되는 문제점과 해충기피효과마저 미흡하다는 문제점이 있어 생산자 단체에서는 소독제의 소독효력을 감소시키지 않으면서 해충기피효과가 우수한 소독제 개발을 정부에 요구하고 있는 실정이다.
Therefore, many livestock farms use barn disinfectants and pest repellents separately, but they frequently complain of discomfort due to frequent use, and some farms use disinfectants combined with pest repellents, but the disinfecting efficacy is reduced due to the stability of the disinfecting ingredients. Due to the problem and the problem that the insect repelling effect is insufficient, the producers' groups are demanding the government to develop a disinfecting agent having an excellent insect repelling effect without reducing the disinfecting effect of the disinfectant.
따라서, 상기와 같은 문제점을 해소하고자 본 발명은 축사에 살포하여 해충이 기피하도록 하여 가축의 질병을 예방하고, 약품 사용에 대한 안정성을 향상시켜 수요를 증대시킬 수 있도록 한 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제공하고자 안출된 목적이 있다.
Therefore, in order to solve the above problems, the present invention prevents pest diseases by spraying the barn to prevent pests and improve the stability of drug use, thereby improving the insect repellent effect. The purpose is to provide a composite composition for use disinfectants.
상기와 같은 목적을 달성하기 위한 본 발명의 기술적 수단은 염화벤잘코늄(Benzalkonium chloride), 인산(Phosphoric acid), 프로필렌글리콜(Propylene glycol), 염화암모늄(Ammonium chloride), 계피알코올(Cinnamyl alcohol) 및 정제수(Purified water)을 함유하는 복합조성물로서, 상기 복합조성물은 그 성분 조성비를 염화벤잘코늄 5~20중량%, 인산 10~35중량%, 프로필렌글리콜 10~35중량%, 염화암모늄 3~10중량%, 계피알코올 1~8중량% 및 정제수 4~71중량%로 이루어진 것을 특징으로 한다.
Technical means of the present invention to achieve the above object is benzalkonium chloride (Benzalkonium chloride), phosphoric acid (Phosphoric acid), propylene glycol (Propylene glycol), ammonium chloride (Ammonium chloride), cinnamon alcohol (Cinnamyl alcohol) and purified water As a composite composition containing (Purified water), the composite composition is composed of 5 to 20% by weight of benzalkonium chloride, 10 to 35% by weight of phosphoric acid, 10 to 35% by weight of propylene glycol, and 3 to 10% by weight of ammonium chloride. , Cinnamon alcohol is characterized by consisting of 1 to 8% by weight and 4 to 71% by weight of purified water.
상술한 바와 같이 본 발명에 따른 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제공함으로써, 축사를 소독하기 위하여 사용되는 축산용 소독제에 해충 기피제를 복합 조성하여 안정성이 우수하고, 해충 기피효과를 크게 향상시켜 가축의 질병 발생을 억제하며, 가축의 성장을 저해하는 요소를 미연에 방지하는 동시에 소독력을 크게 향상시킬 수 있는 매우 유용한 효과가 있다.
As described above, by providing a composite composition of a livestock disinfectant with improved pest repellent effect according to the present invention, the pest repellent is compounded in a livestock disinfectant used for disinfecting livestock to provide excellent stability and greatly improve the insect repellent effect. It improves and suppresses the occurrence of disease in livestock, and prevents the factors that inhibit the growth of livestock at the same time, and has a very useful effect that can greatly improve disinfecting power.
이하, 본 발명을 구체적으로 설명한다.Hereinafter, the present invention will be described in detail.
본 발명에 따른 해충 기피효과가 개선된 축사용 소독제 복합조성물은 소독성분인 염화벤잘코늄, pH조절제인 인산, 안정제인 프로필렌글리콜, 해충 기피효과 상승제인 염화암모늄, 해충 기피제인 계피알코올 및 정제수를 복합하여 구성한 것으로 기존 해충 기피효과가 있는 소독제의 문제점인 소독효력 저하 및 해충 기피효과가 미흡하다는 문제점을 해결하기 위한 것이다.The composite composition of the disinfectant for livestock use with improved pest repellent effect according to the present invention is a combination of benzalkonium chloride as a disinfecting component, phosphoric acid as a pH adjusting agent, propylene glycol as a stabilizer, ammonium chloride as a pest repellent enhancer, cinnamon alcohol as a pest repellent, and purified water This is to solve the problem that the disinfecting effect, which is a problem of the existing disinfecting agent having an insect repelling effect, and the insect repelling effect are insufficient.
이러한, 상기 해충 기피효과가 개선된 축사용 소독제 복합조성물의 성분 조성비는 염화벤잘코늄 5~20중량%, 인산 10~35중량%, 프로필렌글리콜 10~35중량%, 염화암모늄 3~10중량%, 계피알코올 1~8중량% 및 정제수 4~71중량%로 이루어짐이 가장 바람직하다.Such, the composition ratio of the compound composition of the livestock disinfectant with improved pest repellent effect is 5 to 20% by weight of benzalkonium chloride, 10 to 35% by weight of phosphoric acid, 10 to 35% by weight of propylene glycol, 3 to 10% by weight of ammonium chloride, Most preferably, it is composed of cinnamon alcohol 1-8% by weight and purified water 4-71% by weight.
본 발명에 사용되는 소독성분인 염화벤잘코늄은 전체 조성물의 중량을 기준으로 5~20중량%를 사용하는 것이 바람직하다.Benzalkonium chloride, which is a disinfecting component used in the present invention, is preferably 5 to 20% by weight based on the weight of the total composition.
상기 염화벤잘코늄이 5중량% 이하인 경우에는 살균소독효과가 미흡하고, 20중량% 이상일 때에는 조성물의 안정성이 저하되어 바람직하지 못하다.When the benzalkonium chloride is 5% by weight or less, the sterilization and disinfection effect is insufficient, and when it is 20% by weight or more, the stability of the composition is lowered, which is not preferable.
상기 해충 기피효과가 개선된 축사용 소독제 복합조성물의 pH조절제인 인산은 전체 조성물의 중량을 기준으로 10~35중량% 포함하는 것이 바람직하다. Phosphoric acid, which is a pH control agent for the composite composition of the disinfectant for livestock with improved pest repellent effect, is preferably included in an amount of 10 to 35% by weight based on the total composition weight.
상기 인산이 10중량% 이하인 경우에는 살균소독효과 미흡하고, 35중량% 이상인 경우에는 조성물의 안정성이 저하되어 바람직하지 못하다.When the phosphoric acid is 10% by weight or less, the sterilization effect is insufficient, and when it is 35% by weight or more, the stability of the composition is lowered, which is not preferable.
본 발명에 안정제로 사용되는 프로필렌글리콜은 전체 조성물의 중량을 기준으로 10~35중량%를 사용하는 것이 바람직하다. Propylene glycol used as a stabilizer in the present invention, it is preferable to use 10 to 35% by weight based on the weight of the total composition.
상기 프로필렌글리콜이 10중량% 이하이거나 35중량 이상인 경우에는 조성물의 해충 기피효과가 저하되어 바람직하지 못하다.When the propylene glycol is 10% by weight or less or 35% or more, the insect repellent effect of the composition is lowered, which is not preferable.
본 발명에 해충 기피효과 상승제로 사용되는 염화암모늄은 전체 조성물의 중량을 기준으로 3~10중량%를 사용하는 것이 바람직하다. Ammonium chloride used as an insect repellent synergist in the present invention is preferably 3 to 10% by weight based on the weight of the total composition.
상기 염화암모늄이 3중량% 이하인 경우에는 기피효과 상승 효과가 미흡하고 10중량 이상인 경우에는 조성물의 안정성이 저하되어 바람직하지 못하다.When the ammonium chloride is 3% by weight or less, the synergistic effect is insufficient, and when it is 10% or more, the stability of the composition is lowered, which is not preferable.
본 발명에 해충 기피제로 사용되는 계피알코올은 전체 조성물의 중량을 기준으로 1~8중량%를 사용하는 것이 바람직하다. Cinnamon alcohol used as a pest repellent in the present invention, it is preferable to use 1 to 8% by weight based on the weight of the total composition.
상기 계피알코올이 1중량% 이하인 경우에는 해충 기피효과가 미흡하고 8중량 이상인 경우에는 조성물의 안정성이 저하되어 바람직하지 못하다.When the cinnamon alcohol is 1% by weight or less, the insect repellent effect is insufficient, and when it is 8% or more, the stability of the composition is lowered, which is not preferable.
본 발명은 다음 실시 예 및 실험 예에 의해서 보다 구체적으로 이해될 수 있으며, 다음의 실시 예는 본 발명을 예시하기 위한 것에 지나지 않으며 본 발명의 범위를 제한하고자 하는 것은 아님을 밝히는 바이다.
The present invention can be understood in more detail by the following examples and experimental examples, and the following examples are only intended to illustrate the invention and are not intended to limit the scope of the invention.
다음의 표 1과 같은 성분으로부터 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제조한다.From the components shown in Table 1 below, a composite composition for a livestock disinfectant with improved pest repellency is prepared.
[표 1]의 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제조하는 공정은 다음과 같다. The process of manufacturing a composite composition for a livestock disinfectant with improved insect repellent effect in Table 1 is as follows.
상기 원료를 각각 교반기에 투입한 후 60rpm 속도로 30분간 혼합한 후 50㎛ 필터를 통하여 저장조로 이송하여 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제조하는 것이다. It is to prepare a composite composition for a livestock disinfectant with improved insect repellent effect by introducing the raw materials into a stirrer and mixing them at 60 rpm for 30 minutes and then transferring them to a storage tank through a 50 µm filter.
다음의 표 2와 같은 성분으로부터 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제조한다.From the components shown in Table 2 below, a composite composition for a livestock disinfectant with improved pest repellency is prepared.
[표 2]의 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제조하는 공정은 다음과 같다. The process of manufacturing a composite composition of a livestock disinfectant with improved insect repellent effect in Table 2 is as follows.
상기 원료를 각각 교반기에 투입한 후 60rpm 속도로 30분간 혼합한 후 50㎛ 필터를 통하여 저장조로 이송하여 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제조하는 것이다. It is to prepare a composite composition for a livestock disinfectant with improved insect repellent effect by introducing the raw materials into a stirrer and mixing them at 60 rpm for 30 minutes and then transferring them to a storage tank through a 50 µm filter.
다음의 표 3과 같은 성분으로부터 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제조한다.From the components shown in Table 3 below, a composite composition for a livestock disinfectant with improved pest repellency is prepared.
[표 3]의 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제조하는 공정은 다음과 같다. The process of manufacturing a composite composition of a livestock disinfectant with improved pest repellent effect in [Table 3] is as follows.
상기 원료를 각각 교반기에 투입한 후 60rpm 속도로 30분간 혼합한 후 50㎛ 필터를 통하여 저장조로 이송하여 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제조하는 것이다. It is to prepare a composite composition for a livestock disinfectant with improved insect repellent effect by introducing the raw materials into a stirrer and mixing them at 60 rpm for 30 minutes and then transferring them to a storage tank through a 50 µm filter.
다음의 표 4와 같은 성분으로부터 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제조한다.From the components shown in Table 4 below, a composite composition for a livestock disinfectant with improved pest repellency is prepared.
[표 4]의 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제조하는 공정은 다음과 같다. The process of manufacturing a composite composition for a livestock disinfectant with improved pest repellent effect in [Table 4] is as follows.
상기 원료를 각각 교반기에 투입한 후 60rpm 속도로 30분간 혼합한 후 50㎛ 필터를 통하여 저장조로 이송하여 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제조하는 것이다.It is to prepare a composite composition for a livestock disinfectant with improved insect repellent effect by introducing the raw materials into a stirrer and mixing them at 60 rpm for 30 minutes and then transferring them to a storage tank through a 50 µm filter.
다음의 표 5와 같은 성분으로부터 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제조한다.From the components shown in Table 5 below, a composite composition for a livestock disinfectant with improved pest repellency is prepared.
[표 5]의 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제조하는 과정은 다음과 같다. The process of preparing a composite composition for a livestock disinfectant with improved pest repellent effect in [Table 5] is as follows.
교반기에 적당량의 정제수를 넣고 염화암모늄을 투입하여 완전히 용해시킨 다음 나머지원료를 교반기에 투입한 후 전체 중량이 1kg이 되도록 정제수룰 투입한 후 60rpm 속도로 30분간 혼합한 후 50㎛ 필터를 통하여 저장조로 이송하여 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제조하는 것이다.After adding the appropriate amount of purified water to the stirrer and dissolving it completely by adding ammonium chloride, add the remaining raw materials to the stirrer, add purified water so that the total weight is 1 kg, mix for 30 minutes at a speed of 60 rpm, and then flow through the 50 µm filter to the storage tank. It is to manufacture a composite composition of livestock disinfectant with improved insect repellent effect by transferring.
다음의 표 6과 같은 성분으로부터 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제조한다.From the components shown in Table 6 below, a composite composition for a livestock disinfectant with improved pest repellency is prepared.
[표 6]의 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제조하는 과정은 다음과 같다. The process of preparing a composite composition for a livestock disinfectant with improved pest repellent effect in [Table 6] is as follows.
교반기에 적당량의 정제수를 넣고 염화암모늄을 투입하여 완전히 용해시킨 다음 나머지원료를 교반기에 투입한 후 전체 중량이 1kg이 되도록 정제수룰 투입한 후 60rpm 속도로 30분간 혼합한 후 50㎛ 필터를 통하여 저장조로 이송하여 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제조하는 것이다.After adding the appropriate amount of purified water to the stirrer and dissolving it completely by adding ammonium chloride, add the remaining raw materials to the stirrer, add purified water so that the total weight is 1 kg, mix for 30 minutes at a speed of 60 rpm, and then use a 50 μm filter to store. It is to manufacture a composite composition of livestock disinfectant with improved insect repellent effect by transferring.
다음의 표 7과 같은 성분으로부터 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제조한다.A composite composition for a livestock disinfectant with improved pest repellent effect is prepared from the components shown in Table 7 below.
[표 7]의 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제조하는 과정은 다음과 같다. The process of preparing a composite composition for a livestock disinfectant with improved insect repellent effect in [Table 7] is as follows.
상기 원료를 각각 교반기에 투입한 후 60rpm 속도로 30분간 혼합한 후 50㎛ 필터를 통하여 저장조로 이송하여 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제조하는 것이다.It is to prepare a composite composition for a livestock disinfectant with improved insect repellent effect by introducing the raw materials into a stirrer and mixing them at 60 rpm for 30 minutes and then transferring them to a storage tank through a 50 µm filter.
다음의 표 8과 같은 성분으로부터 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제조한다.From the components shown in Table 8 below, a composite composition for a livestock disinfectant with improved pest repellency is prepared.
[표 8]의 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제조하는 과정은 다음과 같다. The process of preparing a composite composition for a livestock disinfectant with improved pest repellent effect in [Table 8] is as follows.
교반기에 적당량의 정제수를 넣고 염화암모늄을 투입하여 완전히 용해시킨 다음 나머지원료를 교반기에 투입한 후 전체 중량이 1kg이 되도록 정제수룰 투입한 후 60rpm 속도로 30분간 혼합한 후 50㎛ 필터를 통하여 저장조로 이송하여 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제조하는 것이다.After adding the appropriate amount of purified water to the stirrer and dissolving it completely by adding ammonium chloride, add the remaining raw materials to the stirrer, add purified water so that the total weight is 1 kg, mix for 30 minutes at a speed of 60 rpm, and then flow through the 50 µm filter to the storage tank. It is to manufacture a composite composition of livestock disinfectant with improved insect repellent effect by transferring.
다음의 표 9와 같은 성분으로부터 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제조한다.From the components shown in Table 9 below, a composite composition for a livestock disinfectant with improved pest repellency is prepared.
[표 9]의 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제조하는 과정은 다음과 같다. The process of preparing a composite composition for a livestock disinfectant with improved insect repellent effect in [Table 9] is as follows.
교반기에 적당량의 정제수를 넣고 염화암모늄을 투입하여 완전히 용해시킨 다음 나머지원료를 교반기에 투입한 후 전체 중량이 1kg이 되도록 정제수룰 투입한 후 60rpm 속도로 30분간 혼합한 후 50㎛ 필터를 통하여 저장조로 이송하여 해충 기피효과가 개선된 축사용 소독제 복합조성물을 제조하는 것이다.After adding the appropriate amount of purified water to the stirrer and dissolving it completely by adding ammonium chloride, add the remaining raw materials to the stirrer, add purified water so that the total weight is 1 kg, mix for 30 minutes at a speed of 60 rpm, and then flow through the 50 µm filter to the storage tank. It is to manufacture a composite composition of livestock disinfectant with improved insect repellent effect by transferring.
[해충 기피효과가 개선된 축사용 소독제 복합조성물의 구성]
[Composition of composite composition for livestock disinfectant with improved insect repellent effect]
[실험예 1][Experimental Example 1]
1. 실험 방법1. Experimental method
각각의 실시예 조성물 1kg씩을 플라스틱용기(PE)에 분병하여 차광된 실온에서 보관하면서 0, 3, 6, 12개월 후 안정성을 측정하였다.Stability was measured after 0, 3, 6, and 12 months while storing 1 kg of each example composition in a plastic container (PE) and storing at shaded room temperature.
2. 실험 결과2. Experimental results
실시예 1 조성물은 해충 기피성분이 안정한 반면 소독성분이 불안정 하였으며, 실시예 2, 3, 5, 8 조성물은 해충 기피성분뿐만 아니라 소독성분도 불안정하였다. 실시예 4 조성물은 소독성분이 안정한 반면 해충 기피성분이 불안정 하였다. 실시예 6, 7, 9 조성물만이 소독성분과 해충 기피성분이 안정하였다.The composition of Example 1 was stable while the pest repellent component was stable, while the compositions of Examples 2, 3, 5, and 8 were unstable as well as the pest repellent component. The composition of Example 4 had a stable disinfecting component, while the pest repellent component was unstable. Only the compositions of Examples 6, 7, and 9 were stable in disinfection and pest repellent.
각 실시예 조성물의 안정성은 다음의 표 11과 같다.The stability of each example composition is shown in Table 11 below.
(1) Benzalkonium chloride 함량(1) Benzalkonium chloride content
(2) 실시예 1 조성물 : Cinnamic acid 함량, 실시예 2, 4, 5, 6 조성물 : Cinnamaldehyde 함량, 실시예 3, 7, 8, 9 조성물 : Cinnamic alcohol 함량
(2) Example 1 composition: Cinnamic acid content, Examples 2, 4, 5, 6 Composition: Cinnamaldehyde content, Examples 3, 7, 8, 9 Composition: Cinnamic alcohol content
[실험예 2][Experimental Example 2]
1. 실험 방법1. Experimental method
와구모 기피효과 실험은 해충 기피성분의 안정성이 입증된 실시 예 1, 6, 7 및 9조성물에 한하여 실시하였다. 와구모에 감염되지 않은 50 ~ 52주령 갈색산란계를 5마리씩 5개군으로 나누어 완전히 격리된 5개의 케이지에 임의적으로 배치하여 1주간 순치한 후 각 개체에 시험액 10mL씩을 체표면에 골고루 분사하였다. 시험액 분사 10분 후에 각 개체에 와구모 15mg씩을 정확하게 달아 인공감염 시킨 후 1시간, 6시간, 12시간, 24시간 후에 암관이 설치된 플라스틱 통을 이용하여 와구모를 채집하여 와구모의 무게를 측정하여 기피율(채집한 와구모 무게/인공 감염시킨 와구모 무게)을 계산하였다. 시험방법은 다음의 표 12와 같다.Wagumo repellent effect experiments were conducted only in Examples 1, 6, 7 and 9 compositions in which the stability of the pest repellent component was proven. 50-52 week old brown scattered eggs that were not infected with wagumo were divided into 5 groups of 5 animals and placed randomly in 5 completely isolated cages for 1 week, and then 10 mL of test solution was evenly sprayed onto the body surface. After 10 minutes of injection of the test solution, 15mg of each bulb hair is accurately weighed and artificially infected. (Collected Wagmo Weight / Artificially Infected Wagmo Weight) was calculated. The test method is shown in Table 12 below.
2. 실험 결과2. Experimental results
대조군인 A군의 기피효과는 전혀 없었으며 실시 예 1조성물을 처치한 B군은 오구모 기피효과가 미흡하였다. 실시 예 6 및 7조성물을 처치한 C군 및 D군의 와구모 기피효과는 양호하였으며 실시 예 9조성물을 처치한 E군의 와구모 기피효과가 가장 우수하였다.There was no repelling effect of the control group A, and the group B treated with the composition of Example 1 had insufficient repellent effect. The group 6 and 7 treated group C and group D groups had a good repellent effect, and the group 9 treated group E had the best group repellent effect.
각 실시예 조성물의 와구모 기피효과는 다음의 표 13과 같다.The repellent effect of each example composition is shown in Table 13 below.
[미흡: 와구모 기피율 50% 미만, 양호: 와구모 기피율 50~75% 미만, 우수: 와구모 기피율 75% 이상]
[Insufficient: Wagumo repelling rate less than 50%, Good: Wagumo repelling rate less than 50-75%, Excellent: Wagumo repelling rate more than 75%]
상기와 같이 본 발명에 따른 해충 기피효과가 개선된 축사용 소독제 복합조성물은 축사를 소독하기 위하여 사용되는 축산용 소독제에 해충 기피제를 복합 조성하여 안정성이 우수하고, 해충 기피효과를 크게 향상시켜 가축의 질병 발생을 억제하며, 가축의 성장을 저해하는 요소를 미연에 방지하는 동시에 소독력을 크게 향상시킬 수 있어 산업상 이용가능성이 매우 높은 발명인 것이다.
As described above, the composite composition of a livestock disinfectant with improved pest repellent effect according to the present invention is excellent in stability by combining a pest repellent compound with a livestock disinfectant used to disinfect the livestock, thereby improving the insect repellent effect and greatly improving the insect repellent effect. It is an invention that has high industrial applicability because it suppresses disease occurrence and prevents factors that inhibit the growth of livestock, while at the same time significantly improving disinfecting power.
Claims (2)
상기 염화벤잘코늄 5~20중량%, 인산 10~35중량%, 프로필렌글리콜 10~35중량%, 염화암모늄 3~10중량%, 계피알코올 1~8중량% 및 정제수 4~71중량%로 이루어진 것을 특징으로 하는 해충 기피효과가 개선된 축사용 소독제 복합조성물.
Contains Benzalkonium chloride, Phosphoric acid, Propylene glycol, Ammonium chloride, Cinnamyl alcohol and Purified water,
The benzalkonium chloride 5 to 20% by weight, phosphoric acid 10 to 35% by weight, propylene glycol 10 to 35% by weight, ammonium chloride 3 to 10% by weight, cinnamon alcohol 1 to 8% by weight and purified water 4 to 71% by weight A composite composition for livestock disinfectants with improved insect repellent.
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| JP2003534354A (en) * | 2000-05-26 | 2003-11-18 | エコスマート テクノロジーズ，インコーポレーテッド | Non-toxic pest control |
| JP2007500028A (en) | 2003-07-30 | 2007-01-11 | バイオタル リミテッド | Disinfection of contaminated environment |
| KR100865979B1 (en) | 2007-08-08 | 2008-10-29 | 강경종 | Disinfectant lime composition and its preparing method |
| JP2016529252A (en) | 2013-08-07 | 2016-09-23 | サニット テクノロジーズ エルエルシーＳａｎｉｔ Ｔｅｃｈｎｏｌｏｇｉｅｓ ＬＬＣ | Antibacterial disinfectant composition and method for producing the same |
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| KR100935427B1 (en) | 2007-09-29 | 2010-01-11 | 최제영 | Insect repellent |
| KR101295228B1 (en) | 2011-01-05 | 2013-08-09 | 동부팜한농 주식회사 | An insecticidal composition for disinfecting stable and poultry farm |
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| JP2003534354A (en) * | 2000-05-26 | 2003-11-18 | エコスマート テクノロジーズ，インコーポレーテッド | Non-toxic pest control |
| JP2007500028A (en) | 2003-07-30 | 2007-01-11 | バイオタル リミテッド | Disinfection of contaminated environment |
| KR100865979B1 (en) | 2007-08-08 | 2008-10-29 | 강경종 | Disinfectant lime composition and its preparing method |
| JP2016529252A (en) | 2013-08-07 | 2016-09-23 | サニット テクノロジーズ エルエルシーＳａｎｉｔ Ｔｅｃｈｎｏｌｏｇｉｅｓ ＬＬＣ | Antibacterial disinfectant composition and method for producing the same |
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