KR20150077107A - Chemical Vapor Deposition - Google Patents
Chemical Vapor Deposition Download PDFInfo
- Publication number
- KR20150077107A KR20150077107A KR1020130166000A KR20130166000A KR20150077107A KR 20150077107 A KR20150077107 A KR 20150077107A KR 1020130166000 A KR1020130166000 A KR 1020130166000A KR 20130166000 A KR20130166000 A KR 20130166000A KR 20150077107 A KR20150077107 A KR 20150077107A
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- KR
- South Korea
- Prior art keywords
- gas
- showerhead
- process chamber
- susceptor
- supply pipe
- Prior art date
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Classifications
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
- C23C16/455—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for introducing gases into reaction chamber or for modifying gas flows in reaction chamber
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
- C23C16/458—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for supporting substrates in the reaction chamber
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- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Chemical Vapour Deposition (AREA)
Abstract
The present invention relates to a chemical vapor deposition apparatus, which comprises a process chamber, a susceptor for supporting a wafer inside the process chamber, a first process gas and a second process gas which are provided above the susceptor, And a jetting unit disposed in the center of the showerhead for jetting the inert gas radially from the inside toward the outside with respect to the center of the showerhead. to provide.
According to an embodiment of the present invention, a separate injection part is provided below the center of the shower head to uniformly distribute the process gas in the process chamber, thereby achieving uniform deposition of the thin film.
Description
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a chemical vapor deposition apparatus, and more particularly, to a chemical vapor deposition apparatus capable of depositing a uniform thin film by controlling a flow rate while injecting gas injected in a process chamber in a horizontal direction.
Chemical vapor deposition refers to a process of forming a thin film on a substrate using a chemical reaction of the process gas. Accordingly, the chemical vapor deposition apparatus supplies at least one process gas having good reactivity into the chamber, and activates the process gas using light, heat, plasma, microwave, X-ray, electric field, To form a high-quality thin film on the substrate.
A chemical vapor deposition apparatus for performing such a process is a device for manufacturing semiconductor devices and light emitting devices such as OLEDs and LEDs. Specifically, the chemical vapor deposition is performed by sequentially laminating a buffer layer made of GaN crystal, an n-type doping layer made of n-type GaN crystal, and a p-type doping layer made of InGaN by using a nitride material on a substrate or wafer such as sapphire Emitting device.
Such chemical vapor deposition apparatuses include CVD (Chemical Vapor Deposition) and MOCVD (Metalorganic Chemical Vapor Deposition), in which a process gas is sprayed onto a substrate accommodated in the substrate to react the substrate with the process gas, .
Conventionally, there has been a problem in that a uniform thin film deposition can not be performed because the distribution of the process gas inside the chamber injected from the shower head is concentrated to the outside due to the influence of the exhaust pump in the lower part of the chamber.
In order to solve the above-described problems, the present invention has a separate injection part below the center of the showerhead to uniformly distribute the process gas in the process chamber to achieve uniform deposition of the thin film.
The present invention relates to a process chamber, comprising a process chamber, a susceptor for supporting a wafer inside the process chamber, a first supply pipe for supplying a first process gas and a second process gas into the process chamber, And a spraying portion disposed at the center of the showerhead, for spraying the inert gas radially from the inside toward the outside with respect to the center of the showerhead.
The injection unit may include a gas pipe passing through the center of the showerhead and connected to an external supply line, and an injector located below the shower head and injecting the gas supplied from the gas pipe into the process chamber.
In addition, the injector may further include a plurality of ejection openings along a cylindrical outer circumferential surface.
The injection unit may further include a controller for controlling the horizontal velocity of the inert gas injected from the jetting unit so as to control the uniformity of the thin film deposited on the wafer surface.
In addition, the gas pipe penetrates the center of the showerhead, and can function to prevent sagging of the lower part due to the fastening structure with the upper part or the lower part of the shower head.
The first process gas and the second process gas supplied from the first supply pipe and the second supply pipe may be arranged to be injected in the direction of the susceptor.
In addition, the amount of the gas to be injected can be selectively controlled by the first process gas injected from the first supply pipe, the second process gas injected from the second supply pipe, and the inert gas injected from the injection part.
A plasma processing apparatus comprising: a process chamber; a susceptor for supporting a wafer in the process chamber; a first supply pipe provided above the susceptor for supplying a first process gas into the process chamber; And a spraying unit for spraying the process gas in a horizontal direction from the inside to the outside with respect to the center of the showerhead.
The injector may include a gas pipe passing through the center of the showerhead and connected to an external supply line and an injector disposed below the showerhead and injecting the second process gas supplied from the gas pipe into the process chamber have.
The injector may have a control unit for controlling the horizontal velocity of the gas injected from the jetting unit so as to control the uniformity of the thin film deposited on the wafer surface.
Further, a cooling chamber may be provided under the shower head and between the first supply pipe and the second supply pipe to cool the first process gas and the second process gas supplied into the process chamber.
The connection portion of the gas pipe and the injection port may have a curved shape so that the inert gas supplied to the gas pipe or the second process gas can smoothly pass through the injection port.
In addition, the injector may include a diffuser portion that forms a space for supplying inert gas or a second process gas supplied to the gas pipe to the process chamber when the process gas is supplied into the process chamber.
The details of other embodiments are included in the detailed description and drawings.
According to the present invention, the shower head has a separate spray part under the center of the shower head to uniformly distribute the process gas in the process chamber, thereby achieving uniform deposition of the thin film.
In addition, each process gas or inert gas is cross-jetted in different directions to control the wafer surface velocity.
In addition, there is an effect that a tube can be installed inside the shower head to prevent sagging under the shower head.
1 is a cross-sectional view of a chemical vapor deposition apparatus according to an embodiment of the present invention.
2 is a cross-sectional view of a shower head and an injection part of a chemical vapor deposition apparatus according to an embodiment of the present invention.
3 is a cross-sectional view illustrating a showerhead and a spraying unit of a chemical vapor deposition apparatus according to another embodiment of the present invention.
FIG. 4 is an exploded perspective view of a showerhead and an injection unit according to another embodiment of the present invention. FIG.
Hereinafter, a chemical vapor deposition apparatus according to an embodiment of the present invention will be described in detail with reference to the accompanying drawings.
In this embodiment, a description will be given of a chemical vapor deposition process using a process gas containing an organic metal compound (Metal Organic Chemical Vapor Deposition). However, the present invention is not limited thereto and can be applied to a chemical vapor deposition process apparatus using various process gases.
A chemical vapor deposition apparatus includes a process chamber, a susceptor for supporting the wafer inside the process chamber, a showerhead disposed above the susceptor, for spraying the first process gas toward the susceptor into the process chamber, And a jetting unit for jetting the second process gas in a horizontal direction from the inside to the outside with respect to the center of the showerhead.
The showerhead or jetting portion described above may be a first supply pipe or a second supply pipe, and the process gas supplied to each showerhead or jetting portion may be a first process gas, a second process gas, or an inert gas.
1 is a cross-sectional view of a chemical vapor deposition apparatus according to an embodiment of the present invention.
1, a chemical
The
The
The
The
A
The
The
As in the present embodiment, MOCVD using a process gas using an organometallic compound is generally performed by using a hydride gas containing a Group 5 element such as ammonia (NH 3) and a trivalent element such as tri-metal gallium It is preferable to use an organometallic compound such as trimethylgallium (TMGa), trimethyl-indium (TMI), or trimethyl-aluminum (TMA).
Accordingly, a separate supply pipe for separately supplying the Group 3 gas and the Group 5 gas is connected to the
When the
2 is a cross-sectional view of a showerhead according to an embodiment of the present invention.
1 and 2, a
A space for receiving the first process gas G1 and the second process gas G2, which are introduced from the external gas line, may be formed above the
The
A plurality of
The
A plurality of
A plurality of
Specifically, the
And an
The
The
The
As the substrate becomes larger, the configuration of the
The gas pipe (310) penetrates the center of the showerhead (200) and forms a fastening structure with the showerhead (200) so as to prevent breakage due to sagging and damage of internal equipment.
That is, the
At this time, the
The upper surface of the
A rotary motor (not shown) may be disposed between the lower part of the
Also, the
The inert gas G3 supplied from the external line can move smoothly because the connection portion between the
The
The
The
The inert gas G3 whose supply amount or velocity component is controlled by the
The
The
In addition, it is preferable that the
The
Specifically, the inert gas G3 transferred from the
According to the embodiment, the
The jetting
That is, the inert gas G3 injected from the
Since the inert gas G3 injected in the horizontal direction blows toward the
That is, since the inert gas G3 injected from the jetting
In addition, the position of the
Specifically, an exhaust pump (not shown) is disposed below the
However, in the case of the present invention, the jetting
Therefore, according to the present invention, due to a process in which the density distribution of the process gas in the
Therefore, the uniformity of the thin film deposited on the wafer S placed on the upper surface of the
The cooling
The cooling
The first and
In addition, an inlet and an outlet may be provided so that the refrigerant can flow into and circulate in the
The inert gas G3 or the second process gas G2 supplied to the gas pipe is supplied to the
The
The inert gas G3 supplied from the
In this embodiment, the first process gas G1 is supplied to the
3 is a cross-sectional view of a shower head according to another embodiment of the present invention.
1 and 3, the
A space for receiving the first process gas G1 introduced from the external gas line may be formed on the
It is also possible to constitute the
The
A plurality of
In addition, a
That is, a
3, the jetting
The
The second process gas G2 injected from the
Specifically, since the second process gas G2 is injected in the horizontal direction from the inner side to the outer side of the lower surface of the
Therefore, the process gas may be deposited on the periphery of the lower surface of the
As described above, the first and second process gases G1 and G2 are biased toward the outside of the
Accordingly, the deposition of the thin film having improved uniformity can be performed according to the structure of the
FIG. 4 is an exploded perspective view of a showerhead and a spraying unit of a chemical vapor deposition apparatus according to another embodiment of the present invention. FIG.
However, the description of the configuration corresponding to the previous embodiment will be omitted in order to avoid duplication.
The opening portions of the
Further, the structure of the bottom portion of the
At this time, the
The inert gas G3 injected into the
While the present invention has been described in connection with what is presently considered to be practical exemplary embodiments, it is to be understood that the invention is not limited to the disclosed embodiments, but, on the contrary, . Therefore, it should be understood that the above-described embodiments are illustrative in all aspects and not restrictive. The scope of the present invention is defined by the appended claims rather than the detailed description and all changes or modifications derived from the meaning and scope of the claims and their equivalents are to be construed as being included within the scope of the present invention do.
Process chamber: 100 Showerhead: 200
First supply pipe: 210 Second supply pipe: 230
Delivery Division: 300 Gas Pipes: 310
Injector: 330 nozzle: 350
Susceptor: 400 wafers: S
First process gas: G1 Second process gas: G2
Inert gas: G3 Diffuser part: 340
Control section: 360
Claims (14)
A susceptor for supporting the wafer inside the process chamber;
A showerhead disposed above the susceptor and having a first supply pipe and a second supply pipe for supplying a first process gas and a second process gas into the process chamber; And
And a jetting portion disposed at the center of the showerhead for jetting an inert gas radially from the inside to the outside with respect to the center of the showerhead.
Wherein the jetting portion passes through the center of the showerhead and is connected to an external supply line,
And an injector disposed under the shower head and injecting the inert gas supplied from the gas pipe into the process chamber.
Wherein the injector further comprises a plurality of ejection openings along a cylindrical outer circumferential surface.
Wherein the jetting unit further comprises a control unit for controlling the horizontal velocity of the inert gas jetted from the jetting unit so as to control the uniformity of the thin film deposited on the surface of the wafer.
Wherein the first process gas and the second process gas supplied from the first supply pipe and the second supply pipe are arranged to be injected in the direction of the susceptor.
Characterized in that the amount of the gas injected from the first process gas injected from the first supply pipe, the second process gas injected from the second supply pipe, and the inert gas injected from the injection part can be selectively controlled A chemical vapor deposition apparatus.
And a cooling chamber provided between the lower portion of the showerhead and the first supply pipe and the second supply pipe to cool the first process gas and the second process gas supplied into the process chamber, .
Wherein the connection portion of the gas pipe and the injection port has a curved shape so that the inert gas supplied to the gas pipe can smoothly pass through the injection port.
And a diffuser part for forming a uniform space for uniform thin film deposition inside the injector.
A susceptor for supporting the wafer inside the process chamber;
A showerhead disposed above the susceptor and having a first supply pipe for supplying a first process gas into the process chamber; And
And a jetting portion disposed at the center of the showerhead for jetting a second process gas in a horizontal direction from the inside to the outside with respect to the center of the showerhead.
Wherein the jetting portion passes through the center of the showerhead and is connected to an external supply line,
And an injector disposed below the showerhead and injecting the second process gas supplied from the gas pipe into the process chamber.
Wherein the injector has a control unit for controlling the horizontal velocity of the gas injected from the jetting unit so as to control the uniformity of the thin film deposited on the surface of the wafer.
Wherein the gas pipe passes through the center of the showerhead and is fastened to the upper or lower portion of the showerhead to prevent sagging of the bottom of the showerhead.
A susceptor for supporting the wafer inside the process chamber;
A showerhead installed above the susceptor and injecting a first process gas into the process chamber toward the susceptor; And
And a spraying portion disposed at the center of the showerhead for spraying gas in a horizontal direction toward the outside from the center portion of the showerhead.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR1020130166000A KR20150077107A (en) | 2013-12-27 | 2013-12-27 | Chemical Vapor Deposition |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR1020130166000A KR20150077107A (en) | 2013-12-27 | 2013-12-27 | Chemical Vapor Deposition |
Publications (1)
Publication Number | Publication Date |
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KR20150077107A true KR20150077107A (en) | 2015-07-07 |
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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KR1020130166000A KR20150077107A (en) | 2013-12-27 | 2013-12-27 | Chemical Vapor Deposition |
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KR (1) | KR20150077107A (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109457236A (en) * | 2019-01-04 | 2019-03-12 | 中晟光电设备(上海)股份有限公司 | A kind of air inlet top plate and metal-organic chemical vapor deposition equipment reactor |
CN114622182A (en) * | 2020-12-10 | 2022-06-14 | 中国科学院微电子研究所 | Shower nozzle and have its chemical vapor deposition device |
-
2013
- 2013-12-27 KR KR1020130166000A patent/KR20150077107A/en not_active Application Discontinuation
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109457236A (en) * | 2019-01-04 | 2019-03-12 | 中晟光电设备(上海)股份有限公司 | A kind of air inlet top plate and metal-organic chemical vapor deposition equipment reactor |
CN114622182A (en) * | 2020-12-10 | 2022-06-14 | 中国科学院微电子研究所 | Shower nozzle and have its chemical vapor deposition device |
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