KR20120109133A - Natural dyeing method - Google Patents
Natural dyeing method Download PDFInfo
- Publication number
- KR20120109133A KR20120109133A KR1020110027329A KR20110027329A KR20120109133A KR 20120109133 A KR20120109133 A KR 20120109133A KR 1020110027329 A KR1020110027329 A KR 1020110027329A KR 20110027329 A KR20110027329 A KR 20110027329A KR 20120109133 A KR20120109133 A KR 20120109133A
- Authority
- KR
- South Korea
- Prior art keywords
- casein
- natural
- weight
- solution
- powder
- Prior art date
Links
Images
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Coloring (AREA)
Abstract
Description
본 발명은 카제인 함유 천연염색 고착제 및 천연염색 방법에 관한 것으로서, 더욱 상세하게는 밀크 카제인, 계란 흰자, 콩 단백질 및 천연아교 중에서 선택되는 어느 하나의 카제인 분말 85~90 중량%, 탄산수소나트륨 10~15 중량% 및 초산으로 이루어진 천연염색 고착제와 이를 사용한 염색방법에 관한 것이다.The present invention relates to a casein-containing natural dye fixing agent and a natural dyeing method, more specifically, any one casein powder 85 ~ 90% by weight selected from milk casein, egg white, soy protein and natural glue, sodium hydrogen carbonate 10 ~ It relates to a natural dye fixing agent consisting of 15% by weight and acetic acid and a dyeing method using the same.
단백질은 기원전부터 사용해온 물질로 우리의 의식주 생활 속에 다양한 방법을 통해 직간접적으로 널리 이용했다. 전통 천연염색은 다양한 색을 섬유 등에 염착시켜 사용하고 있다. 염료를 섬유 등에 염착시키기 위해서는 우유, 콩즙, 석회, 철, 동, 알미늄, 아교, 잿물 등의 다양한 광물, 동물, 식물성을 이용한 전통 천연 매염재를 사용하여 염색 견뢰도를 높이고 있다. 다양한 매염재 중에 단백질이 염료를 고착시켜 견뢰도를 높여주는 역할을 한다.Protein is a substance that has been used since BC, and has been widely used directly and indirectly in various ways in our life. Traditional natural dyeing is used by dyeing various colors in textiles. In order to dye dyes into textiles, dyeing fastness is increased by using traditional natural mordants using various minerals such as milk, soybean, lime, iron, copper, aluminum, glue, lye, animal and vegetable. Among various mordants, the protein sticks the dye to increase the fastness.
오랜 염색을 해온 전통 염장인들은 염료의 숙성정도를 조절하고 매염재 제조 조건을 맞추어 흡착도를 높이는 숙련된 기술을 가지고 있다. 일반 염색인들은 보편적인 방법이나 화학적 매염재를 이용해 염색을 하여 사용하고 있다. 전통 천연염색은 염료의 온도, 숙성, 발효 등의 조건과 매염재의 물, 온도, 습도, 숙성도 등을 맞추기 어려워 견뢰도 높은 염색은 전문 염장인들이 가능하고 일반 염색인들은 어려운 편이다. 염색 시 피염물에 염료가 잘 흡착되어 견뢰도 높은 염색이 되어 실용성이 높아야 한다. 현재까지 전통 천연염색은 견뢰도를 잘 해결하지 못한 것이 문제점이다.
Traditional dyeers who have been dyeing for a long time have the skill to adjust the degree of aging of dyes and to increase the adsorption rate by adjusting the condition of making mordant. General dyeers use a common method or dyeing using chemical mordant. Traditional natural dyeing is difficult to match the conditions such as dye temperature, ripening, fermentation, and water, temperature, humidity, and maturity of mordant, so high-speed dyeing is possible for professional dyeers and general dyeers are difficult. When dyeing, dye should be well adsorbed to the dye to be fastened with high fastness and high practicality. Traditional natural dyeing has not been able to solve the fastness well.
본 발명은 소비자들이 천연염색을 하면서 발생되는 물빠짐, 탈색, 변색 등 천연염색 견뢰도의 문제점을 해결하기 위한 천연염색 천연고착제 및 그 패키지 제품을 제공하는 것이다.
The present invention is to provide a natural dyeing natural fixing agent and a packaged product for solving the problems of natural dyeing fastness such as water fall, discoloration, discoloration generated while consumers natural dyeing.
본 발명은 밀크 카제인, 계란 흰자, 콩 단백질 및 천연아교 중에서 선택되는 어느 하나의 카제인 분말 85~90 중량%, 탄산수소나트륨 10~15 중량% 및 초산으로 이루어진 천연염색 고착제와 이를 사용한 염색방법에 관한 것이다.The present invention relates to a natural dye fixing agent consisting of 85-90% by weight of a casein powder selected from milk casein, egg white, soy protein and natural glue, 10-15% by weight sodium bicarbonate and acetic acid and a dyeing method using the same will be.
본 발명은 천연염색 고착에 필요한 밀크 카제인, 탄산수소나트륨 및 초산을 포함한 고착제 조성물 및 상기 조성물의 포장제, 천연염색 기법 설명서, 고착제 사용설명서를 패키지로 함으로서 천연염색을 처음으로 하는 사람도 쉽게 염색을 하고, 견뢰도가 우수한 천연염색 결과물을 얻을 수 있는 효과가 있다.According to the present invention, a dyeing agent composition comprising milk casein, sodium hydrogen carbonate, and acetic acid required for fixing natural dyes, and a packaging agent, a natural dyeing technique manual, and a fixing agent manual for packaging the composition are easily dyed even for the first person. And, there is an effect that can obtain a natural dyeing result excellent in color fastness.
도 1은 본 발명의 천연염색 고착제 조성물을 밀봉 포장한 팩의 사진.
도 2는 본 발명의 천연염색 안료 염료를 밀봉 포장한 팩의 사진.1 is a photograph of a pack sealed packaging of the natural dye fixing composition of the present invention.
Figure 2 is a photograph of a pack sealed packaging of the natural dye pigment dye of the present invention.
본 발명은 밀크 카제인, 계란 흰자, 콩 단백질 및 천연아교 중에서 선택되는 어느 하나의 카제인 분말 85~90 중량%, 탄산수소나트륨 10~15 중량% 및 탄산수소나트륨을 가한 카제인 수용액의 Ph를 4.5?5로 조정하는 조정량의 초산으로 이루어진 것을 특징으로 하는 카제인 함유 천연염색 고착제에 관한 것이다.According to the present invention, the pH of the casein solution to which 85-90 wt% of casein powder selected from milk casein, egg white, soy protein and natural glue, 10-15 wt% of sodium bicarbonate and sodium bicarbonate is added is 4.5-5. It relates to a casein-containing natural dye fixing agent comprising an acetic acid of the adjusted amount adjusted to.
본 발명은 밀크 카제인, 계란 흰자, 콩 단백질 및 천연아교 중에서 선택되는 어느 하나의 카제인 분말 85~90 중량%, 탄산수소나트륨 10~15 중량% 및 탄산수소나트륨을 가한 카제인 수용액의 Ph를 4.5?5로 조정하는 조정량의 초산으로 이루어진 천연염색 고착제를 준비하는 단계; 70?100℃의 물 50 중량부에 상기 카제인 분말 1 중량부를 넣은 후 탄산수소나트륨을 가하여 카제인 분말을 용해시켜 카제인 수용액을 제조하는 단계; 상기 카제인 수용액에 천연염색을 끝마친 피염물 200?300 중량부를 넣고 주무르고 짠 후 털어주는 단계; 피염물을 꺼낸 카제인 수용액에 초산을 가하여 Ph 4.5?5로 조정하는 단계; 상기 피염물을 다시 상기 카제인 수용액에 넣고 주무른 후 피염물에 침전시키는 단계; 및 상기 피염물을 카제인 수용액에서 꺼내 건조시키는 단계로 이루어진 것을 특징으로 하는 카제인 함유 천연염색 고착제를 사용한 천연염색 방법에 관한 것이다. According to the present invention, the pH of the casein solution to which 85-90 wt% of casein powder selected from milk casein, egg white, soy protein and natural glue, 10-15 wt% of sodium bicarbonate and sodium bicarbonate is added is 4.5-5. Preparing a natural dye fixing agent consisting of an adjusted amount of acetic acid adjusted to; Preparing a casein aqueous solution by dissolving the casein powder by adding 1 part by weight of the casein powder to 50 parts by weight of water at 70 ° C. to 100 ° C .; Putting 200-300 parts by weight of the finished dyeing solution in natural casein solution, kneading, squeezing and whisking; Adding acetic acid to an aqueous solution of casein from which the brine was taken out and adjusted to Ph 4.5-5; Putting the chlorine back into the aqueous casein solution and then rubbing the precipitate; And it relates to a natural dyeing method using a casein-containing natural dye fixing agent, characterized in that consisting of the step of taking out the chlorine from the aqueous solution of casein.
본 발명은 광물성 염재, 식물성 염재 및 동물성 염재 중에서 선택된 어느 하나의 염재를 분말 안료화한 천연염료에 있어서 밀크 카제인, 계란 흰자, 콩 단백질 및 천연아교 중에서 선택되는 어느 하나의 카제인 분말 85~90 중량%, 탄산수소나트륨 10~15 중량% 및 탄산수소나트륨을 가한 카제인 수용액의 Ph를 4.5?5로 조정하는 조정량의 초산으로 이루어진 천연염색 고착제가 함유된 천연염료에 관한 것이다.The present invention is 85 to 90% by weight of any casein powder selected from milk casein, egg white, soy protein and natural glue in a natural pigment powder pigmented any one selected from mineral salts, vegetable salts and animal salts It relates to a natural dye containing a natural dye fixing agent consisting of an adjusted amount of acetic acid to adjust the pH of the aqueous solution of casein added with sodium bicarbonate 10-15% by weight and sodium bicarbonate.
본 발명에서 사용되는 밀크 카제인은 우유에서 추출되는 동물성 단백질로서 특별한 제한이 없으며 우유를 이용하여 카제인을 추출하거나 상업용으로 판매되고 있는 카제인을 활용할 수 있다. 카제인은 우유단백질의 약 80%를 차지한다. 우유단백질은 칼슘 및 인산과 결합된 수용성으로 초산용액을 가하여 PH를 등전점인 4.5~4.6으로 하면 침전되므로 이를 분리하여 카제인을 추출할 수 있다.
The milk casein used in the present invention is an animal protein extracted from milk, and there is no particular limitation, and casein may be extracted using milk or casein sold commercially. Casein makes up about 80% of milk protein. Milk protein is water-soluble combined with calcium and phosphoric acid, and then added with acetic acid solution to set the pH to 4.5-4.6, which is an isoelectric point.
실시예 1: 카제인 분말의 제조Example 1 Preparation of Casein Powder
우유를 비이커에 넣고 70?100℃로 가열한 후 10% 초산 용액을 가하면서 PH를 등전점인 4.6으로 조정하면 카제인이 침전된다. 상기 침전물을 여과한 후 물로 잘 세척한다. 침전된 카제인을 80~90℃로 열풍, 건조하여 100~200 mesh가 되도록 분말화시키면 카제인 분말이 얻어진다.
The milk is placed in a beaker, heated to 70-100 ° C, and the pH is adjusted to 4.6, the isoelectric point, while adding 10% acetic acid solution to precipitate casein. The precipitate is filtered off and washed well with water. Casein powder is obtained when the precipitated casein is hot-air dried at 80-90 ° C. and dried to powder 100-200 mesh.
실시예 2: 카제인 수용액의 제조 Example 2: Preparation of Aqueous Casein Solution
카제인 분말은 불용성이므로 직접 사용할 수 없어 수용액으로 만들어 사용해야 한다. 카제인 분말을 물에 용해한 용액을 조정(PH 7 내외)시키면 카제인 수용액이 된다. 뜨거운 물(약 70?100℃)에 카제인 분말을 넣고 탄산수소나트륨을 가하여 PH 7이 되도록 조정시키고 완전히 용해될 때까지 저어주면 카제인 수용액이 얻어진다.Casein powder is insoluble and cannot be used directly. The solution of casein powder dissolved in water is adjusted (approximately PH 7) to give an aqueous casein solution. Casein powder is added to hot water (about 70 to 100 ° C), sodium bicarbonate is added to adjust to pH 7, and stirred until completely dissolved to obtain a casein aqueous solution.
물 1L(약 70?100℃)에 카제인 분말 40g 및 탄산수소나트륨 5g을 혼합하여 잘 저어주면 완전 용해되어 카제인 수용액이 얻어진다. 천연염색을 끝마친 제품(원단 포함)을 후매염 처리하기 위하여 카제인 분말 및 탄산수소나트륨으로 이루어진 카제인 고착제를 뜨거운 물(70?100℃)에 풀어 넣고 희석시키면 카제인 수용액이 얻어진다. 카제인 분말 및 탄산수소나트륨으로 이루어진 고착제 : 물의 혼합 비율은 1 : 50이 바람직하고, 카제인 분말 및 탄산수소나트륨으로 이루어진 고착제 100ml에 물 5L를 혼합하는 것이 바람직하다.
40 g of casein powder and 5 g of sodium hydrogen carbonate are mixed with 1 L of water (about 70 to 100 ° C.) and stirred well to completely dissolve to obtain an aqueous casein solution. Casein fixing agent consisting of casein powder and sodium hydrogencarbonate is dissolved in hot water (70-100 ° C.) in order to post-dye the finished product (including fabric) after natural dyeing, and a casein aqueous solution is obtained. The mixing ratio of casein powder and sodium hydrogencarbonate: water is preferably 1:50, and it is preferable to mix 5 L of water with 100 ml of the casein powder and sodium hydrogencarbonate.
실시예 3: 천연염색 방법 Example 3: Natural Dyeing Method
물 1L(약 70?100℃)에 카제인 분말 40g 및 탄산수소나트륨 5g을 혼합하여 잘 저어주면 완전 용해되어 카제인 수용액이 얻어지고, 물 5L에 상기 카제인 수용액 100ml를 사용하여 천연염색 경우 피염물 200~300g이 적정하다. 카제인 수용액에 피염물을 넣고 가볍게 주무르고 짠 후 털어준다. 피염물을 커낸 후 카제인 수용액에 초산을 가하여 ph 4.5~5 정도로 조정시킨다. 카제인 수용액에 다시 피염물을 넣고 주무른 후 약 30분 정도 침전시킨다. 피염물, 천연염색 염료 및 카제인 삼자 간의 응고현상이 일어난다. 피염물을 가볍게 짜서 건조시킨다. 잘 건조된 피염물을 열처리(다림질)한다. 위와 같은 과정을 거치면서 피염물은 견뢰도가 뛰어난 완벽한 천연염색 제품으로 탈바꿈된다. 후매염 염색과정이 끝난 피염물의 세탁 견뢰도가 4 내지 5로 크게 향상되었다.
When 40 g of casein powder and 5 g of sodium hydrogen carbonate are mixed and stirred well in 1 L of water (about 70 to 100 ° C.), the solution is completely dissolved to obtain a casein aqueous solution. 300 g is appropriate. Add the salt to the aqueous casein solution, knead lightly, squeeze, and shake. After the brine is grown, acetic acid is added to the aqueous casein solution to adjust the pH to about 4.5-5. Add the brine again to the aqueous casein solution and knead it for about 30 minutes. Coagulation between the salts, the natural dyes and the casein triad occurs. Squeeze the salt to dry lightly. Heat dried (ironed) well-dried salts. Through the above process, the dye is transformed into a perfect natural dyeing product with high color fastness. The wash fastnesses of the stain after the post-dyeing dyeing process were greatly improved to 4-5.
실시예 4: 천연염색 방법 Example 4: Natural Dyeing Method
광물성 염재, 식물성 염재 및 동물성 염재 중에서 선택된 어느 하나의 염재를 분말 안료화한 천연염료 20g, 카제인 분말 4g 및 탄산수소나트륨 0.5g을 혼합하여 천연염료를 만든다. 상기 천연염료를 80℃ 물4L에 풀어 3시간 숙성시킨 후 30℃에서 중매염 염색과정이 끝난 피염물을 직접 염색한다. 이때 혼합된 염료를 80℃에 3시간 숙성시키면 잘 용해되어 흡착률을 매우 높여 고착이 잘 된다. 후매염 염색과정이 끝난 피염물의 세탁 견뢰도가 4 내지 5로 크게 향상되었다.
A natural dye is prepared by mixing 20 g of a natural pigment powdered with a pigment selected from mineral salts, vegetable salts and animal salts, 4 g of casein powder and 0.5 g of sodium bicarbonate. After dissolving the natural dye in 4L of water at 80 ℃ and aged for 3 hours, the dye dyeing process is finished dyeing directly at 30 ℃. In this case, when the mixed dye is aged at 80 ° C. for 3 hours, the dye is dissolved well, and the adsorption rate is very high, and the adhesion is well achieved. The wash fastnesses of the stain after the post-dyeing dyeing process were greatly improved to 4-5.
실험예 1: 견뢰도 시험Experimental Example 1: Fastness Test
본 발명의 고착제를 사용한 천연염색 제품과 본 발명의 고착제를 사용하지 않은 천연염색 제품을 대비하여 견뢰도 평가를 수행하였다. 본 발명의 고착제를 사용한 천연염색 제품이 세탁, 일광, 마찰 및 땀에 대한 견뢰도에 있어서 아주 우수한 특성을 나타내고 있음을 알 수 있다. 본 발명의 고착제를 사용한 천연염색 제품은 세탁 견뢰도가 4 내지 5로 크게 향상되었다.The fastness evaluation was performed in comparison with the natural dyeing product using the fixing agent of the present invention and the natural dyeing product without using the fixing agent of the present invention. It can be seen that the natural dyeing product using the fixing agent of the present invention exhibits very excellent properties in the fastness to washing, sunlight, friction and sweat. Natural dyeing products using the fixing agent of the present invention was greatly improved to wash fastness to 4-5.
본 발명의 고착제와 같은 조성물을 함량비에 따라 각각 또는 혼합하여 밀봉하여 포장한 후 여기에 측정을 위한 리트머스 시험지, 천연염색 염색설명서 및 고착제 사용설명서를 더 포함시켜 천연염색 전문가용 필수 매염제로 또는 학습용 교구 및 취미용 용품으로 판매하거나 사용할 수 있는 패키지 상품으로 구성할 수 있다. 본 발명의 고착제를 사용한 천연염색은 천연염색의 견뢰도(햇빛, 세탁, 일광, 마찰, 땀)가 현저하게 증가되며 천연염색을 하고난 후 사용자가 직접 후처리(후매염)을 하여 천연염색의 견뢰도를 획기적으로 증가시킬 수 있도록 천연염색에 필요한 용품을 한꺼번에 포함시켜 판매할 수 있어 학습용, 취미용 또는 전문적으로 사용할 수 있는 패키지 제품으로 판매할 수 있는 것이다.After packing the composition, such as the fixing agent of the present invention, individually or mixed and sealed according to the content ratio, it further includes litmus test paper, natural dyeing manual and fixing agent instructions for measurement as essential mordant for natural dyeing or learning It can be configured as a packaged product that can be sold or used as a parish or hobby item. Natural dyeing using the fixing agent of the present invention is significantly increased the fastness of the natural dyeing (sunlight, washing, daylight, friction, sweat) and after the natural dyeing, the user directly post-treatment (post-salting) fastness of the natural dyeing It can be sold as a package product that can be used for learning, hobby or professional use by including all the necessary products for natural dyeing so that it can increase dramatically.
100: 천연염색 고착제 200: 천연염색 안료 염료100: natural dye fixing agent 200: natural dye pigment dye
Claims (3)
In a natural pigment powder pigmented any one selected from mineral salts, vegetable salts and animal salts, the natural dye is any one casein powder selected from milk casein, egg white, soy protein and natural glue 85-90 A natural dye containing a natural dye fixing agent consisting of an adjusted amount of acetic acid to adjust the pH of the aqueous solution of casein added with weight%, sodium hydrogen carbonate 10-15% by weight and sodium hydrogen carbonate to 4.5-5.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR1020110027329A KR101199258B1 (en) | 2011-03-28 | 2011-03-28 | natural dyeing method |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR1020110027329A KR101199258B1 (en) | 2011-03-28 | 2011-03-28 | natural dyeing method |
Publications (2)
Publication Number | Publication Date |
---|---|
KR20120109133A true KR20120109133A (en) | 2012-10-08 |
KR101199258B1 KR101199258B1 (en) | 2012-11-12 |
Family
ID=47280558
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1020110027329A KR101199258B1 (en) | 2011-03-28 | 2011-03-28 | natural dyeing method |
Country Status (1)
Country | Link |
---|---|
KR (1) | KR101199258B1 (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110273307A (en) * | 2019-06-17 | 2019-09-24 | 吉林化工学院 | A kind of environment protection type color fixing agent preparation of natural pigment and its color-fixing method |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110565410A (en) * | 2019-08-18 | 2019-12-13 | 贵州省麻江河坝民族工艺品有限公司 | Method for making Yao nationality egg powder |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2009019297A (en) | 2007-07-11 | 2009-01-29 | Nakajima Kk | Color-developed processed product |
-
2011
- 2011-03-28 KR KR1020110027329A patent/KR101199258B1/en active IP Right Grant
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110273307A (en) * | 2019-06-17 | 2019-09-24 | 吉林化工学院 | A kind of environment protection type color fixing agent preparation of natural pigment and its color-fixing method |
CN110273307B (en) * | 2019-06-17 | 2022-03-01 | 吉林化工学院 | Preparation and color fixing method of environment-friendly color fixing agent for natural pigment |
Also Published As
Publication number | Publication date |
---|---|
KR101199258B1 (en) | 2012-11-12 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN103669031B (en) | The colouring method of blended yarn woven fabric | |
CN103571223A (en) | Formula and production method for preparing bright yellow wheat straw dye | |
CN105714578B (en) | A kind of colouring method of fruit button | |
CN106436373A (en) | Pigment printing technology of cotton ramie fabric | |
KR101199258B1 (en) | natural dyeing method | |
CN107627424A (en) | A kind of colouring method of sun-proof raffia compile cap | |
CN106592272B (en) | A kind of method of natural black dyes real silk fabric | |
CN105040481B (en) | Printing paste containing laccaic acid pigment and printing technology thereof | |
Blackburn et al. | A dye–fibre system from food waste: Dyeing casein fibres with anthocyanins | |
CN108403580A (en) | A kind of natural plant pigment hair dye and preparation method thereof and preparation method thereof | |
CN106367957B (en) | Tea contaminates the preparation method of garment material | |
CN103491789A (en) | Polyphenol increasing agent for plant leaves, resin pellet, plant leaf storage sheet, and manufacturing method therefor | |
JP2009007414A (en) | Quercetin sulfonic acid-containing dye, and dyeing method | |
CN113774685B (en) | Preparation method of anti-wrinkle antibacterial intelligent home textile fabric | |
CN105949819B (en) | A kind of cottonseed hull natural dye extracting method and tint applications | |
JP2004190186A (en) | Method for producing color cotton | |
TWI736794B (en) | Reactive dye composition and dyeing method using the same | |
CN103103832A (en) | Denim discharge printing paste and preparation method thereof | |
KR101312171B1 (en) | Dyeing method, Preparation method for blue pigments and Kit for the same | |
CN105171873A (en) | Treating agent with characteristic of convenient corn skin dyeing | |
KR101253026B1 (en) | Dyeing method, Preparation method for blue pigments and Kit for the same | |
CN110863369A (en) | Low-energy-consumption natural dye dyeing method for real silk fabric | |
CN104924395A (en) | Treating agent convenient for corn bran dyeing | |
CN106835772B (en) | A kind of cotton dyeing method | |
WO2005047591A1 (en) | Method for coloring corporeal substance having polyamide bond and corporeal substance colored by such method |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
A201 | Request for examination | ||
E701 | Decision to grant or registration of patent right | ||
GRNT | Written decision to grant | ||
FPAY | Annual fee payment |
Payment date: 20151012 Year of fee payment: 4 |
|
FPAY | Annual fee payment |
Payment date: 20161021 Year of fee payment: 5 |
|
FPAY | Annual fee payment |
Payment date: 20171020 Year of fee payment: 6 |
|
FPAY | Annual fee payment |
Payment date: 20191029 Year of fee payment: 8 |