KR20130116422A - Method for preparing the spherical granules of red ginseng extract concentrates by using micronized red ginseng powder - Google Patents
Method for preparing the spherical granules of red ginseng extract concentrates by using micronized red ginseng powder Download PDFInfo
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Abstract
Description
The present invention relates to a method for producing red ginseng concentrate granules using ultra fine red ginseng powder, more specifically, by applying the ultra fine red ginseng powder to the outside of 100% red ginseng concentrate granules using a fluidized bed coater, The present invention relates to a method for preparing red ginseng concentrate granules using ultra-fine red ginseng powder to prevent the aggregation of red ginseng concentrate granules as much as possible while maintaining a soft texture that is an advantage of ingestion.
Currently, the red ginseng products are differentiated from the existing red ginseng product types such as red ginseng concentrate, round red ginseng, red ginseng powder, red ginseng slices through 'method of producing 100% red ginseng concentrate with only red ginseng concentrate without adding excipients'. It has a high concentration of red ginseng functional ingredient, so the daily intake is very small, and it is easy to carry in the form of granules, so it is easily dissolved in water and is easily consumed. By solving the inconveniences of drinking process, management difficulty of use container, and distribution problem of liquid product, it contributes greatly to the increase of farm income and the improvement of Korean red ginseng by increasing exports. have.
However, the 100% red ginseng concentrate granules according to the prior art have a partial phenomenon of agglomeration of red ginseng concentrate granules during careless storage after disassembling the product in a hot region such as summer or Southeast Asia where humidity and temperature are high. In order to promote domestic consumption and expand exports of red ginseng concentrate granule products, which are proud of, it is necessary to solve such problems such as aggregation.
In general, food or pharmaceutical products use a lot of hygroscopic agents such as hydroxy propyl methyl cellulose (HPMC) to prevent the hygroscopicity of the product, but the characteristics of this product manufactured using only red ginseng as well as the customer's avoidance of food additives In consideration of this, by applying the ultra-fine red ginseng powder to the outside of the red ginseng concentrate granules using a fluidized bed coater, the red ginseng concentrate granules can be prevented as much as possible while maintaining the soft texture of the red ginseng concentrate granules. By doing so, it will be possible to improve the physical properties of 100% red ginseng concentrate granules using ultra-fine red ginseng powder.
Advantages and features of the present invention, and methods for accomplishing the same will become apparent with reference to the embodiments described below in detail in conjunction with the accompanying drawings. And, the terminology used herein is for the purpose of describing particular embodiments only and is not intended to be limiting of the invention. Unless specifically defined otherwise, 'red ginseng' includes ginseng, and 'concentrate granules' includes concentrated liquid rings. do.
Accordingly, an object of the present invention is to use a red ginseng powder having a moisture-proof effect without using a food additive absorbent, such as HPMC, to prevent the aggregation of red ginseng concentrate granules even under high temperature and high humidity conditions. The present invention provides a method for preparing red ginseng concentrate granules.
Another object of the present invention is to apply ultrafine red ginseng powder having a soft texture to the outside of the red ginseng concentrate granules by ultra-crushing the red ginseng powder to maintain the soft texture of the red ginseng concentrate granules to maximize the soft texture. To provide a method for producing red ginseng concentrate granules using fine red ginseng powder.
Red ginseng concentrate granules using ultra-fine red ginseng powder according to the present invention for solving the above problems, while spraying red ginseng concentrate in the form of bottom spray (bottom spray) under fluidized bed drying conditions, red ginseng concentrate through repetitive fluidization A first step of producing a ring (grain); A second step of preparing an ultra-fine red ginseng powder, which is a red ginseng concentrate ring coating material, using an ultra-fine red ginseng powder prepared by an ultra-fine grinder; And a coating content of 1% to 9% of the total red ginseng concentrate ring (grains) by spraying the ultrafine red ginseng powder prepared in the second step into the bottom spray form on the red ginseng concentrate ring (grain) prepared in the first step. It is characterized in that it comprises a third step of manufacturing a red ginseng concentrate ring (grains) to prevent moisture absorption by coating so as to be%.
According to an embodiment of the present invention, the particle size of the red ginseng concentrate ring (grains) is 700-5,000 μm, the particle size of the ultra fine red ginseng powder is 5-100 μm, and the solid content of the ultra fine red ginseng powder solution. The concentration is characterized in that it comprises the step of coating to be 0.1-20%.
The present invention, through the manufacture of 100% red ginseng concentrate granules, to solve the inconvenience of drinking red ginseng concentrate, difficulty in managing the container, and distribution problems of the liquid product, as well as increase the farm household income through promoting domestic consumption of red ginseng In addition, it will greatly contribute to improving the status of Korean red ginseng.
In particular, red ginseng concentrate granules (red ginseng stage) products can be easily prevented due to inadvertent aggregation of red ginseng concentrate granules due to careless storage after disassembly of the product packaging in summer or high temperature and high humidity regions of Southeast Asia. Can greatly contribute to domestic consumption and export expansion.
The effects of the present invention are not limited only to the above-mentioned effects, and other effects not mentioned above will be clearly understood by those skilled in the art from the description of the claims.
1 is a process chart showing the manufacturing step of red ginseng concentrate granules using ultra-fine red ginseng powder according to the present invention.
The present invention is coated with a ginseng or red ginseng ultra-fine powder of 5-100㎛ particle size to 1-9% of the ginseng or red ginseng concentrate ring (grains) weight to maintain a soft texture to the maximum while ingesting red ginseng concentrate ring It relates to a method for producing (grains).
Hereinafter, embodiments of the present invention will be described in more detail with reference to the accompanying drawings in order to describe the present invention in more detail.
Figure 1 shows the manufacturing step (process) of red ginseng concentrate granules using ultra-fine red ginseng powder according to the present invention. As shown in Figure 1, the manufacturing method of the red ginseng concentrate granules using the ultra-fine red ginseng powder according to the present invention comprises the steps of preparing the red ginseng concentrate granules (S11), preparing a red ginseng powder for spraying using the ultra-fine red ginseng powder (S12), and the step (S13) to produce a hygroscopically prevented red ginseng concentrate granules, which will be described in detail for each step.
Manufacture of red ginseng concentrate granules (S11: 1st process)
Sprayed red ginseng with solid content in the range of 10-50% under fluidized bed coating conditions such as suction air temperature 80-150 ℃, spray air pressure 0.5-5.0 bar, charge tube temperature 20-80 ℃, feed rate 5-5,000g / min Red ginseng concentrate granules having a particle size of 700-5,000 μm are prepared through repetitive fluidization while spraying the concentrate in the form of a bottom spray.
Preparation of sprayed red ginseng powder (S12: 2nd process)
After grinding red, red ginseng in the 1st, 2nd and 3rd stages with an air-jet mill, the particle size was analyzed using a particle size analyzer (Mavern, Master sizer). It is prepared by grinding. If the size of the red ginseng powder is 100㎛ or more, there is a problem in product quality due to the rough coating surface and poor texture. Therefore, the size of the red ginseng powder is preferably 8-60 μm.
In addition, the solid concentration of red ginseng powder is suitable in the range of 0.1-20%, preferably 10% is optimal for spraying, at 20% or more to form a porridge, difficult to spray, 0.1% or less is not economical.
Preparation of red ginseng concentrate granules with moisture absorption prevention (S13: 3rd process)
While spraying the red ginseng powder prepared in the first step in the form of a bottom spray to the red ginseng concentrate prepared in the first step, the coating content is in the range of 1-9% of the total weight of the red ginseng concentrate granules, that is, 1%, 3 Coated to%, 6% and 9% to prepare a ginseng concentrate granules with a soft texture and moisture absorption.
Hereinafter, the manufacturing method of the present invention will be described in more detail with reference to Examples, but the scope of the present invention is not limited by the following Examples.
Example 1
Under the fluidized bed coating conditions such as suction air temperature 90 ℃, spray air pressure 2.0 bar, input tube temperature 60 ℃ and injection speed 300g / min, spraying red ginseng concentrate with a solid content of 40% in the form of bottom spray The red ginseng concentrate ring (grain) of 700-5,000㎛ particle size was prepared through repetitive fluidization (first step), and the red ginseng concentrate powder coating material was prepared with 10% solution of red ginseng super fine powder with particle size of 8㎛. It prepared (2nd process). Then, the red ginseng concentrate ring prepared in the first step is coated while spraying a 10% solution (red ginseng concentrate ring coating material) of 8 g of red ginseng ultrafine powder (particles of the red ginseng concentrate ring) prepared in the second step in the form of a bottom spray. The coating content was 3% of the total weight of the red ginseng concentrate ring to prepare a "red ginseng concentrate ring with a soft texture and preventing moisture absorption" (third step).
Example 2
The first step and the second step are the same as in Example 1, the third step is the concentration of red ginseng ultra fine powder having a particle size of 8㎛ prepared in the second step in the red ginseng concentrate ring prepared in the first step 10 While spraying the% solution in the form of a bottom spray (bottom spray), the coating content was coated to 6% of the total weight of the red ginseng concentrate ring to prepare a "red ginseng concentrate ring with a soft texture and preventing moisture absorption."
Example 3
The first step and the second step are the same as in Example 1, the third step is the concentration of red ginseng ultra fine powder having a particle size of 8㎛ prepared in the second step in the red ginseng concentrate ring prepared in the first step 10 While spraying the% solution in the form of a bottom spray (bottom spray) coating was coated so that the coating content is 9% of the total weight of the red ginseng concentrate ring to prepare a "red ginseng concentrate ring with a soft texture and preventing moisture absorption."
Example 4
The first step was the same as in Example 1, the second step was to prepare a red ginseng concentrate ring coating material with a concentration of 10% red ginseng ultra fine powder having a particle size of 20㎛, the third step was While spraying 10% solution of red ginseng ultra fine powder with particle size of 20㎛ prepared in the second process into bottom spray form, 3% of the total weight of red ginseng concentrate ring Coated to prepare a "red ginseng concentrate ring with a soft texture, preventing moisture absorption".
Example 5
The first step and the second step are the same as in Example 4, the third step is the concentration of red ginseng ultrafine powder having a particle size of 20㎛ prepared in the second step in the red ginseng concentrate ring prepared in the first step 10 While spraying the% solution in the form of a bottom spray (bottom spray), the coating content was coated to 6% of the total weight of the red ginseng concentrate ring to prepare a "red ginseng concentrate ring with a soft texture and preventing moisture absorption."
Example 6
The first step and the second step are the same as in Example 4, the third step is the concentration of red ginseng ultrafine powder having a particle size of 20㎛ prepared in the second step in the red ginseng concentrate ring prepared in the first step 10 While spraying the% solution in the form of a bottom spray (bottom spray) coating was coated so that the coating content is 9% of the total weight of the red ginseng concentrate ring to prepare a "red ginseng concentrate ring with a soft texture and preventing moisture absorption."
Example 7
The first step was the same as in Example 1, the second step was to prepare a red ginseng concentrate ring coating material with a concentration of 10% red ginseng ultra fine powder having a particle size of 35㎛, the third step was While spraying a 10% solution of red ginseng ultra fine powder with a particle size of 35 μm prepared in the second process into the bottom spray form, the coating content was 3% of the total weight of the red ginseng concentrate ring. Coated to prepare a "red ginseng concentrate ring with a soft texture, preventing moisture absorption".
Example 8
The first step and the second step are the same as in Example 7, the third step is the red ginseng concentrate fine powder having a particle size of 35㎛ prepared in the second step in the red ginseng concentrate ring prepared in the first step has a concentration of 10 While spraying the% solution in the form of a bottom spray (bottom spray), the coating content was coated to 6% of the total weight of the red ginseng concentrate ring to prepare a "red ginseng concentrate ring with a soft texture and preventing moisture absorption."
Example 9
The first step and the second step are the same as in Example 7, the third step is the red ginseng concentrate fine powder having a particle size of 35㎛ prepared in the second step in the red ginseng concentrate ring prepared in the first step has a concentration of 10 While spraying the% solution in the form of a bottom spray (bottom spray) coating was coated so that the coating content is 9% of the total weight of the red ginseng concentrate ring to prepare a "red ginseng concentrate ring with a soft texture and preventing moisture absorption."
Example 10
The first step was the same as in Example 1, the second step was prepared red ginseng concentrate ring coating material with a concentration of 10% red ginseng super fine powder with a particle size of 52㎛, the third step was While spraying 10% solution of red ginseng ultra fine powder with a particle size of 52㎛ prepared in the second process into the bottom spray form, 3% of the total weight of red ginseng concentrate ring Coated to prepare a "red ginseng concentrate ring with a soft texture, preventing moisture absorption".
Example 11
The first step and the second step are the same as in Example 1, the third step is the concentration of red ginseng ultrafine powder having a particle size of 52㎛ prepared in the second step in the red ginseng concentrate ring prepared in the first step 10 While spraying the% solution in the form of a bottom spray (bottom spray), the coating content was coated to 6% of the total weight of the red ginseng concentrate ring to prepare a "red ginseng concentrate ring with a soft texture and preventing moisture absorption."
Example 12
The first step and the second step are the same as in Example 10, the third step is the concentration of red ginseng ultrafine powder having a particle size of 52㎛ prepared in the second step in the red ginseng concentrate ring prepared in the first step 10 While spraying the% solution in the form of a bottom spray (bottom spray) coating was coated so that the coating content is 9% of the total weight of the red ginseng concentrate ring to prepare a "red ginseng concentrate ring with a soft texture and preventing moisture absorption."
Experimental Example: Determination of red ginseng component content, sensory characteristics and anti-hygroscopic effect of "red ginseng concentrate ring with soft texture and prevention of moisture absorption"
The red ginseng component content, sensory characteristics, and moisture resistance of the "red ginseng concentrate ring with a soft texture and prevention of moisture absorption" prepared in Examples were measured, and the experimental results are shown in Tables 1, 2, and 3, respectively. As shown in Table 1, the "red ginseng concentrate ring with soft texture and prevention of moisture absorption" compared the contents of the "regular red ginseng concentrate ring" (control) and ginsenoside Rg1 and Rb1. When considering the coated red ginseng powder content, it was found that there was almost no change in red ginseng functional components during the manufacturing process, as shown in Table 2. The smaller the particle size of the ultra-red ginseng powder, the better the texture and roughness. In particular, the ultra fine red ginseng powder of less than 20㎛ showed almost the same value as the 100% red ginseng concentrate ring (control) in texture and roughness. However, as shown in Table 3, under the conditions of the present experiment, the "hygroscopic red ginseng concentrate ring" is less hygroscopic during storage than the "normal red ginseng concentrate ring" (control) to prevent agglomeration when exposed to moist air. I could see that.
Experimental Example 1: Measurement of the content of red ginseng components of the "red ginseng concentrate ring prevented absorption"
The red ginseng component content of "general red ginseng concentrate ring" (control) and "red ginseng concentrate ring with a soft texture and prevention of moisture absorption" prepared in the above example was measured by using a high-performance liquid chromatography method. 2 g of each sample was precisely weighed, completely dissolved in 50 mL of distilled water, and then filtered (0.45 μm) to obtain a test solution. Standard stock solution for measuring red ginseng components by high-performance liquid chromatograph method was dissolved in methanol by ginsenoside Rg1 and Rb1 standards and filtered (0.45㎛), respectively. ) And dilute the standard stock solution with methanol to make a standard solution. 20 μL of standard solution and test solution were injected, respectively, and the peaks were separated by high performance liquid chromatography, and ginsenoside Rg1 and Ginsenoside Rg1 of the test solution were determined using a calibration curve determined by the area of the peak of the standard solution. The concentration of Rb1 (Rb1) was determined and the ginsenoside Rg1 and Rb1 contents of the sample were determined by the following equation. The results were expressed in the content of ginsenoside Rg1 and Rb1 sum (mg / g).
[formula]
Ginsenoside egg support (Rg1) = s × {(a × b) / sample collection (g)} × 1/1000)
Ginsenoside Albione (Rb1) = s × {(a × b) / Sample Collection (g)} × 1/1000)
Where s is the concentration of individual ginsenosides (μg / mL) in the test solution,
a is the total amount of the test solution (mL),
b means dilution factor.
As shown in Table 1, the "red ginseng concentrate ring with soft texture and prevention of moisture absorption" compared the contents of the "regular red ginseng concentrate ring" (control) and ginsenoside Rg1 and Rb1. When considering the coated red ginseng powder content, it can be seen that there is almost no change in the red ginseng functional component during the manufacturing process.
Experimental Example 2. Sensory evaluation of "red ginseng concentrate ring with a soft texture and prevention of moisture absorption"
In the sensory evaluation, eight well-trained sensory evaluation agents were selected as descriptive analysis agents, and four training sessions were conducted for 30 minutes on texture and roughness, and the intensity of each term was compared with the score of the standard product. Objective evaluation was conducted. The sensory evaluation evaluated 0.3g of red ginseng concentrate ring coated with red ginseng powder, "the softness (texture) felt on the tongue when melted and swallowed" and "the roughness remaining in the mouth after swallowing." When tasting milk, it is the intensity that is felt in the mouth when it is 9 points, and the roughness is the intensity that is felt when the roughness remaining in the mouth is 9 points after swallowing 0.3g of glutinous rice flour on the market. The evaluation was performed using a 9-point scale, with 1 point being very weak, 5 points being moderate, and 9 points being very strong.
As shown in Table 2, the smaller the particle size of the red ginseng powder was, the better the texture and roughness were. The ultra fine red ginseng powder having a thickness of 20 μm or less was 100% red ginseng concentrate solution (control) and texture. Nearly similar values showed very good sensory properties.
Experimental Example 3 Determination of the Hygroscopic Effects of "General Red Ginseng Concentrate Ring" (Control) and "Soft Ginseng Containing Red Ginseng Concentration Ring"
The anti-moisture effect on the "regular red ginseng concentrate ring" (control) and the "soft and hygroscopically prevented red ginseng concentrate ring" prepared in the above example was evaluated as follows: 20 g of each sample was placed in a 50 mL beaker. The sample was sealed in a desiccator controlled at 83% relative humidity and then stored at 35 o C for 7 days to evaluate the hygroscopicity of each sample. The hygroscopicity was measured using a 5-point scale on 15 trained sensory personnel. Evaluation was made.
* Hygroscopicity of the sample: +++++ (very much), ++++ (very much), +++ (usually),
++ (low), + (very low)
As shown in Table 3, under the conditions of the present experiment, the "hygroscopic red ginseng concentrate ring" has less moisture absorption during storage than the "normal red ginseng concentrate ring" (control) to prevent agglomeration when exposed to humid air. I could see that ..
As described above, although the present invention has been described by means of a limited embodiment (red ginseng) and drawings, the present invention is not limited by this and the technical spirit of the present invention by those skilled in the art to which the present invention pertains. Various modifications and variations are possible within the scope of the claims and the appended claims.
S11: preparing red ginseng concentrate granules;
S12: preparing a red ginseng powder for spraying;
S13: step of preparing the hygroscopic red ginseng concentrate granules
Claims (5)
2) preparing a red ginseng ultra fine powder coating material in an aqueous solution using red ginseng ultrafine grinder; And
3) While spraying the red ginseng super fine powder coating material prepared in step 2) in the form of a bottom spray to the red ginseng concentrate granules prepared in step 1), the coating content is 1% by weight to 9% by weight of the total weight of the red ginseng concentrate granules. Method of producing a red ginseng concentrate granules using ultra-fine red ginseng powder, characterized in that it comprises a step of preparing a soft ginseng concentrate granules with a soft texture to prevent moisture absorption.
The particle size of the red ginseng concentrate granules of 700-5,000㎛ characterized in that the manufacturing method of red ginseng concentrate granules using ultra-fine red ginseng powder.
The particle size of the ultra-fine red ginseng powder coating material is 5-100㎛ characterized in that the manufacturing method of red ginseng concentrate granules using ultra-fine red ginseng powder.
Method for producing red ginseng concentrate granules using ultra-fine red ginseng powder, characterized in that the concentration of the ultra-fine red ginseng powder coating material is 0.1-20% by weight.
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