KR20140012911A - Method for extracting rubus coreanus miquel, method for preparing drink and tablet containing the same - Google Patents

Method for extracting rubus coreanus miquel, method for preparing drink and tablet containing the same Download PDF

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KR20140012911A
KR20140012911A KR1020130147831A KR20130147831A KR20140012911A KR 20140012911 A KR20140012911 A KR 20140012911A KR 1020130147831 A KR1020130147831 A KR 1020130147831A KR 20130147831 A KR20130147831 A KR 20130147831A KR 20140012911 A KR20140012911 A KR 20140012911A
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extract
rubus coreanus
fruits
stirring
brambles
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KR101468625B1 (en
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권찬명
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농업회사법인 주식회사 헬스페이스
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/02Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
    • A23L2/04Extraction of juices
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/02Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
    • A23L2/08Concentrating or drying of juices
    • A23L2/12Concentrating or drying of juices by freezing
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/385Concentrates of non-alcoholic beverages
    • A23L2/39Dry compositions
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/70Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
    • A23L2/72Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by filtration
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/15Vitamins

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  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Non-Alcoholic Beverages (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)

Abstract

The present invention relates to a rubus coreanus fruit extracting method and a method for producing beverages and tablets containing rubus coreanus fruits and more specifically, to a rubus coreanus fruit extracting method capable of obtaining extracts and extracted powder from rubus coreanus fruits which facilitates the ingestion of valid components of rubus coreanus fruits; and a method for producing beverages and tablets containing rubus coreanus fruits which produces beverages and tablets containing the valid components which facilitate the ingestion of valid components of rubus coreanus fruits and strengthens vitamins and other nutritional contents by adding extracts of oranges and onions. The rubus coreanus fruit extracting method according to the present invention includes a freezing step removing some of moisture by freezing rubus coreanus fruits at a temperature of -30°C for 30 minutes; a grinding step grinding the frozen rubus coreanus fruits which some of the moisture is removed; a sorting step sorting particles of a 48 mesh by filtering the ground rubus coreanus fruits with a filter; a stirring step stirring the sorted ground rubus coreanus fruits; a refrigerating step refrigerating the stirred rubus coreanus fruits at a room temperature for 5-7 days; a centrifugal filtration step centrifugally filtering the refrigerated materials and obtaining rubus coreanus fruit extracts; and a sterilization and filtration step sterilizing and filtering the centrifugally filtered extracts. [Reference numerals] (AA) Rubus coreanus fruits/oranges/onions; (BB) Rubus coreanus fruit extract orange extract onion extract; (S101,S101',S101'') Freeze-drying; (S102,S102',S102'') Pulverizing; (S103.S103',S103'') Apple; (S104,S104'.S104'') Stirring; (S105,S105',S105'') Cooling and settling; (S106,S106',S106'') Centrifugation;

Description

복분자의 추출 방법, 복분자 함유 음료 및 정제의 제조 방법{METHOD FOR EXTRACTING RUBUS COREANUS MIQUEL, METHOD FOR PREPARING DRINK AND TABLET CONTAINING THE SAME}FIELD OF THE INVENTION [0001] The present invention relates to a method for extracting bokbunja, a method for producing a bokbunja-containing beverage,

본 발명은 복분자의 추출 방법, 복분자 함유 음료 및 정제의 제조 방법에 관한 것으로, 보다 상세하게는 복분자의 유효성분을 섭취가 용이하게 하는 복분자 추출액 및 추출 분말을 얻을 수 있는 복분자의 추출 방법과, 복분자의 유효성분을 섭취가 용이한 음료 및 정제 형태로 제조하되 오렌지 및 양파 추출물을 첨가함으로써 비타민류와 기타 영양성분을 보강할 수 있는 복분자가 함유된 음료 및 정제를 제조할 수 있는 복분자 함유 음료 및 정제의 제조 방법에 관한 것이다.The present invention relates to a method for extracting bokbunja, a method for producing a bokbunja containing beverages and tablets, and more specifically, bokbunja extract and extract powder to obtain the bokbunja active ingredient easy to ingest the active ingredient of bokbunja, and bokbunja Bokbunja-containing beverages and tablets, which can be prepared in the form of beverages and tablets that can be easily consumed, but can be prepared with beverages and tablets containing bokbunja that can supplement vitamins and other nutrients by adding orange and onion extracts. It relates to a method for producing.

복분자(Rubus coreanus Miquel)는 식용으로 뿐만 아니라 예로부터 한방에서 덜 익은 복분자과일을 건조시켜 약재로 사용되고 있으며, 동의보감에 의하면 신정, 신 및 간을 보호하고 눈을 밝게 하며 스테미너 증진에 효과가 있는 것으로 알려져 있으며, 맛이 달고 독이 없으며, 붉은색을 띠고 있어 적용되는 식품에 따라 기호성을 높일 수 있는 가공식품용 재료로 적용가능할 뿐만 아니라, 최근에는 항암활성 및 면역증진효과, 항산화 및 항균활성, 헤파티티스 비 바이러스(Hepatitis B virus) 억제 등 다양한 생리활성기능을 가진 것으로 알려지고 있다.Rubus coreanus Miquel is used as a medicinal herb by drying berry fruit not only in edible form but also in one way, and according to Donguibogam, it is known to protect the newborn, god and liver, brighten the eyes and improve stamina. And it is not only poisonous, but also has a red color. Therefore, it can be applied as a material for processed food which can enhance the palatability according to the applied food. In addition, it has recently been applied to anticancer activity and immunity enhancing effect, antioxidant and antimicrobial activity, And hepatitis B virus (HBV) suppression.

이상에서 살펴본 바와 같이 복분자의 성분, 효능에 대해서는 많은 것들이 밝혀지고 있으나, 복분자의 가공제품화와 관련되어 주로 복분자주(酒)의 품질 고급화를 위한 연구에 집중되어 있을 뿐, 특별히 복분자를 이용하여 상업적인 식품화 개발이 거의 이루어지지 않은 실정이다.As described above, many of the components and efficacy of the bokbunja have been clarified. However, it has been focused mainly on the research for quality upgrading of bokbunjaju (liquor) in connection with the commercialization of the bokbunja. In particular, Development has been hardly achieved.

최근 고창군 부안농협에서는 복분자즙 제품을 개발하여 생산, 판매하고 있으나, 상기 복분자즙 제품은 원료 고유의 적색 색상을 충분히 발현시키지 못하였고 음용시 신맛이 강할 뿐 아니라 음용 후 떫은맛이 느껴지는 등 제품의 품질 개선이 절실히 요구되고 있으며, 주요 소비층도 장년층으로 국한되고 있는 것으로 조사됨에 따라 기존의 장년층뿐만 아니라 젊은층에 이르기까지 소비계층의 폭을 넓힐 수 있는 대중적인 식품의 개발이 요청되고 있다. Recently, the Buan Agricultural Cooperative in Gochang County has developed and produced bokbunja juice, but the bokbunja juice did not sufficiently express the original red color of the raw material. And the major consumers are confined to the elderly, it is required to develop a popular food that can broaden the range of consumers from the old to the young.

본 발명은 상기와 같은 점을 인식하여 안출된 것으로 본 발명의 목적은 복분자의 유효성분을 섭취가 용이하게 하는 복분자 추출액 및 추출 분말을 얻을 수 있는 복분자의 추출 방법을 제공하기 위한 것이다.The present invention has been made in view of the above point is an object of the present invention is to provide a method for extracting bokbunja extract to obtain the bokbunja extract and extract powder to facilitate the ingestion of the active ingredient of bokbunja.

아울러 본 발명의 또 다른 목적은, 복분자의 유효성분을 섭취가 용이한 음료 및 정제 형태로 제조하되 오렌지 및 양파 추출물을 첨가함으로써 비타민류와 기타 영양성분을 보강할 수 있는 복분자가 함유된 음료 및 정제를 제조할 수 있는 복분자 함유 음료 및 정제의 제조 방법을 제공하기 위한 것이다.In addition, another object of the present invention is to prepare an active ingredient of bokbunja in easy-to-drink beverages and tablets in the form of beverages and tablets containing bokbunja that can reinforce vitamins and other nutrients by adding orange and onion extract To provide a method for producing bokbunja containing beverages and tablets that can be prepared.

상기와 같은 목적을 달성하고자 본 발명에 따른 복분자의 추출 방법은, 복분자를 -30℃의 온도로 30분간 냉동시켜 수분의 일부를 제거하는 냉동단계와, 수분의 일부가 제거된 냉동된 복분자를 분쇄하는 분쇄단계와, 복분자 분쇄물을 체로 걸러 48mesh의 입자를 선별하는 사과단계와, 사과된 분쇄물을 교반하는 교반단계와, 교반된 재료 분쇄물을 실온에서 5~7일간 냉침하는 냉침단계와, 냉침된 재료를 원심분리하여 복분자추출액을 얻는 원심분리단계와, 원심분리된 추출액을 살균시키고 여과하는 제균 및 여과단계를 포함하는 것을 특징으로 한다.To achieve the above object, the present invention provides a bacterium extracting method comprising: a freezing step of freezing brambles at a temperature of -30 DEG C for 30 minutes to remove a part of water; and a step of crushing frozen brambles, An apple step for screening the particles of 48mesh by sieving the crushed brambled material, a stirring step for stirring the pulverized material, a cooling step for cooling the pulverized material at room temperature for 5 to 7 days, A centrifugation step of centrifuging the frozen material to obtain a brambly extract, and a sterilization and filtration step of sterilizing and filtering the centrifuged extract.

또한, 본 발명에 따른 복분자의 추출 방법은, 복분자를 -30℃의 온도로 30분간 냉동시켜 수분의 일부를 제거하는 냉동단계와, 수분의 일부가 제거된 냉동된 복분자를 분쇄하는 분쇄단계와, 복분자 분쇄물을 체로 걸러 48mesh의 입자를 선별하는 사과단계와, 사과된 분쇄물을 교반하는 교반단계와, 교반된 재료 분쇄물을 실온에서 5~7일간 냉침하는 냉침단계와, 냉침된 재료를 원심분리하여 복분자추출액을 얻는 원심분리단계와, 원심분리된 복분자추출액을 -30℃의 온도로 급속 냉각시켜 함수율이 5%가 되도록 동결건조시키는 동결건조단계와, 동결건조된 추출 고형물을 분쇄하는 단계와, 분쇄된 추출물을 살균하고 150~200mesh 입자크기의 추출분말을 얻는 제균 및 사과단계를 포함하는 것을 특징으로 한다.The method of extracting brambles according to the present invention includes a freezing step of freezing brambles at a temperature of -30 DEG C for 30 minutes to remove a part of water, a grinding step of grinding frozen brambles with a part of water removed, An apple step for screening 48 meshes of particles of crushed macromolecule, a stirring step for stirring the pulverized material, a cooling step for cooling the agitated material for 5 to 7 days at room temperature, A lyophilizing step of rapidly lyophilizing the centrifuged bramblor extract at a temperature of -30 DEG C to give a water content of 5%; and a step of pulverizing the lyophilized extract solid And an eradication and apple step of sterilizing the pulverized extract to obtain an extract powder having a particle size of 150 to 200 mesh.

또한, 본 발명에 따른 복분자함유 음료의 제조 방법은, 상기의 방법으로 추출된 복분자추출액과, 오렌지 추출액 및 양파추출액을 배합하여 혼합 용액을 제조하는 배합단계와, 혼합 용액을 원심분리하여 침전물과 부유물로부터 분리된 액상을 분리하는 원심분리단계와, 비타민 C, 구연산, 향료 첨가물을 첨가하여 혼합하는 혼합단계와, 첨가물이 혼합된 용액을 여과하는 여과단계와, 여과 용액을 살균하고 냉각시키는 살균 및 냉각단계를 포함하는 것을 특징으로 한다.The method for producing a berry containing drink according to the present invention comprises a mixing step of blending an extract of brambles extracted with the above method with an orange extract and an onion extract to prepare a mixed solution and a step of centrifuging the mixed solution to obtain a precipitate and a suspension A step of adding a vitamin C, a citric acid, and an additive of flavor to the mixture, a step of filtering the solution mixed with the additive, a step of sterilizing and cooling the filtrate, The method comprising the steps of:

또한, 본 발명에 따른 복분자 함유 정제의 제조 방법은, 상기의 방법으로 추출된 복분자추출분말과, 오렌지추출분말 및 양파추출분말을 배합하여 혼합 용액을 제조하는 배합단계와, 혼합 용액을 균질화시키는 균질화단계와, 균질화된 혼합 용액에 첨가물 및 부형제를 첨가하여 혼합하는 혼합단계와, 첨가물이 혼합된 용액에 유기용매를 혼합하여 교반하는 혼합 및 교반단계와, 교반된 혼합 용액을 감압으로 농축시켜 농축된 용액으로 정제를 성형하는 농축 및 성형단계를 포함하는 것을 특징으로 한다.The method for producing a bacterium-containing tablet according to the present invention comprises a mixing step of mixing a bacterium extract powder extracted with the above method with an orange extract powder and an onion extract powder to prepare a mixed solution, Mixing and mixing the organic solvent with the solution mixed with the additives, stirring and mixing the mixed solution with the organic solvent, and concentrating the mixture with the reduced pressure to concentrate the mixture And a concentrating and forming step of forming the tablet into a solution.

상기와 같은 구성에 의하여 본 발명에 따른 복분자 추출 방법은 복분자의 유효성분을 섭취가 용이하게 하는 복분자 추출액 및 추출 분말을 얻을 수 있는 장점을 갖는다.The bokbunja extraction method according to the present invention by the configuration as described above has the advantage to obtain the bokbunja extract and extract powder to facilitate the ingestion of the active ingredient of bokbunja.

아울러 본 발명에 따른 복분자 함유 음료 및 정제의 제조 방법은 복분자의 유효성분을 섭취가 용이한 음료 및 정제 형태로 제조하되 오렌지 및 양파 추출물을 첨가함으로써 비타민류와 기타 영양성분을 보강할 수 있는 복분자가 함유된 음료 및 정제를 제조할 수 있는 장점을 갖는다.In addition, the method for producing bokbunja-containing beverages and tablets according to the present invention is prepared in the form of beverages and tablets easy to consume the active ingredient of bokbunja but bokbunja who can reinforce vitamins and other nutrients by adding orange and onion extract It has the advantage of being able to produce contained beverages and tablets.

도 1은 오렌지/양파 추출액을 추출하는 과정을 포함하여 본 발명의 일실시예에 따른 복분자의 추출 방법을 도시한 흐름도
도 2는 도 1에 도시된 복분자 추출 방법에 의해 얻은 추출액을 이용하여 복분자 함유 음료의 제조 방법을 도시한 흐름도
도 3은 오렌지/양파 추출분말을 제조하는 과정을 포함하여 본 발명의 다른 실시예에 따른 복분자의 추출 방법을 도시한 흐름도
도 4는 도 3에 도시된 복분자의 추출 방법에 의해 얻은 추출분말을 이용하여 복분자 함유 정제의 제조 방법을 도시한 흐름도
FIG. 1 is a flowchart illustrating a method of extracting brambles according to an embodiment of the present invention, including a process of extracting orange / onion extracts.
Fig. 2 is a flow chart showing a method for producing a brambled beverage containing drink using the extract obtained by the brambler extraction method shown in Fig. 1
FIG. 3 is a flow chart illustrating a method of extracting brambles according to another embodiment of the present invention, including a process of preparing orange / onion extract powder.
FIG. 4 is a flow chart showing a method for producing a bacterium-containing tablet using the extracted powder obtained by the brambler extraction method shown in FIG.

이하에서는 도면 및 실시예를 참조하여 본 발명에 따른 복분자의 추출 방법, 복분자 함유 음료 및 정제의 제조 방법을 보다 상세하게 설명하기로 한다.Hereinafter, a method for extracting brambles according to the present invention, a method for producing a brambled beverage, and a method for producing tablets will be described in detail with reference to the drawings and examples.

도 1은 오렌지/양파 추출액을 추출하는 과정을 포함하여 본 발명의 일실시예에 따른 복분자의 추출 방법을 도시한 흐름도이다. 이하의 <실시예1>은 도 1에 도시된 복분자 추출 방법에 따라 복분자 추출액을 얻는 과정을 설명한 것이다. 다만, 설명의 편의를 위해 실시예1에서는 복분자 추출액과 함께 오렌지 추출액 및 양파 추출액을 얻는 과정을 동시에 설명하기로 한다.1 is a flowchart illustrating a method of extracting brambles according to an embodiment of the present invention, including a process of extracting orange / onion extracts. The following <Example 1> describes a process of obtaining the brambler extract according to the brambles extraction method shown in FIG. For convenience of explanation, the process of obtaining the orange extract and the onion extract together with the bokbunja extract in Example 1 will be explained at the same time.

<실시예1 : 복분자추출액, 오렌지추출액 및 양파추출액 제조>&Lt; Example 1: Preparation of bokbunja extract, orange extract and onion extract >

복분자추출액/오렌지추출액/양파추출액 각각은 다음과 같은 과정을 거쳐 제조된다.Each of the bokbunja extract / orange extract / onion extract is prepared by the following process.

(1) 냉동단계(S101,S101',S101")(1) refrigeration step (S101, S101 ', S101 ")

재료(복분자, 오렌지, 양파) 각각을 약 -30℃의 온도로 30분간 급냉시키는 단계이다. 이 냉동단계에서는 재료가 동결되면서 냉동건조로 수분을 일부 제거된다.Each of the materials (bokbunja, orange, onion) is quenched at a temperature of about -30 캜 for 30 minutes. In this freezing step, the material is frozen and some moisture is removed by freeze drying.

(2) 분쇄단계(S102,S102',S102")(2) Grinding steps (S102, S102 ', S102 ")

냉동된 재료 각각을 분쇄기로 분쇄하는 단계이다.And crushing each of the frozen materials with a crusher.

(3) 사과단계(S103,S103',S103")(3) Apple stage (S103, S103 ', S103 ")

재료 분쇄물 각각을 체(Sieve)로 걸러 일정 크기 이하의 입자로 선별하는 단계이다. 이 사과단계에서는 다음 단계의 원활한 진행을 위해 선별된 재료 분쇄물은 그 입자가 48mesh 정도가 적당하다.Each of the material crushed materials is sieved and sorted into particles of a certain size or smaller. In order to proceed smoothly in the next step of the apple stage, the selected material pulverized material has a particle size of about 48 mesh.

(4) 교반단계(S104,S104',S104")(4) Stirring step (S104, S104 ', S104 ")

재료 분쇄물의 입자가 고르게 섞이도록 교반하는 단계이다.Stirring is performed so that the particles of the material pulverized material are evenly mixed.

(5) 냉침단계(S105,S105',S105")(5) Cooling step (S105, S105 ', S105 ")

교반된 재료 분쇄물을 실온(18±2℃)에서 5~7일(day)간 냉침하는 단계이다. 실온에서 충분히 냉침되는 과정에서 재료 분쇄물은 수분이 녹으면서 침전물이 액체의 하부로 침전이 진행된다.The agitated material is cooled down at room temperature (18 ± 2 ℃) for 5 ~ 7 days (day). In the process of sufficiently cooling at room temperature, the material crushed material is dissolved in water, and the precipitate proceeds to the bottom of the liquid.

(6) 원심분리단계(S106,S106',S106")(6) Centrifugation step (S106, S106 ', S106 ")

냉침된 재료 각각을 원심분리기로 원심분리(1200~1500rpm, 1분~1분30초)하여 복분자추출액, 오렌지추출액 및 양파추출액 각각을 얻는 단계이다.Each of the frozen materials is centrifuged (1200 to 1500 rpm, 1 minute to 1 minute 30 seconds) using a centrifuge to obtain brambles, orange extracts, and onion extracts.

(7)제균 및 여과단계(S107,S107',S107")(7) Erosion and filtration steps (S107, S107 ', S107 ")

원심분리된 추출액 각각을 살균시키고 여과하는 단계이다. 살균은 원심분리된 추출액을 복사열로 가열하여 이루어지고, 여과는 여과지로 화선지를 사용하여 원심분리된 추출액을 실온에서 3일(day) 정도 여과하여 이루어진다.
And sterilizing and filtering each of the centrifuged extracts. The sterilization is performed by heating the centrifuged extract with radiant heat, and the filtration is performed by filtering the extract which is centrifuged using a filter paper as filter paper for about 3 days at room temperature.

도 2는 도 1에 도시된 복분자 추출 방법에 의해 얻은 추출액을 이용하여 복분자 함유 음료의 제조 방법을 도시한 흐름도이다. 이하의 <실시예2>에서 도 2에 도시된 방법에 따라 복분자 함유 음료를 제조하는 과정을 설명한다.FIG. 2 is a flow chart showing a method for producing a bacterium-containing beverage using the extract obtained by the bacterium extraction method shown in FIG. In the following <Example 2>, a process for producing a bokbunja-containing beverage according to the method shown in FIG. 2 will be described.

<실시예2 : 복분자 함유 혼합음료의 제조>&Lt; Example 2: Preparation of mixed drink containing bokbunja >

(1) 추출액 제조 단계(S10,S10',S10")(1) Extraction liquid manufacturing step (S10, S10 ', S10 ")

상기 실시예1의 과정을 거쳐 재료(복분자, 오렌지, 양파)로부터 복분자 추출액, 오렌지추출액 및 양파추출액을 얻는 단계이다.(Bokbunja, orange, onion), orange extract, and onion extract through the process of Example 1 above.

(2) 배합단계(S20)(2) Mixing step (S20)

상기 복분자추출액, 오렌지추출액, 양파추출액, 정제수를 배합하여 혼합하여 혼합용액을 얻는 단계이다. 배합비는 복분자추출액:오렌지추출액:양파추출액:정제수=20:10:10:50(부피비)이며, 이 배합단계에서 액상과당이 소량(혼합용액 전체 대비 약2~3부피% 정도) 첨가된다.An orange extract, an onion extract, and purified water are mixed and mixed to obtain a mixed solution. The mixing ratio is as follows: brambone extract: orange extract: onion extract: purified water = 20:10:10:50 (volume ratio). In this mixing step, a small amount of liquid fructose is added (about 2 to 3 vol.

(3) 원심분리단계(S30)(3) Centrifugation step (S30)

혼합 용액을 원심분리기로 원심분리(1200~1500rpm, 1분~1분30초)하여 하층의 침전물과 상층의 부유물을 제거하여 그 침전물과 부유물과 분리된 원심분리액을 얻는 단계이다.The mixed solution is centrifuged (1200 ~ 1500 rpm, 1 minute ~ 1 minute 30 seconds) by centrifuge to remove sediment in the lower layer and suspension in the upper layer to obtain centrifuged liquid separated from the sediment and suspension.

(4) 혼합단계(S40)(4) Mixing step (S40)

원심분리액에 비타민 C, 구연산, 향료 첨가물 등을 첨가하여 혼합하는 단계이다. 비타민 C는 상기 배합단계에서 배합된 정제수 대비 1/5(비타민C 부피/정제수 부피) 정도 첨가되며, 구연산, 향료 등 기타 첨가물은 소량 첨가된다.Adding vitamin C, citric acid, fragrance additives, and the like to the centrifugal separation solution and mixing them. Vitamin C is added in a ratio of 1/5 (volume of vitamin C volume / purified water volume) to the purified water mixed in the mixing step, and a small amount of citric acid, flavor and other additives are added.

(5) 여과단계(S50)(5) Filtration step (S50)

첨가물이 첨가된 용액에 함유된 미세한 입자를 제거하기 위한 공정이다.This is a process for removing fine particles contained in a solution to which an additive is added.

(6) 살균 및 냉각단계(S60)(6) Sterilization and cooling step (S60)

여과된 용액을 순간의 고열로 가열하여 살균하고 냉각시켜 복분자 함유 음료를 얻는 단계이다.The filtered solution is sterilized by heating at a high temperature in an instant, and cooled to obtain a beverage containing a macromolecule.

(7) 포장단계(S70)(7) Packaging step (S70)

제조된 복분자 함유 음료를 용기에 담아 포장하는 단계이다.
Containing brewer's beverage into the container and packing the container.

도 3은 오렌지/양파 추출분말을 제조하는 과정을 포함하여 본 발명의 다른 실시예에 따른 복분자의 추출 방법을 도시한 흐름도이다. 이하의 <실시예3>은 도 3에 도시된 복분자 추출 방법에 따라 복분자 추출분말을 얻는 과정을 설명한 것이다. 다만, 설명의 편의를 위해 실시예1에서는 복분자 추출분말과 함께 오렌지 추출분말 및 양파 추출분말을 얻는 과정을 동시에 설명하기로 한다.FIG. 3 is a flowchart illustrating a method of extracting brambles according to another embodiment of the present invention, including a process of preparing an orange / onion extract powder. <Example 3> described below is a process of obtaining the brambly extract powder according to the brambler extraction method shown in FIG. However, for convenience of explanation, the process of obtaining the orange extract powder and the onion extract powder together with the brambler extract powder will be described in the first embodiment.

<실시예3 : 복분자추출분말, 오렌지추출분말 및 양파추출분말 제조>&Lt; Example 3: Preparation of bramble extract powder, orange extract powder and onion extract powder >

복분자추출분말/오렌지추출분말/양파추출분말 각각은 다음과 같은 과정을 거쳐 제조된다.Each of the brambly extract powder / orange extract powder / onion extract powder is manufactured by the following process.

(1) 냉동단계(P101,P101',P101")(1) Refrigeration step (P101, P101 ', P101 ")

재료(복분자, 오렌지, 양파) 각각을 약 -30℃의 온도로 30분간 급냉시키는 단계이다. 이 냉동단계에서는 재료가 동결되면서 냉동건조로 수분을 일부 제거된다.Each of the materials (bokbunja, orange, onion) is quenched at a temperature of about -30 캜 for 30 minutes. In this freezing step, the material is frozen and some moisture is removed by freeze drying.

(2) 분쇄단계(P102,P102',P102")(2) Grinding step (P102, P102 ', P102 ")

냉동된 재료 각각을 분쇄기로 분쇄하는 단계이다.And crushing each of the frozen materials with a crusher.

(3) 사과단계(P103,P103',P103")(3) Apple stage (P103, P103 ', P103 ")

재료 분쇄물 각각을 체(Sieve)로 걸러 일정 크기 이하의 입자로 선별하는 단계이다. 이 사과단계에서는 다음 단계의 원활한 진행을 위해 선별된 재료 분쇄물은 그 입자가 48mesh 정도가 적당하다.Each of the material crushed materials is sieved and sorted into particles of a certain size or smaller. In order to proceed smoothly in the next step of the apple stage, the selected material pulverized material has a particle size of about 48 mesh.

(4) 교반단계(P104,P104',P104")(4) Stirring step (P104, P104 ', P104 ")

재료 분쇄물의 입자가 고르게 섞이도록 교반하는 단계이다.Stirring is performed so that the particles of the material pulverized material are evenly mixed.

(5) 냉침단계(P105,P105',P105")(5) Cooling step (P105, P105 ', P105 ")

교반된 재료 분쇄물을 실온(18±2℃)에서 5~7일(day)간 냉침하는 단계이다. 실온에서 충분히 냉침되는 과정에서 재료 분쇄물은 수분이 녹으면서 침전물이 액체의 하부로 침전이 진행된다.The agitated material is cooled down at room temperature (18 ± 2 ℃) for 5 ~ 7 days (day). In the process of sufficiently cooling at room temperature, the material crushed material is dissolved in water, and the precipitate proceeds to the bottom of the liquid.

(6) 원심분리단계(P106,P106',P106")(6) Centrifugation step (P106, P106 ', P106 ")

냉침된 재료 각각을 원심분리기로 원심분리(1200~1500rpm, 1분~1분30초)하여 복분자추출액, 오렌지추출액 및 양파추출액 각각을 얻는 단계이다.Each of the frozen materials is centrifuged (1200 to 1500 rpm, 1 minute to 1 minute 30 seconds) using a centrifuge to obtain brambles, orange extracts, and onion extracts.

(7) 동결건조단계(P107,P107',P107")(7) Freeze-drying step (P107, P107 ', P107 ")

원심분리된 추출액 각각을 -30℃의 온도로 급속 냉각시켜 동결건조시키는 단계이다. 동결건조된 추출물은 함수율이 약 5%정도로 건조된다.Each of the centrifuged extracts is rapidly cooled to a temperature of -30 DEG C and lyophilized. The lyophilized extract is dried to a moisture content of about 5%.

(8) 분쇄단계(P108,P108',P108")(8) Grinding step (P108, P108 ', P108 ")

동결건조된 추출 고형물을 분쇄기로 분쇄하는 단계이다.The lyophilized extracted solids are pulverized by a pulverizer.

(9) 제균 및 사과단계(P109,P109',P109")(9) Erosion and apple steps (P109, P109 ', P109 ")

분쇄된 추출물을 살균하고 일정 크기 이하의 입자크기의 추출분말을 얻는 단계이다. 추출분말은 150~200mesh의 입자 크기를 갖는 것이 바람직하다.
Sterilizing the pulverized extract and obtaining an extract powder having a particle size of a certain size or less. The extracted powder preferably has a particle size of 150 to 200 mesh.

도 4는 도 3에 도시된 복분자 추출 방법에 의해 얻은 추출분말을 이용하여 복분자 함유 정제의 제조 방법을 도시한 흐름도이다. 이하의 <실시예4>에서는 도 4에 도시된 방법에 따라 복분자 함유 정제를 제조하는 과정을 설명한다.FIG. 4 is a flowchart showing a method for producing a bacterium-containing tablet using the extracted powder obtained by the brambler extraction method shown in FIG. In the following <Example 4>, a process for producing a bacterium-containing tablet according to the method shown in FIG. 4 will be described.

<실시예4 : 복분자 함유 정제의 제조>&Lt; Example 4: Preparation of a bacterium-containing tablet &

(1) 추출분말 제조 단계(P10,P10',P10")(1) Extraction powder production step (P10, P10 ', P10 ")

상기 실시예3의 과정을 거쳐 재료(복분자, 오렌지, 양파)로부터 복분자추출분말, 오렌지추출분말 및 양파추출분말 얻는 단계이다.(Bokbunja, orange, onion), orange extract powder and onion extract powder through the process of Example 3 above.

(2) 배합단계(P20)(2) Mixing step (P20)

상기 복분자추출분말, 오렌지추출분말, 양파추출분말, 정제수를 배합하여 혼합하여 혼합용액을 얻는 단계이다. 배합비는 복분자추출분말:오렌지추출분말:양파추출분말:정제수=20:10:10:50(중량비)으로 배합된다.The brambled extract powder, orange extract powder, onion extract powder, and purified water are mixed and mixed to obtain a mixed solution. The blending ratio is blended with the bokbunja extract powder: orange extract powder: onion extract powder: purified water = 20: 10: 10: 50 (weight ratio).

(3) 균질화단계(P30)(3) Homogenization step (P30)

혼합 용액을 균질화 장치로 분말이 정제수 내에 균일하게 혼합되도록 혼합시키는 단계이다.The mixed solution is mixed with the homogenizer so that the powder is uniformly mixed in the purified water.

(4) 혼합단계(P40)(4) Mixing step (P40)

균질화된 혼합 용액에 첨가물 및 부형제를 첨가하여 혼합하는 단계이다. 상기 첨가물로는 녹차 추출분말 및 착색료(이산화티타늄, 식용색소 황색5호, 적색3호, 적색40호, 청색1호 등)이 첨가되고, 부형제로는 포도씨유나 팜유가 첨가된다.Adding the additives and excipients to the homogenized mixed solution and mixing them. Green tea extract powder and coloring agent (titanium dioxide, food coloring yellow No. 5, red No. 3, red No. 40, blue No. 1, etc.) are added as the above additives, and grape seed oil or palm oil is added as an excipient.

녹차 추출분말(동서산업)은 상기 정제수 대비 1/5중량비(녹차 추출분말/정제수)로 첨가되며, 착색료는 소량이 첨가된다. 또한, 포도씨유나 팜유는 정제수 대비 혼합 용액 200g당 약 10ml 정도 첨가된다.Green tea extract powder (Dongseo Industrial Co., Ltd.) is added at a weight ratio of 1/5 (green tea extract powder / purified water) to the purified water, and a small amount of coloring agent is added. Grape seed oil or palm oil is added in an amount of about 10 ml per 200 g of the mixed solution of purified water.

(5) 혼합 및 교반단계(P50)(5) Mixing and stirring step (P50)

첨가물이 혼합된 용액에 유기용매(함수 에탄올)를 혼합하여 교반하는 단계이다. 유기용매(함수에탄올)은 혼합 용액 200g당 약 100ml 정도 혼합된다.An organic solvent (hydrous ethanol) is mixed with a solution in which the additives are mixed and stirred. The organic solvent (hydrous ethanol) is mixed with about 100 ml per 200 g of the mixed solution.

(6) 농축 및 성형단계(P60)(6) Concentration and Forming Step (P60)

교반된 혼합 용액을 700mHg, 40℃의 온도로 감압 농축시키고, 농축된 용액으로 정제 형상으로 성형하는 단계이다.The stirred mixed solution is concentrated under reduced pressure at a temperature of 40O &lt; 0 &gt; C and 700mHg, and is formed into a tablet shape with a concentrated solution.

(7) 포장단계(P70)(7) Packaging step (P70)

제조된 복분자 함유 정제를 포장에 담아 포장하는 단계이다.
And packing the produced bacterium-containing tablets into a package.

상기의 실시예에 따라 제조된 복분자 추출물은 복분자를 그대로 이용하지 않고, 복분자로부터 추출된 복분자 추출물을 이용함으로써 복분자가 갖는 기능성 유효 성분을 그대로 활용할 수 있도록 한 것을 특징으로 한다. 특히, 본 발명은 복분자추출물에 오렌지 추출물 및 양파추출물을 혼합하여 비타민류와 기타 영양성분이 보강된 음료나 정제 등의 다양한 제품을 제조할 수 있도록 한 것을 특징으로 한다.The bacterium extract prepared according to the above embodiment is characterized in that the bacterium extract can be utilized as it is by using the bacterium extract extracted from the bacterium without using the bacterium as it is. In particular, the present invention is characterized in that a variety of products such as beverages and tablets reinforced with vitamins and other nutritional components can be prepared by mixing the bokbunja extract with the orange extract and the onion extract.

앞에서 설명되고 도면에 도시된 복분자 추출, 음료 및 정제의 제조 방법은 본 발명을 실시하기 위한 하나의 실시예에 불과하며, 본 발명의 기술적 사상을 한정하는 것으로 해석되어서는 안된다. 본 발명의 보호범위는 이하의 특허청구범위에 기재된 사항에 의해서만 정하여지며, 본 발명의 요지를 벗어남이 없이 개량 및 변경된 실시예는 본 발명이 속하는 기술분야에서 통상의 지식을 가진 자에게 자명한 것인 한 본 발명의 보호범위에 속한다고 할 것이다.The method of producing the bramble extract, beverage and tablet as described above and shown in the drawings is only one embodiment for carrying out the present invention and should not be construed as limiting the technical idea of the present invention. The scope of protection of the present invention is defined only by the matters set forth in the claims below, and the embodiments which have been improved and changed without departing from the gist of the present invention will be apparent to those skilled in the art. It will be said to belong to the protection scope of the present invention.

Claims (4)

복분자를 -30℃의 온도로 30분간 냉동시켜 수분의 일부를 제거하는 냉동단계와,
수분의 일부가 제거된 냉동된 복분자를 분쇄하는 분쇄단계와,
복분자 분쇄물을 체로 걸러 48mesh의 입자를 선별하는 사과단계와,
사과된 분쇄물을 교반하는 교반단계와,
교반된 재료 분쇄물을 실온에서 5~7일간 냉침하는 냉침단계와,
냉침된 재료를 원심분리하여 복분자추출액을 얻는 원심분리단계와,
원심분리된 추출액을 살균시키고 여과하는 제균 및 여과단계를 포함하는 것을 특징으로 하는 복분자의 추출 방법.
A freezing step of freezing the brambles at a temperature of -30 DEG C for 30 minutes to remove a part of water,
A crushing step of crushing frozen brambles having a part of water removed,
An apple stage for screening particles of 48 meshes by sieving crushed bokbun powder,
A stirring step of stirring the pulverized material,
A cold-grinding step of cooling the pulverized material at room temperature for 5 to 7 days,
A centrifugal separation step of centrifugally separating the frozen material to obtain a brambled extract,
A method of extracting brambles comprising the steps of: sterilizing and filtering the centrifuged extract and filtering.
복분자를 -30℃의 온도로 30분간 냉동시켜 수분의 일부를 제거하는 냉동단계와,
수분의 일부가 제거된 냉동된 복분자를 분쇄하는 분쇄단계와,
복분자 분쇄물을 체로 걸러 48mesh의 입자를 선별하는 사과단계와,
사과된 분쇄물을 교반하는 교반단계와,
교반된 재료 분쇄물을 실온에서 5~7일간 냉침하는 냉침단계와,
냉침된 재료를 원심분리하여 복분자추출액을 얻는 원심분리단계와,
원심분리된 복분자추출액을 -30℃의 온도로 급속 냉각시켜 함수율이 5%가 되도록 동결건조시키는 동결건조단계와,
동결건조된 추출 고형물을 분쇄하는 단계와,
분쇄된 추출물을 살균하고 150~200mesh 입자크기의 추출분말을 얻는 제균 및 사과단계를 포함하는 것을 특징으로 하는 복분자의 추출 방법.
A freezing step of freezing the brambles at a temperature of -30 DEG C for 30 minutes to remove a part of water,
A crushing step of crushing frozen brambles having a part of water removed,
An apple stage for screening particles of 48 meshes by sieving crushed bokbun powder,
A stirring step of stirring the pulverized material,
A cold-grinding step of cooling the pulverized material at room temperature for 5 to 7 days,
A centrifugal separation step of centrifugally separating the frozen material to obtain a brambled extract,
Lyophilizing step wherein the centrifuged bramblor extract is rapidly cooled to a temperature of -30 캜 and lyophilized to have a water content of 5%
Pulverizing the lyophilized extract solids,
A method for extracting brambles comprising sterilizing the pulverized extract and obtaining an extract powder having a particle size of 150 to 200 mesh.
제1항의 방법으로 추출된 복분자추출액과, 오렌지 추출액 및 양파추출액을 배합하여 혼합 용액을 제조하는 배합단계와,
혼합 용액을 원심분리하여 침전물과 부유물로부터 분리된 액상을 분리하는 원심분리단계와,
비타민 C, 구연산, 향료 첨가물을 첨가하여 혼합하는 혼합단계와,
첨가물이 혼합된 용액을 여과하는 여과단계와,
여과 용액을 살균하고 냉각시키는 살균 및 냉각단계를 포함하는 것을 특징으로 하는 복분자 함유 음료의 제조 방법.
Mixing a brambled extract extracted by the method of claim 1 with an orange extract and an onion extract to prepare a mixed solution;
A centrifugal separation step of separating the liquid phase separated from the precipitate and suspended matter by centrifuging the mixed solution,
Vitamin C, citric acid, and flavoring additives,
A filtration step of filtering a solution mixed with additives,
And a sterilization and cooling step of sterilizing and cooling the filtration solution.
제2항의 방법으로 추출된 복분자추출분말과, 오렌지추출분말 및 양파추출분말을 배합하여 혼합 용액을 제조하는 배합단계와,
혼합 용액을 균질화시키는 균질화단계와,
균질화된 혼합 용액에 첨가물 및 부형제를 첨가하여 혼합하는 혼합단계와,
첨가물이 혼합된 용액에 유기용매를 혼합하여 교반하는 혼합 및 교반단계와,
교반된 혼합 용액을 감압으로 농축시켜 농축된 용액으로 정제를 성형하는 농축 및 성형단계를 포함하는 것을 특징으로 하는 복분자 함유 정제의 제조 방법.
Mixing an extract of the brambles extracted with the method of claim 2, an orange extract powder and an onion extract powder to prepare a mixed solution;
A homogenization step of homogenizing the mixed solution,
A mixing step of adding and mixing an additive and an excipient into the homogenized mixed solution,
A mixing and stirring step in which an organic solvent is mixed and stirred in a solution in which additives are mixed,
And concentrating and stirring the mixed solution under reduced pressure to form a tablet with a concentrated solution.
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104544047A (en) * 2014-12-11 2015-04-29 张莘蔓 Original orange-flavor buccal tablets prepared from sodium L-ascorbate, and preparation method of buccal tablets
KR102137210B1 (en) * 2019-11-26 2020-07-24 (주)바이오시엠 Methods for extracting compound byproduct of Rubus coreans miquel and their composition containing compound byproducts
KR102155897B1 (en) * 2020-03-06 2020-09-14 (주)바이오시엠 Methods for extracting compound byproduct of Rubus coreans miquel and their composition containing compound byproducts

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KR100533196B1 (en) * 2005-09-22 2005-12-02 임규순 Method for preparing a beverage containing extracts of rubus coreanus miquel

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104544047A (en) * 2014-12-11 2015-04-29 张莘蔓 Original orange-flavor buccal tablets prepared from sodium L-ascorbate, and preparation method of buccal tablets
KR102137210B1 (en) * 2019-11-26 2020-07-24 (주)바이오시엠 Methods for extracting compound byproduct of Rubus coreans miquel and their composition containing compound byproducts
KR102155897B1 (en) * 2020-03-06 2020-09-14 (주)바이오시엠 Methods for extracting compound byproduct of Rubus coreans miquel and their composition containing compound byproducts

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