KR20120090656A - Lip care cosmetic composition containing natural pigments - Google Patents

Abstract

PURPOSE: A cosmetic composition containing natural pigment is provided to ensure antioxidation, antibacterial, and whitening effects. CONSTITUTION: A cosmetic composition for lip contains natural pigment as an active ingredient, from black rice, mulberry leaves, Rehmanniae radix, grape skin, red cabbage, mulberry, Lithospermum erythrorhizon Siebold & Zucc., balsam pear, cactus, or onion skin. The composition additionally contains wax and oil. The composition is manufactured in a lip stick, lip gloss, lip pencil, lip balm, or lip cream.

Description

Lip care cosmetic composition containing natural pigments

The present invention relates to a cosmetic composition for lips containing natural pigments excellent in antimicrobial, antioxidant activity and skin lightening effect, and more specifically, black rice, mulberry leaves, turmeric, grape skin, red cabbage, bitter gourd, mulberry, jichi It relates to a cosmetic composition for lips using natural pigment extracted from baeknyeoncho or onion skin.

As modern people are increasingly pursuing eco-friendly life that promotes naturalistic life, the desire to decorate the surrounding environment and body with natural materials is increasing. The history of makeup on people's faces began with the history of mankind.In the early days, all pigments in cosmetics were taken from natural animals and plants or minerals, but chemical pigments appeared in a wide range of products. Was used.

Indiscriminate use of color cosmetics using chemical pigments has been pointed out in recent years, but the use of natural pigments is still low in color cosmetics.

As the skin ages, the elasticity and wrinkles increase, and the lips undergo the same process of change, but most people care for the facial skin, and the lip skin is relatively neglected. However, if the lip is sensitive to skin tissue and comes into contact with an unsanitary environment, it is highly susceptible to infection with various germs, and in particular, harmful chemicals such as lipsticks, lip glosses, and other synthetic fragrances, pigments, and preservatives, etc. It may be.

Therefore, it is necessary to prevent these side effects by manufacturing cosmetics for the lips with a natural material that is safe for the human body and also prevents discoloration of lips due to harmful ingredients.

Natural colors using natural colors as well as natural materials have the function of the medicinal herbs. For example, gardenia detoxification as an anti-inflammatory agent, safflower seed is beneficial to the bone, joiner has antibacterial action, central inhibitory action, action on the intestinal vessels. In addition, Schisandra chinensis is used as a medicine for coughing and skin treatment, and the side has the effect of cleansing the liver with chemotherapy and at the same time has its own unique pigment, which is also used in the manufacture of cosmetics.

Since cosmetics are used repeatedly in daily life or over a long period of time, safety and side effects must be guaranteed. Recently, as natural products such as plant extracts have been used as cosmetic raw materials, the effectiveness and safety of these natural products have been actively reviewed, and with the development of biotechnology, a lot of studies on the introduction of new natural materials and skin physiology have been conducted. It is done.

As such, interest in natural extracts is gradually increasing along with the development of extraction and safety technology of natural substances, but the use of such natural substances is still largely used as a component of basic cosmetics.

Therefore, there is a need for the development of a cosmetic composition using a proven natural pigment to solve these problems and to manufacture a healthy and safe lip cosmetic product.

Therefore, the present inventors are trying to develop natural lip care products that meet the consumer's preference for a safer and more naturalistic life compared to the existing color cosmetics using synthetic colors, black rice, mulberry leaves, turmeric, grape peel, red cabbage When used in the manufacture of lip cosmetics, natural pigments present in yeast, odyssey, chichi, zinnia and onion skins, not only produce beautiful colors but also have excellent effects on antibacterial, sun protection, antioxidant, whitening and moisturizing. By confirming that the present invention was completed.

Therefore, an object of the present invention comprises a cosmetic composition for lips comprising at least one natural pigment selected from the group consisting of black rice, mulberry leaves, turmeric, grape peel, red cabbage, bitter gourd, mulberry, chichi, baeknyeoncho and onion peel To provide.

Another object of the present invention is freeze-dried at least one selected from the group consisting of black rice, mulberry leaves, turmeric, grape skin, red cabbage, bitter gourd, mulberry, jichi, baeknyeoncho and onion peel, pulverized to 100 ~ 200㎛ diameter To provide a method for producing a cosmetic composition for lips comprising the step of obtaining a natural pigment powder.

In order to achieve the object of the present invention as described above, the present invention is effective in at least one natural pigment selected from the group consisting of black rice, mulberry leaves, turmeric, grape peel, red cabbage, bitter gourd, mulberry, jichi, baeknyeoncho and onion peel It provides a cosmetic composition for lips comprising as a component.

In one embodiment of the present invention, the black rice, mulberry leaves, turmeric, grape peel, red cabbage, bitter gourd, mulberry, jichi, baeknyeoncho or onion peel may include 5-20% by weight relative to the total weight of the composition.

In one embodiment of the invention, the composition may further comprise a wax and oil.

In one embodiment of the present invention, the wax and oil may be that containing 5 to 20% by weight and 20 to 50% by weight of the wax relative to the total weight of the composition.

In one embodiment of the present invention, the composition may be one having an antibacterial effect, a sunscreen effect, an antioxidant effect or a whitening effect.

In addition, the present invention is freeze-dried at least one selected from the group consisting of black rice, mulberry leaves, turmeric, grape peel, red cabbage, bitter gourd, mulberry, jichi, baeknyeoncho and onion peel, and pulverized to 100 ~ 200㎛ diameter It provides a method for producing a cosmetic composition for lips comprising the step of obtaining a natural pigment powder.

In one embodiment of the present invention, the composition may be prepared in a formulation selected from the group consisting of lipstick, lip gloss, lip balm (Lipbalm) and lip cream.

Natural cosmetics according to the present invention, such as black rice pigment, mulberry leaf pigment, yellow-yellow pigment, grape peel pigment, red cabbage pigment, bitter orange pigment, mulberry pigment, borage pigment, zinnia pigment or onion peel pigment is an antibacterial effect, antioxidant Excellent effect and whitening effect, excellent moisturizing effect and stability against UV rays, not only can be usefully used as a cosmetic composition, but also by using natural pigments, it is environmentally friendly and safer for human body. .

1 shows a natural pigment powder used in the present invention.
Figure 2a is Escherichia using agar medium diffusion method It shows the inhibitory activity of natural pigment on coli , A is ripe bitter gourd, paprika, popliteal, gardenia, and B is immature bitter gourd, mulberry leaf, onion peel, gardenia blue, C is purple sweet potato , Audi, grape skin, red cabbage, D represents red beet, black rice, ripe bitter gourd, purple sweet potato clockwise.
2b is a Bacillus using agar medium diffusion method It shows the inhibitory activity of natural pigment against subtilis , A is ripe bitter gourd, paprika, popliteal, gardenia, and B is immature bitter gourd, mulberry leaf, onion peel, gardenia blue, C is purple sweet potato , Audi, grape skin, red cabbage, D represents red beet, black rice, ripe bitter gourd, purple sweet potato clockwise.
Figure 2c is Vibrio using agar medium diffusion method It shows the inhibitory activity of natural pigments against parahaemdyticus , where A is ripe bitter melon, paprika, vulgaris, and gardenia, B is immature bitter melon, mulberry leaves, onion peel, gardenia blue, and C is purple sweet potato , Audi, grape skin, red cabbage, D represents red beet, black rice, ripe bitter gourd, purple sweet potato clockwise.
Figure 2d Salmonella using agar medium diffusion method It shows the inhibitory activity of natural pigments against typhymurium , A is ripe bitter gourd , paprika, dill, and gardenia, B is immature bitter gourd , mulberry leaf, onion peel, gardenia blue, C is purple sweet potato , Audi, grape skin, red cabbage, D represents red beet, black rice, ripe bitter gourd, purple sweet potato clockwise.
Figure 2e is Proteus using agar medium diffusion method It shows the inhibitory activity of natural pigment against mirabilis , A is ripe bitter gourd, paprika, dill, and gardenia, B is immature bitter gourd, mulberry leaf, onion peel, gardenia blue, and C is purple sweet potato , Audi, grape skin, red cabbage, D represents red beet, black rice, ripe bitter gourd, purple sweet potato clockwise.
Figure 2f is a micrococcus using agar medium diffusion method It shows the inhibitory activity of natural pigments against luteus , where A is ripe bitter melon, paprika, popliteal, gardenia, and B is immature bitter melon, mulberry leaf, onion peel, gardenia blue, and C is purple sweet potato , Audi, grape skin, red cabbage, D represents red beet, black rice, ripe bitter gourd, purple sweet potato clockwise.
3 is a graph showing whether the natural pigment itself affects the cell death of skin cells.
Figure 4 is a graph showing the effect of inhibiting apoptosis according to the treatment of natural pigment extract against skin cell death irradiated with UV-B (* p <0.05 vs. control, ** p <0.05. Vs. UV alone)
Figure 5 shows the blocking effect of the natural pigment extract on the expression effect of the cell death promoting proteins Bax and cell death inhibitory protein Bcl-2 by skin in skin cells.

The present invention provides a lip cosmetics for use in lips that have a high probability of contacting skin tissue with sensitive and unsanitary environments.There are no side effects in the body and functional lip cosmetics having useful physiological activities such as antibacterial and antioxidant activities in the body. It is characterized by providing, more specifically, black rice, mulberry leaves, sulfur, grape peel, red cabbage, bitter gourd, mulberry, chichi, baeknyeoncho and onion skin containing one or more natural pigments extracted from natural ingredients as an active ingredient It is characterized by providing a cosmetic composition for the lip.

In the present invention, in the preparation of the cosmetic composition for the lips, black rice, mulberry leaves, turmeric, grape skin, red cabbage, bitter gourd, audi, jichi, baeknyeoncho and onion skin used natural materials, black rice and mulberry used in the present invention is aged It contains an anthocyanin-based compound that has excellent antioxidant activity and suppresses black color. Black rice contains various beneficial nutrients such as calcium, vitamins, iron and selenium, and Audi has high blood pressure as well as anti-aging antioxidant pigment C3G. It contains a lot of health functional ingredients such as rutin, an inhibitor, and DNJ, a blood sugar lowering substance.

In addition, the grape skin and red cabbage used in the present invention also contain an anthocyanin-based compound with excellent antioxidant activity and have a red color, and the grape skin contains a large amount of tannin and resveratrol, which is excellent in anticancer and antioxidant activity. Red cabbage contains vitamin U, called S-methyl methionine, an effective ingredient for gastrointestinal disorders.

In addition, the mulberry leaf used in the present invention is effective in preventing various adult diseases and heavy metals, liver, and green to the extent that it is a fresh medicinal chlorophyll-based fresh medicine.

In addition, yogurt, bitter gourd and onion peel is yellow with carotenoid series, and the pasteurized chrysanthemum has antipyretic, detoxification, cardiopulmonary and hemostatic effects. It has excellent effects on storol, diabetes, cataracts, and dementia.

In addition, the chichi and baeknyeoncho used in the present invention is an anthocyanin-based pigment of reddish purple, and has excellent efficacy in preventing cancer, antibacterial, antidiabetic and hypertension.

As described above, the natural ingredients used in the preparation of the cosmetics for lips in the present invention, black rice, mulberry leaves, turmeric, grape skin, red cabbage, bitter gourd, mulberry, chichi, zinnia and onion peels contain useful functions in the body and have side effects. It has a natural color and has the feature of producing cosmetics that can produce natural and beautiful colors.

The black rice, mulberry leaves, turmeric, grape peel, red cabbage, bitter gourd, mulberry, zizi, baeknyeoncho or onion skin used in the present invention can be used as long as it can be purchased on the market, preferably black rice, mulberry leaves, turmeric , Grape skin, red cabbage, bitter gourd, mulberry, jichi, baeknyeoncho or onion peel freeze-dried, the natural pigment obtained by grinding to a diameter of 100 ~ 200㎛ can be used.

On the other hand, natural pigments of black rice, mulberry leaves, turmeric, grape peel, red cabbage, bitter gourd, mulberry, chichi, baeknyeoncho or onion peel according to the present invention is characterized by having antibacterial, sunscreen, antioxidant and whitening activity.

According to one embodiment of the present invention, as a result of observing the microbial inhibitory ring using a disk agar plate diffusion method on the natural pigment extracts obtained from the natural materials, all harmful microorganisms used in the experiment On the contrary, the natural pigments of the present invention all formed an inhibitory ring, and in particular, it was found that a mulberry leaf, grape skin, and turmeric have very good antibacterial activity (Figs. 2a, 2b, 2c, 2d and 2e). And FIG. 2F).

In addition, as a result of analyzing the effect of the natural pigment itself on the skin cells by setting the appropriate concentration for each natural pigment, it was shown that the natural pigments according to the present invention does not affect the apoptosis of the skin cells (see Fig. 3) When the skin cells were irradiated with ultraviolet rays and treated with natural pigments, it was observed that the natural pigment extracts had an effect of inhibiting apoptosis caused by ultraviolet rays (see FIG. 4). Was found to be suppressed (see FIG. 5).

Therefore, it can be seen from the above results that natural pigments according to the present invention have excellent antimicrobial effect and cytoprotective effect by UV light.

Furthermore, the present invention can provide a method for preparing the cosmetic composition for the lips containing the natural pigment according to the present invention, preferably black rice, mulberry leaves, sulfur, grape peel, red cabbage, bitter gourd, mulberry, branch, zinnia or After freeze-drying the onion skin, and dissolving the natural pigment powder obtained by grinding to a diameter of 100 ~ 200㎛ in distilled water, and then adding wax and oils to make an emulsion, the general addition used in the preparation of cosmetics for lips It may include the step of adding the material and mixing.

At this time, the powder of the natural pigment is preferably pulverized to have a diameter of 100 ~ 200㎛, when the powder diameter is larger than the above range, the pigment may be present in the form of agglomeration is not only easy to dissolve in distilled water, but also clean color There is a problem that can not be expressed, when the powder diameter is smaller than the above range there is a problem that the stability of the pigment is reduced and the durability of the makeup is weakened.

In addition, the natural pigment may include a pigment of black rice, mulberry leaves, turmeric, grape peel, red cabbage, bitter gourd, mulberry, chichi, baeknyeoncho or onion peel in an amount of 5 to 20% by weight relative to the total weight of the cosmetic composition. , The natural pigments can be used alone or in combination of one or more, and when used in combination with each other, there is a feature that can produce a variety of colors than the color that can be used alone, the mixture of pigments The content may be included in an amount of 5 to 20% by weight based on the total weight of the cosmetic composition.

When the content of the natural pigment is contained in less than 5% by weight, the desired beautiful color is not properly developed, there is a problem that the effect of the makeup is weak, and when used in excess of 20% by weight, the pigment is deposited, evenly in the composition It doesn't dissolve, so it doesn't look beautiful.

In addition, the wax (solid) and oil (including butter) which is a component included in the cosmetic composition of the present invention is added as a component to add a soft feeling and an emulsifier to facilitate mixing with the pigment extract (aqueous), The type of wax and oil need not be particularly limited, and any wax or oil may be used. In addition, the wax and oil may include 5 wt% to 20 wt% wax, and the oil may include 20 wt% to 50 wt%, based on the total weight of the composition of the present invention.

At this time, if the wax is less than 5% by weight and the oil content is less than 20% by weight, the composition is not easily emulsified and the feeling of use of the cosmetics produced is not smooth, while the wax is more than 20% by weight and the oil content is 50% If the weight percentage is exceeded, the pigments, oils and waxes may spread to prevent aesthetic appearance of beautiful makeup. Therefore, it is preferable to use the cosmetics for the lips within the above-described content range in order to enable a clean makeup having an appropriate viscosity and hardness.

In addition to glycerin and water-soluble natural betaine, the additives which can be used in the preparation of the cosmetic composition of the present invention include other conventional ingredients such as nutrients, solubilizers, pigments and flavorings such as conventional auxiliaries, antioxidants, and preservatives. can do. However, in principle, natural materials should be used to add these additional materials.

In addition, preferably, the cosmetic composition for lips according to the present invention may further include a plant extract, the plant extract is licorice extract, fish extract, green tea extract, calendula extract, iris extract, Schisandra chinensis extract, ginseng extract, Angelica Extracts or ginkgo biloba extracts can be used. These extracts can also be used as a solvent for dissolving the pigment.

These plant extracts are already known as plants containing a large amount of the above useful pharmacological components, and are widely used in foods and cosmetics in addition to drugs, and when these are further included, the effects of improving the various functions of the cosmetic composition of the present invention can be further improved. Can be obtained. When the plant extract is further included, the plant extract may be added in an amount of 5 to 10% by weight based on the total weight of the composition.

On the other hand, the cosmetic composition for lips of the present invention prepared by the method described above is characterized by having excellent lip moisturizing power, stability against ultraviolet rays and antioxidant effects in addition to the antimicrobial and cytoprotective effects described above.

According to one embodiment of the invention, each of the compositions to the lips for the cosmetic composition containing the natural pigments according to the present invention, and then measured the oil and moisture, as a result, the natural pigments of the present invention In the case of the cosmetic composition prepared using the most appeared to have excellent moisturizing power (see Experimental Example 2).

In addition, according to another embodiment of the present invention, after irradiating ultraviolet rays to each of the cosmetic composition for the lip prepared using each natural pigment and analyzed the stability by absorbance measurement, despite the 12-hour long-term UV irradiation Compositions using natural pigments showed almost the same absorbance as the group not irradiated with ultraviolet rays (see Experimental Example 3).

Therefore, it can be seen from the results that the cosmetic composition for lips of the present invention is excellent in moisturizing power and discoloration stability against ultraviolet rays.

In addition, the cosmetic composition for lips of the present invention is characterized by excellent antioxidant activity, according to one embodiment of the present invention, the total phenolic compound content, flavonoid content, free oxygen scavenging activity and nitrite scavenging ability of natural pigment-containing cosmetic composition is measured As a result of analyzing the antioxidant activity, the natural pigment was found to contain a large amount of phenol and flavonoids (see Table 4), and it was shown that the free oxygen scavenging activity, nitrite scavenging activity and tyrosinase inhibitory activity (Table 5). Reference).

Therefore, the cosmetic composition for lips of the present invention is characterized by excellent antibacterial effect, UV protection effect and antioxidant effect, can be used in the manufacture of a multifunctional lip cosmetics that can produce a clean, healthy and natural lip color.

In addition, the cosmetic composition for lips of the present invention can be prepared in a formulation such as lipstick, lip gloss, lip pencil, lip balm, and lip cream by a conventional manufacturing method, the cosmetic composition for lips of the present invention is used alone or in duplicate It can be used by overlapping application with other cosmetic compositions other than this invention. In addition, the cosmetic composition for lips according to the present invention can be used according to a conventional method of use, the number of times of use may vary depending on the user's skin condition or taste.

Hereinafter, the present invention will be described in more detail with reference to Examples. These examples are only for illustrating the present invention in more detail, it will be apparent to those skilled in the art that the scope of the present invention is not limited to these examples.

&Lt; Example 1 >

Preparation of natural pigment

The present inventors used to prepare natural pigments from each natural material as follows for the manufacture of a cosmetic composition for lips safe to the human body. In other words, black rice, mulberry leaves, turmeric, grape peel, red cabbage, bitter gourd, mulberry, jichi, baeknyeoncho and onion peels are purchased on the market, and these are lyophilized and powdered to a fine density, that is, a diameter of 100 ~ 200㎛ After that, they are all applied to a natural lip care product, so for safety, they are used by dissolving in distilled water without using any organic solvent. At this time, some poorly soluble samples were dissolved by using a magnetic stirrer (Magnetic Stirrer) and then used for the experiment.

Natural colors and color classifications used in the experiments are shown in FIG. 1 and Table 1 below.

Material source Class of coloring matter Red & Purple group
red cabbage
grape peel
cactus fruit
gromwell root
Antocyanins
Antocyanins
Antocyanins
Antocyanins Yellow group
mature bitter melon
Rehmannia glutinosa
onion peel
Carotinoids (including Xanthophylls)
Carotinoids (including Xanthophylls)
Carotinoids (including Xanthophylls) Black group
black rice
mulberry
Antocyanins
Antocyanins Green group
mulberry leave
Chlororolls

< Example  2>

Antimicrobial Activity Assay

In order to determine the antimicrobial activity of each natural pigment extract obtained in Example 1, agar plate diffusion (disk agar plate diffusion method) method was used. That is, a medium suitable for the test microorganisms as shown in Table 2 was made, and the test microorganisms were cultured at a concentration of 10 ⁷ CFU / mL in the soft agar. Then, aliquots were placed in a petri dish, placed on a paper disc, and 40 μl of sample extracts were incubated for 24 hours to observe the formation of inhibitory rings. When the inhibitory ring was formed within 24 hours, it was determined that the antimicrobial activity was positive, and the diameter of the inhibiting ring was measured and compared.

Strains Cultivarion conditions Gram - positive bacteria
Bacillus subtilis (ATCC 6633)
Micrococcus luteus (KCCM 11326)
30 ° C, Trypticase soy agar (BBL)
30 ℃, Nutrient agar Gram - Negative bacteria
Escherichia coli (ATCC 25922)
Salmonella typhymurium (KCCM 40253)
Vibrio parahaemdyticus (ATCC 17802)
Proteus mirabilis (ATCC 7002)
37 ° C, Trypticase soy agar (BBL)
30 ℃, Medium 211
37 ° C., Nutrient agar with 3% NaCl
37 ℃, Nutrient agar

As a result of examining the antimicrobial activity of the natural pigment extract of the present invention, as shown in Figure 2a, Figure 2b, Figure 2c, Figure 2d, Figure 2e and Figure 2f, Gram-positive bacteria Gram-positive strain Bacillus subtilis, Micrococcus luteus and Escherichia , a Gram-negative strain coli , Vibrio parahaemdyticus, Proteus mirabilis , Salmonella Typhymurium showed inhibitory ring in all natural pigments, and showed high antimicrobial activity, especially in mulberry leaves, mulberry leaves, grape skins and turmeric.

< Example  3>

On skin cells  UV protection effect analysis

In order to find out whether natural pigments have a sunscreen effect on skin cells, we first analyzed the effects of natural pigments on skin cells. For this purpose, the appropriate concentration was set for each natural pigment, and the concentration of 50 ㎍ / ml was used for mulberry leaves, Yeoju fruit and gardenia, and the concentration of 500 ㎍ / ml for purple sweet potato, yogurt, and black rice. The effect on the was analyzed.

In addition, the skin cells were irradiated with UV at 50 mJ / cm ² , and the UV-blocking effect was investigated by treating the pigment extraction solvent fractions of natural pigment mulberry leaf, yeast fruit, purple sweet potato, yogurt, gardenia and black rice, respectively.

As a result, as shown in Figure 3, mulberry leaf pigment, yew fruit pigment, yellow-yellow pigment and black pigment itself did not appear to affect the apoptosis of skin cells.

In addition, as shown in Figure 4, the natural pigment extract was shown to have an effect of inhibiting apoptosis by ultraviolet rays, and these results are also shown in Figure 5, in the case of the control group, the cell death promoting protein when irradiated with ultraviolet rays Phosphorus Bax expression was increased, and the expression of apoptosis inhibiting protein Bcl-2 was shown to be decreased, whereas the expression of Bax, apoptosis promoting factor, was significantly suppressed in the natural pigment extract treatment group of the present invention. Appeared.

Therefore, the present inventors found that the natural pigments extracted in the present invention are not only very stable to the skin but also have an activity of inhibiting skin cell death by ultraviolet rays.

< Example  4>

Lips using natural pigment of the present invention Cosmetics  Preparation of the composition

In order to prepare a cosmetic composition for lips comprising a natural pigment extract, the finely powdered natural pigment obtained in Example 1 was dissolved in a plant extract extracted with distilled water using a magnetic stirrer to form a pigment extract, and filtered The water was removed. The pigment extract, from which the residue was removed, was transferred to a heat-resistant container, heated to about 70 ° C. on a hot plate, and mixed with glycerin and natural betaine as an additive. At the same time, oil, butter, and wax materials are put in another heat-resistant container, mixed well and stirred to dissolve completely and heated to around 70 ° C. on a hot plate, and the pigment extract is mixed with a completely dissolved oil-based material with a spoon for reagents. Stir well and pour in little by little to mix well. The mixture was stirred well for about 15 minutes using a hand blender, and all the ingredients were mixed well, and the water-in-oiled composition was cooled slowly at room temperature, and then mixed with an appropriate amount of various additives to prepare a thin gel-type pigment mixture composition. Completed. Detailed materials for preparing such a pigment extract-containing emulsion composition are shown in Table 3 below.

Preparation Example 1 Preparation Example 2 Production Example 3 Production Example 4 Production Example 5 Production Example 6 Preparation Example 7 Preparation Example 8 content(%) Natural materials
(Color Extract) Black rice Mulberry leaf Yellow Grape peel Red Cabbage Yeoju Audi Onion peel 20 Plant extract licorice
extract,
Schisandra
extract Eoseongcho
extract green tea
extract Calendula
extract calamus
extract Ginseng
extract Donkey
extract Ginkgo leaves
extract 5 oil Grape seed
oil,
coconut
oil Avocado Oil, Coconut
oil Jojoba
oil,
Grape seed
oil Jojoba
oil,
Palma Christi
oil Macada
Mia
Nut oil Sweet Almond Oil,
coconut
oil Evening pride
(Flowers, seeds) oil Camellia
Oil, calendula oil 48 butter cocoa
butter Jojoba
butter Mango Butter Shea butter cocoa
butter Mango Butter Shea butter Jojoba
butter 12 Wax Candelilla wax Wax olive
Oil painting wax  Montawax Emulsity
Huaxing Wax Emulsity
Huaxing Wax  Montawax Wax 5 Additive Vegetable
glycerin Vegetable
glycerin Vegetable
glycerin Vegetable
glycerin Vegetable
glycerin Vegetable
glycerin Vegetable
glycerin Vegetable
glycerin 2 receptivity
natural
Betaine receptivity
natural
Betaine receptivity
natural
Betaine receptivity
natural
Betaine receptivity
natural
Betaine receptivity
natural
Betaine receptivity
natural
Betaine receptivity
natural
Betaine 2 Essential
oil Essential
oil Essential
oil Essential
oil Essential
oil Essential
oil Essential
oil Essential
oil 2 natural
Vitamin E natural
Vitamin E natural
Vitamin E natural
Vitamin E natural
Vitamin E natural
Vitamin E natural
Vitamin E natural
Vitamin E 2 natural
antiseptic natural
antiseptic natural
antiseptic natural
antiseptic natural
antiseptic natural
antiseptic natural
antiseptic natural
antiseptic 2 Total content 100

< Experimental Example  1>

Antioxidant and Whitening Effect Analysis

In order to find out whether the natural pigment-containing lip cosmetic composition prepared in Example 4 has an antioxidant effect and a whitening effect, the total phenolic compound content, flavonoid content, free oxygen scavenging activity and nitrite scavenging ability according to methods known in the art Antioxidant activity was measured and Tyrosinase inhibitory activity was measured to determine the whitening effect.

Sample Total polyphenol
(占 퐂 / ml) Total flavonoid
(占 퐂 / ml) grape peel mixed composition 245.1 ± 13.8 153.5 ± 16.1 mulberry mixed composition 320.7 ± 18.7 261.8 ± 22.5 paprika mixed composition  61.5 ± 6.6  25.7 ± 3.1 cactus fruit mixed composition 287.7 ± 15.5 227.4 ± 17.6 gromwell root mixed composition 259.2 ± 21.3 205.6 ± 15.8

Sample DPPH radical
scavenging activity
(RC ₅₀ , μg / ml) Nitrate scavenging
activity
(% of control) Tyrosinase
inhibitory activity
(% of control) grape peel mixed composition 525.2 ± 22.5 71.3 ± 3.4 20.3 ± 2.2 mulberry mixed composition 576.1 ± 31.7 62.5 ± 3.1 17.5 ± 2.6 paprika mixed composition 621.3 ± 28.3 65.2 ± 6.5 19.2 ± 1.8 cactus fruit mixed composition 556.8 ± 32.6 77.1 ± 7.8 23.4 ± 2.5   gromwell root mixed composition 612.2 ± 35.1 59.8 ± 5.2 17.1 ± 1.8

As a result of analyzing the functionality of the cosmetic composition for the lips, as shown in Table 4, in the case of the mixed pigments of the OD pigment, the total phenolic compound content of 320.7㎍ / ㎖, flavonoid content 261.8㎍ / ㎖ to have the highest content appear. In addition, as shown in Table 5, in the case of grape bark pigment composition, the amount of the sample required to inhibit the oxidation by 50% in the free oxygen scavenging ability of the mixed composition was 525.2 ㎍ / ㎖ showed high scavenging activity, The nitrite scavenging activity showed 77.1% scavenging activity compared to the control group, and the inhibition activity against tyrosinase enzyme was 23.4%. The data values of Table 4 and Table 5 represent the mean value ± standard error.

< Experimental Example  2>

Lips skin Moisturizing  analysis

In order to measure the moisturizing power of the natural pigment-containing emulsion composition, 10 women in their 20s to 40s determined to have normal lip skin characteristics were selected. Then, the pigment mixture composition for each natural pigment type was applied to the lip skin, and the moisturizing retention effect was measured at 1 hour intervals using a moisture meter.

Oil  Evaluation standard Moisture Evaluation Criteria Moisture content 33% less than 34-37% 38-42% 43-46% 47% or more Skin type Very dry skin Dry skin Normal skin Moist skin Very moist skin Oil Evaluation Criteria Oil content One 2 3 4 5 Skin type Very dry skin Dry skin Normal skin Oily skin Very oily
Many skin

Composition type moisture(%) Oil 0h 1h 2h 0h 1h 2h Red Cabbage 53 48 42 5 3 3 Audi 53 47 42 5 3 2 Purple sweet potato 49 47 41 5 3 2 Black rice 47 42 37 4 3 2 Grape 52 41 39 5 4 2 Red Beat 53 42 36 5 3 2 Government office 56 43 37 4 3 2 Gardenia 54 41 39 4 3 2 Yellow 52 41 36 5 3 2 paprika 49 42 40 5 3 2 Mulberry leaf 53 46 42 5 4 3 Yeoju 55 45 42 5 4 3 Onion peel 53 40 36 4 3 2 Centennial 55 47 40 5 4 3 Tired 56 42 39 4 3 2

As a result of measuring the moisture and oil content over time to determine the moisturizing power of the natural pigment mixture composition for the lip care product, as shown in Table 7 above, it was slightly different depending on the type of pigment and time, but overall excellent moisturizing power It was found to have.

< Experimental Example  3>

UV Stability Analysis

In order to determine whether the natural pigment mixture composition is modified against UV rays, ultraviolet rays are irradiated at 50 mJ / cm ² to the mixed composition for each natural pigment type using an ultraviolet lamp, and the change in absorbance of each natural pigment mixture composition is 3 hours apart. The stability was analyzed over time, and the absorbance analysis was measured using an optical microscope.

Composition type Optical density 0h 3h 6h 9h 12h Red Cabbage 0.647 0.661 0.673 0.681 0.651 Audi 0.697 0.697 0.698 0.729 0.676 Purple sweet potato 1.229 1.227 1.189 1.217 1.241 Black rice 2.171 2.166 2.171 2.164 2.164 Grape 1.342 1.340 1.340 1.338 1.340 Red Beat 1.243 1.271 1.286 1.268 1.250 Government office 0.813 0.868 0.853 0.846 0.820 Gardenia 0.870 0.855 0.869 0.864 0.856 Yellow 1.458 1.454 1.463 1.453 1.454 paprika 1.108 1.049 1.045 1.049 1.050 Mulberry leaf 1.205 1.189 1.160 1.181 1.179 Yeoju 3.577 3.568 3.569 3.543 3.569 Onion peel 1.445 2.295 2.297 2.293 2.295 Centennial 1.962 1.961 1.960 1.958 1.959 Tired 2.569 2.563 2.562 2.557 2.559

As a result, as shown in Table 8, as a result of observing the color tone change of the composition according to the ultraviolet irradiation for a total of 12 hours, compared with 0h of the pigment mixture composition not irradiated with ultraviolet radiation There was little change in absorbance.

Therefore, the natural pigment mixture composition according to the present invention showed excellent antioxidant and whitening effect as a whole, excellent moisturizing power and discoloration stability against ultraviolet rays.

So far I looked at the center of the preferred embodiment for the present invention. It will be understood by those skilled in the art that various changes in form and details may be made therein without departing from the spirit and scope of the invention as defined by the appended claims. Therefore, the disclosed embodiments should be considered in an illustrative rather than a restrictive sense. The scope of the present invention is defined by the appended claims rather than by the foregoing description, and all differences within the scope of equivalents thereof should be construed as being included in the present invention.

Claims (7)

Lip cosmetic composition comprising at least one natural pigment selected from the group consisting of black rice, mulberry leaves, turmeric, grape peel, red cabbage, bitter gourd, mulberry, jichi, baeknyeoncho and onion peel as an active ingredient. The method of claim 1,
The black rice, mulberry leaves, turmeric, grape peel, red cabbage, bitter gourd, mulberry, jichi, baeknyeoncho or onion peel is a cosmetic composition for lips, characterized in that it comprises 5-20% by weight relative to the total weight of the composition. The method of claim 1,
The composition further comprises a wax and oil cosmetic composition for lips. The method of claim 3, wherein
The wax and oil is a cosmetic composition for the lips, characterized in that 5 to 20% by weight of the wax and 20 to 50% by weight relative to the total weight of the composition. The method of claim 1,
The composition is a cosmetic composition for lips, characterized in that it has an antimicrobial effect, sunscreen effect, antioxidant effect or whitening effect. Freeze-dried at least one selected from the group consisting of black rice, mulberry leaves, turmeric, grape peel, red cabbage, bitter gourd, mulberry, jichi, baeknyeoncho and onion peel, and pulverized to a diameter of 100 ~ 200㎛ to obtain a natural pigment powder Method for producing a cosmetic composition for lips comprising the step of. The method according to claim 6,
The composition is a lipstick, lip gloss, lip pencil, lip balm (Lipbalm) and a lip balm (lip balm) characterized in that the manufacturing method for the preparation of a cosmetic composition for the lips, characterized in that it is prepared from the group consisting of lip cream.

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