KR20100111775A - Fabric softener composition for radiating far-infrared ray - Google Patents
Fabric softener composition for radiating far-infrared ray Download PDFInfo
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- KR20100111775A KR20100111775A KR1020090030145A KR20090030145A KR20100111775A KR 20100111775 A KR20100111775 A KR 20100111775A KR 1020090030145 A KR1020090030145 A KR 1020090030145A KR 20090030145 A KR20090030145 A KR 20090030145A KR 20100111775 A KR20100111775 A KR 20100111775A
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- softener composition
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- 239000000203 mixture Substances 0.000 title claims abstract description 71
- 239000002979 fabric softener Substances 0.000 title abstract description 27
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 42
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 claims abstract description 32
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims abstract description 26
- 230000005855 radiation Effects 0.000 claims abstract description 24
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Chemical compound OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims abstract description 16
- 229910001629 magnesium chloride Inorganic materials 0.000 claims abstract description 16
- MKJXYGKVIBWPFZ-UHFFFAOYSA-L calcium lactate Chemical compound [Ca+2].CC(O)C([O-])=O.CC(O)C([O-])=O MKJXYGKVIBWPFZ-UHFFFAOYSA-L 0.000 claims abstract description 14
- 235000011086 calcium lactate Nutrition 0.000 claims abstract description 14
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims abstract description 13
- 239000001527 calcium lactate Substances 0.000 claims abstract description 13
- 229960002401 calcium lactate Drugs 0.000 claims abstract description 13
- 229910000027 potassium carbonate Inorganic materials 0.000 claims abstract description 13
- 239000001509 sodium citrate Substances 0.000 claims abstract description 12
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 claims abstract description 12
- 239000000835 fiber Substances 0.000 claims description 28
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims description 24
- 239000008213 purified water Substances 0.000 claims description 16
- 239000008103 glucose Substances 0.000 claims description 13
- 239000001103 potassium chloride Substances 0.000 claims description 12
- 235000011164 potassium chloride Nutrition 0.000 claims description 12
- 229930006000 Sucrose Natural products 0.000 claims description 11
- 238000009987 spinning Methods 0.000 claims description 9
- 235000011147 magnesium chloride Nutrition 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 6
- 235000011181 potassium carbonates Nutrition 0.000 claims description 6
- 235000011083 sodium citrates Nutrition 0.000 claims description 6
- 239000000654 additive Substances 0.000 claims description 3
- 239000006185 dispersion Substances 0.000 claims description 3
- 239000003381 stabilizer Substances 0.000 claims description 3
- 230000000996 additive effect Effects 0.000 claims 1
- 230000004060 metabolic process Effects 0.000 abstract description 5
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 abstract description 3
- 239000001110 calcium chloride Substances 0.000 abstract description 3
- 229910001628 calcium chloride Inorganic materials 0.000 abstract description 3
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 abstract 2
- 229910000019 calcium carbonate Inorganic materials 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 29
- 235000019645 odor Nutrition 0.000 description 16
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- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 11
- 239000003093 cationic surfactant Substances 0.000 description 10
- 239000004753 textile Substances 0.000 description 10
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- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 7
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- 238000012360 testing method Methods 0.000 description 7
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 6
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- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 4
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- LSDPWZHWYPCBBB-UHFFFAOYSA-N Methanethiol Chemical compound SC LSDPWZHWYPCBBB-UHFFFAOYSA-N 0.000 description 4
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- VWDWKYIASSYTQR-UHFFFAOYSA-N sodium nitrate Chemical compound [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 description 4
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- MWUXSHHQAYIFBG-UHFFFAOYSA-N nitrogen oxide Inorganic materials O=[N] MWUXSHHQAYIFBG-UHFFFAOYSA-N 0.000 description 3
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- 239000003755 preservative agent Substances 0.000 description 3
- SVTBMSDMJJWYQN-UHFFFAOYSA-N 2-methylpentane-2,4-diol Chemical compound CC(O)CC(C)(C)O SVTBMSDMJJWYQN-UHFFFAOYSA-N 0.000 description 2
- CNGYZEMWVAWWOB-VAWYXSNFSA-N 5-[[4-anilino-6-[bis(2-hydroxyethyl)amino]-1,3,5-triazin-2-yl]amino]-2-[(e)-2-[4-[[4-anilino-6-[bis(2-hydroxyethyl)amino]-1,3,5-triazin-2-yl]amino]-2-sulfophenyl]ethenyl]benzenesulfonic acid Chemical compound N=1C(NC=2C=C(C(\C=C\C=3C(=CC(NC=4N=C(N=C(NC=5C=CC=CC=5)N=4)N(CCO)CCO)=CC=3)S(O)(=O)=O)=CC=2)S(O)(=O)=O)=NC(N(CCO)CCO)=NC=1NC1=CC=CC=C1 CNGYZEMWVAWWOB-VAWYXSNFSA-N 0.000 description 2
- IKHGUXGNUITLKF-UHFFFAOYSA-N Acetaldehyde Chemical compound CC=O IKHGUXGNUITLKF-UHFFFAOYSA-N 0.000 description 2
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
- C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/07—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof
- D06M11/11—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof with halogen acids or salts thereof
- D06M11/13—Ammonium halides or halides of elements of Groups 1 or 11 of the Periodic Table
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/07—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof
- D06M11/11—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof with halogen acids or salts thereof
- D06M11/155—Halides of elements of Groups 2 or 12 of the Periodic Table
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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Abstract
Description
본 발명은 원적외선 방사용 섬유유연제 조성물에 관한 것으로, 보다 상세하게는 섬유 유연 효과가 뛰어나고, 정전기방지에 효과적이며, 원적외선을 방출해 건강증진작용을 할 수 있으며, 인체에 무해하고 친환경적이며 안전해 피부에 자극적이지 않으며, 의류에 대한 흡착성과 섬유유연성을 동시에 만족시킬 수 있는 효과가 있고, 항균 및 냄새제거에 효과적이고, 세탁효능이 증대되어 따로 쓰는 세탁세제의 사용량을 줄일 수 있고 나아가 세탁제와 유연제를 일원화시킬 수 있는 원적외선 방사용 섬유유연제 조성물에 관한 것이다.The present invention relates to a fiber softener composition for far-infrared radiation, and more particularly, it has excellent fiber softening effect, is effective in preventing static electricity, can emit far-infrared radiation and promotes health, it is harmless to humans, environmentally friendly and safe for skin. It is not irritating, and it has the effect of satisfying the adsorption and fiber flexibility of clothes at the same time, it is effective in removing antibacterial and odor, and the washing efficiency is increased, so it can reduce the amount of washing detergent used separately and furthermore, washing agent and softening agent. It relates to a far-infrared radiation fiber softener composition capable of unifying.
일반적으로 가정이나 공장에서 의류 등의 섬유제품을 세탁할 때 섬유유연제를 투입하여 의류 또는 섬유의 세탁 또는 헹굼과 동시에 유연성을 부여하기 위한 노력이 계속되어 왔다. 섬유유연제는 의류에 발생하는 정전기를 방지하고, 섬유의 유연성을 부여하기 위하여 가정에서 널리 사용되고 있으며, 그 사용량이 점차 증가하고 있는 추세이다. 최근에는 소비자들의 생활수준의 향상과 더불어, 위생 및 청 결에 대한욕구가 증가하고 보다 쾌적한 의생활을 추구하려 함에 따라, 의류에 발생할 수 있는 미생물 증식 방지 및 악취제거에 대한 관심이 늘고 있다.In general, when washing textile products such as clothing in homes or factories, efforts have been made to provide flexibility while adding a fabric softener to wash or rinse clothing or textiles. Fabric softeners are widely used in homes to prevent static electricity generated in clothing and to give the flexibility of the fiber, the amount is increasingly used. Recently, with the improvement of consumers' standard of living, the desire for hygiene and cleanliness and the pursuit of a more comfortable medical life, there is a growing interest in preventing microbial growth and odor removal that can occur in clothing.
통상의 세탁세제 또는 헹굼용 섬유유연제에 유연 기능을 부여하기 위하여 사용되는 물질로는 보통 디알킬 디메틸 암모늄염, 디알킬아미도 이미다졸리늄염 또는 디알킬아미도아민의 4급 암모늄염(Quaternary ammonium salt) 형태의 양이온 계면활성제를 사용한다.Materials used to impart softening functions to conventional laundry detergents or rinse fabric softeners are usually dialkyl dimethyl ammonium salts, dialkylamido imidazolinium salts or quaternary ammonium salts of dialkylamidoamines. In the form of cationic surfactants.
이러한 양이온 계면활성제는 의류에 일시적으로 부착되어 유연효과를 발휘한다. 하지만 의류나 섬유의 세탁을 위한 세제의 경우 유연효과를 주기 위한 양이온성 계면활성제와 세탁 효과를 위한 음이온성 계면활성제를 동시에 사용하여야만 하는데, 이 경우에 양이온성 계면활성제와 음이온성 계면활성제는 이온 결합에 의해 검화되거나, 거대 소수성 분자로 변화되어 물에 용해되기 어려워지므로, 이로 인하여 세정력이 오히려 저하될 수 있다. 또한, 의류나 섬유에 유연효과를 주기 위해서는 세탁수 내에 양이온이 존재하여 세탁과정 및 헹굼과정 동안 의류나 섬유에 흡착되어야 하지만, 음이온이 양이온과 결합되면 흡착량이 줄어들어 유연효과를 나타내기 어려워진다.These cationic surfactants temporarily attach to clothes and exert a softening effect. However, detergents for washing clothes or textiles must use both cationic surfactants for softening effect and anionic surfactants for washing effect. In this case, cationic surfactants and anionic surfactants are ion-bonded. It is difficult to dissolve in water because it is converted into a large hydrophobic molecule by saponification, or the washing power may be lowered. In addition, in order to give a softening effect to clothes or fibers, cations are present in the wash water to be adsorbed onto the clothes or fibers during the washing process and the rinsing process. However, when the anions are combined with the cations, the adsorption amount decreases, making it difficult to exhibit the softening effect.
이와 같은 이유 때문에 종래의 섬유유연제로는 양이온 계면활성제, 및 양이온 계면활성제와 결합하지 않는 비이온 계면활성제를 포함하는 세탁 세제가 제안되었다. 그러나 양이온 계면활성제는 시간이 지나면서 산화되거나 자체 분해에 의해서 질소 산화물로 변하면서 의류나 섬유에 남아 백색도를 떨어뜨리는 문제점이 있을 뿐만 아니라, 양이온 계면활성제가 의류에 누적됨에 따라 흰색 의류나 섬유가 누렇게 변하는 황변 현상이 발생하게 된다. 또한, 음이온 전하를 띠고 있는 형광증백제를 세탁 세제에 사용할 경우 양이온 계면활성제가 형광 증백제와 결합하여 백색도를 감소시키게 된다. For this reason, laundry detergents containing a cationic surfactant and a nonionic surfactant which does not bind with a cationic surfactant have been proposed as a conventional fabric softener. However, cationic surfactants not only have a problem of remaining white in clothing or textiles as they are oxidized over time or changed into nitrogen oxides by self-decomposition, and the white clothing or fibers become yellow as the cationic surfactant accumulates in the clothing. Changing yellowing will occur. In addition, when a fluorescent brightener having an anion charge is used in a laundry detergent, a cationic surfactant is combined with the fluorescent brightener to reduce whiteness.
의류를 장시간 착용하는 경우, 또는 우천시나 하절기에 의류 또는 섬유제품을 불완전하게 말릴 경우, 세균이나 곰팡이가 증식하기 쉽고, 의류 및 섬유제품에서 악취가 나게 된다. 이 같은 경우, 의류 및 섬유제품에 번식한 세균이나 곰팡이에 의하여 각종 피부질환이 발병할 수도 있고, 악취로 말미암아 의복 착용시 쾌적감이 떨어질 수도 있다는 문제점이 있다.When clothing is worn for a long time, or when clothing or textile products are incompletely dried during the rainy or summer season, bacteria or mold are easily proliferated, and odors are produced in the clothing and textile products. In this case, various skin diseases may occur due to bacteria or fungi propagated in clothing and textile products, and there is a problem that comfort may be impaired when wearing clothes due to bad smell.
따라서 의류 및 섬유제품에 세균 및 곰팡이의 번식을 방지하기 위하여, 항균제를 적용한 섬유유연제 조성물이 제조되어 왔다. 그러나 종래의 섬유유연제 조성물에 적용된 항균제는 항균제 원료 자체의 항균력은 우수하나, 실제로 섬유유연제에 적용 시에는 그 희석비율 때문에 항균력을 거의 발휘하지 못한다는 문제점이 있다.Therefore, in order to prevent the growth of bacteria and mold in clothing and textile products, a fabric softener composition applying an antimicrobial agent has been prepared. However, the antimicrobial agent applied to the conventional fabric softener composition has an excellent antimicrobial activity of the raw material of the antimicrobial agent itself, but when applied to the fabric softener, there is a problem in that the antimicrobial activity is hardly exhibited due to its dilution ratio.
또한, 종래의 섬유유연제는 섬유 유연효과를 인지할 수 없을 정도로 그 효과가 미미하거나, 반복세탁에 의해 의류나 섬유에 누적되어 나타나는 황변 현상을 극복하지 못하였고, 그 효과의 지속성 또한 매우 짧은 단점이 있다.In addition, the conventional fabric softeners are insignificant to the extent that the fiber softening effect is not recognizable, or the yellowing phenomenon accumulated in clothing or fibers by repeated washing does not overcome, and the sustainability of the effect is also very short. have.
이와 같이 의류 또는 섬유에 유연효과를 주기 위한 다양한 기술들이 개발되고 있으며, 최근에는 섬유유연제에 향 물질을 첨가하거나 항균 및 악취제거 기능이 뛰어난 기능성 섬유유연제에 대한 요구가 점차 증가하고 있는 추세이다. 따라서, 섬유유연제의 기능을 다양화, 고급화하는 방안에 대한 연구가 이루어지고 있다.As described above, various technologies have been developed to give a flexible effect to clothing or textiles. Recently, the demand for functional textile softeners having excellent antibacterial and odor removal capabilities is added to the fabric softeners. Therefore, research has been made on ways to diversify and enhance the function of the fabric softener.
이에 본 발명자들은 기존의 섬유유연제의 기능이 강화된 섬유유연제 조성물을 개발하던 중, 염화칼륨, 탄산칼륨, 염화마그네슘, 젖산칼슘, 구연산나트륨, 정백당, 정제포도당 및 물을 포함하는 조성물이 원적외선을 방사하여 항균 및 악취제거, 정전기 방지에 효율적이고 세탁효능이 증대된 효과가 있음을 발견함으로써 본 발명을 완성하였다.The inventors of the present invention, while developing a fiber softener composition strengthening the function of the conventional fiber softener, the composition containing potassium chloride, potassium carbonate, magnesium chloride, calcium lactate, sodium citrate, white sugar, refined glucose and water to emit far infrared rays The present invention has been completed by discovering that the antimicrobial and odor removal effect is effective in preventing static electricity and the washing effect is increased.
따라서 본 발명의 목적은 염화칼륨, 탄산칼륨, 염화마그네슘, 젖산칼슘, 구연산나트륨, 정백당, 정제포도당 및 물을 포함하는 원적외선 방사용 섬유유연제 조성물을 제공하는 것이다. Accordingly, it is an object of the present invention to provide a far-infrared spinning fiber softener composition comprising potassium chloride, potassium carbonate, magnesium chloride, calcium lactate, sodium citrate, white sugar, refined glucose and water.
상기와 같은 본 발명의 목적을 달성하기 위해서, 본 발명은 염화칼륨, 탄산칼륨, 염화마그네슘, 젖산칼슘, 구연산나트륨, 정백당, 정제포도당 및 물을 포함하는 원적외선 방사용 섬유유연제 조성물을 제공한다.In order to achieve the object of the present invention as described above, the present invention provides a far-infrared radiation fiber softener composition comprising potassium chloride, potassium carbonate, magnesium chloride, calcium lactate, sodium citrate, white sugar, refined glucose and water.
또한, 본 발명은 50~60℃로 가열한 정제수 100 중량부에 대해 염화칼륨 8~10 중량부, 탄산칼륨 40~60 중량부, 염화마그네슘 1~2 중량부, 젖산칼슘 1~2 중량부, 구연산나트륨 3~7 중량부, 정백당 15~30 중량부 및 정제포도당 2~5 중량부를 포함하는 원적외선 방사용 섬유유연제 조성물을 제공한다.In addition, the present invention is 8 to 10 parts by weight of potassium chloride, 40 to 60 parts by weight of potassium carbonate, 1 to 2 parts by weight of magnesium chloride, 1 to 2 parts by weight of calcium lactate, citric acid to 100 parts by weight of purified water heated to 50 to 60 ℃. It provides a far-infrared spinning fiber softener composition comprising 3 to 7 parts by weight of sodium, 15 to 30 parts by weight of white sugar and 2 to 5 parts by weight of refined glucose.
본 발명에 따른 원적외선 방사용 섬유유연제 조성물은 섬유 유연 효과가 뛰어나고, 정전기방지에 효과적이며, 원적외선을 방출함으로써 체내의 신진대사를 원활히 하고, 혈액순환을 증진시키며, 피부 보습효과도 나타내는 효과가 있다.The fiber softener composition for far-infrared radiation according to the present invention has an excellent fiber softening effect, is effective in preventing static electricity, and emits far infrared rays, thereby facilitating metabolism in the body, enhancing blood circulation, and also having a skin moisturizing effect.
또한, 본 발명에 따른 원적외선 방사용 섬유유연제 조성물은 인체에 무해하 고 친환경적이며 안전해 피부에 자극적이지 않으며, 의류에 대한 흡착성과 섬유유연성을 동시에 만족시킬 수 있는 효과가 있다.In addition, the far-infrared radiation softener composition according to the present invention is harmless to the human body, environmentally friendly and safe, not irritating to the skin, and has the effect of simultaneously satisfying the adsorption and fiber flexibility of clothing.
또한, 본 발명에 따른 원적외선 방사용 섬유유연제 조성물은 항균 및 냄새제거에 효과적이고, 세탁효능이 증대되어 따로 쓰는 세탁세제의 사용량을 줄일 수 있고 나아가 세탁제와 유연제를 일원화시킬 수 있는 효과가 있다.In addition, the far-infrared radiation softener composition according to the present invention is effective in removing the antibacterial and odor, and the washing effect is increased to reduce the amount of the laundry detergent used separately, and furthermore it is possible to unify the laundry and softening agent.
본 발명은 염화칼륨, 탄산칼륨, 염화마그네슘, 젖산칼슘, 구연산나트륨, 정백당, 정제포도당 및 물을 포함하는 원적외선 방사용 섬유유연제 조성물을 제공한다. 보다 바람직하게는, 50~60℃로 가열한 정제수 100 중량부에 대해 염화칼륨 8~10 중량부, 탄산칼륨 40~60 중량부, 염화마그네슘 1~2 중량부, 젖산칼슘 1~2 중량부, 구연산나트륨 3~7 중량부, 정백당 15~30 중량부 및 정제포도당 2~5 중량부를 포함하는 원적외선 방사용 섬유유연제 조성물을 제공한다.The present invention provides a far-infrared spinning fiber softener composition comprising potassium chloride, potassium carbonate, magnesium chloride, calcium lactate, sodium citrate, white sugar, refined glucose, and water. More preferably, 8 to 10 parts by weight of potassium chloride, 40 to 60 parts by weight of potassium carbonate, 1 to 2 parts by weight of magnesium chloride, 1 to 2 parts by weight of calcium lactate, and citric acid to 100 parts by weight of purified water heated to 50 to 60 ° C. It provides a far-infrared spinning fiber softener composition comprising 3 to 7 parts by weight of sodium, 15 to 30 parts by weight of white sugar and 2 to 5 parts by weight of refined glucose.
본 발명의 일실시예에서는 50~60℃로 가열한 정제수 1ℓ를 기준으로 염화칼륨 80~100g, 탄산칼륨 400~600g, 염화마그네슘 10~20g, 구연산나트륨 30~70g, 젖산칼슘 10~20g, 정백당 150~300g 및 정제포도당 20~50g을 첨가하고 용해하여 이온화시킴으로써 원적외선 방사용 섬유유연제 조성물을 제조하였다.In one embodiment of the present invention, based on 1 liter of purified water heated to 50 ~ 60 ℃ potassium chloride 80 ~ 100g, potassium carbonate 400 ~ 600g, magnesium chloride 10 ~ 20g, sodium citrate 30 ~ 70g, calcium lactate 10 ~ 20g, 150 per white Far-infrared spinning fabric softener composition was prepared by adding ~ 300 g and 20-50 g of purified glucose, dissolving, and ionizing the same.
본 발명에 따른 원적외선 방사용 섬유유연제 조성물을 제조하기 위한 상기 물은 물속에 존재하는 원생생물 및 이물질이 제거되도록 취수원에서 보내진 원수를 당업계에 공지된 방법에 따라 정제할 수 있다. 바람직하게는 여과를 통해 수행할 수 있으며, 더욱 바람직하게는 활성탄 여과조 또는 초정밀 여과 장치를 이용하여 수행할 수 있다.The water for preparing the far-infrared spinning softener composition according to the present invention can be purified according to a method known in the art so that the raw water sent from the water intake source to remove the protists and foreign substances present in the water. Preferably, it may be carried out through filtration, and more preferably, it may be performed using an activated carbon filtration tank or an ultra-precision filtration device.
이후, 여과를 통해 이물질이 제거된 정제수에 미네랄 물질들을 용해시켜 본 발명의 조성물을 제조할 수 있으며, 바람직하게는 상기 정제수를 가열하여 사용할 수 있다. 본 발명에 따른 조성물의 제조에 있어서 가열한 정제수를 사용하는 이유는 차가운 정제수를 사용할 경우, 미네랄 성분들이 완전히 용해되지 않은 채 침전물로 남아있을 수 있기 때문이며, 따라서 상기 가열은 혼합된 미네랄 성분들이 침전되지 않을 정도로 정제수를 가열하는 것이 바람직하며, 더욱 바람직하게는 50℃ 내지 60℃의 온도로 가열하는 것이 바람직하다.Thereafter, the composition of the present invention may be prepared by dissolving mineral substances in purified water from which foreign substances have been removed through filtration, and preferably, the purified water may be heated. The reason for using heated purified water in the preparation of the composition according to the present invention is that when cold purified water is used, the mineral components may remain as precipitates without being completely dissolved, so that the heating does not precipitate the mixed mineral components. It is preferable to heat purified water so that it may not, and it is more preferable to heat it to the temperature of 50 degreeC-60 degreeC more preferably.
따라서 상기 방법으로 제조된 본 발명의 원적외선 방사용 섬유유연제 조성물은 물속에서 이온화되어 알칼리성을 띄는 칼륨, 나트륨, 마그네슘 및 칼슘의 미네랄 성분들을 포함한다.Therefore, the far-infrared radiation softener composition of the present invention prepared by the above method contains mineral components of potassium, sodium, magnesium and calcium that are ionized in water and become alkaline.
특히, 본 발명에 사용된 미네랄 성분 중 칼륨은 세포내 액의 주된 양이온으로 세포 외액의 주된 양이온인 나트륨과 함께 삼투압과 수분 평형 조절에 관여하며, 산과 알칼리의 균형 유지에 필수적인 역할을 한다. 그러나 칼륨이 결핍되면 조직분해 또는 설사나 구토 증상이 유발될 수 있으며, 반면 칼륨을 과잉 섭취하게 되면 갑상선 기능 저하 등을 유발시킬 수 있다. 따라서 본 발명의 조성물은 체내에서 부작용이 없도록 정제수 1000ml에 대하여 염화칼륨을 80~100g 포함하는 것이 바람직하며, 탄산칼륨은 400~600g 포함하는 것이 바람직하다.In particular, potassium in the mineral component used in the present invention is a major cation of intracellular fluids and is involved in the osmotic pressure and water balance control together with sodium, the main cation of extracellular fluids, and plays an essential role in maintaining the balance between acid and alkali. However, potassium deficiency can cause histolysis, diarrhea or vomiting, whereas excessive potassium can cause hypothyroidism. Therefore, the composition of the present invention preferably contains 80 to 100 g of potassium chloride with respect to 1000 ml of purified water so that there are no side effects in the body, and preferably contains 400 to 600 g of potassium carbonate.
나트륨은 칼륨과 함께 삼투압을 조절하는 기능이 있고, 세포의 물질교환에 있어서 중요한 역할을 하며, 정상적인 근육의 자극반응 및 흥분성을 유지하는데 관여 한다. 따라서, 나트륨이 결핍되면 식욕부진, 소화불량, 근육위축, 장내가스 축적 등의 원인이 될 수 있고, 나트륨이 과도하면 피로, 신경불안증, 발작, 두통 및 잇몸질환 등을 유발시킬 수 있다. 따라서 본 발명의 조성물은 정제수 1000ml에 대하여 구연산나트륨을 30~70g 포함하는 것이 바람직하다.Sodium, together with potassium, functions to regulate osmotic pressure, plays an important role in cell mass exchange, and is involved in maintaining normal muscle irritation and excitability. Therefore, lack of sodium may cause anorexia, indigestion, muscle atrophy, intestinal gas accumulation, etc., and excessive sodium may cause fatigue, nervousness, seizures, headaches and gum disease. Therefore, it is preferable that the composition of this invention contains 30-70 g of sodium citrate with respect to 1000 ml of purified water.
칼슘은 물과 매우 격렬하게 반응하기 때문에 일반적으로 알칼리성의 용액 제조에 사용이 불가능하다. 그러나 본 발명에서는 적절한 양의 칼슘을 첨가하여 다른 미네랄 성분들과 함께 단시간에 알칼리성을 유지하는 수용액을 만들 수 있게 한다. 따라서 이와 같은 점을 고려하여, 본 발명의 조성물은 정제수 1000ml에 대하여 젖산칼슘을 10~20g 포함하는 것이 바람직하다. Calcium reacts so violently with water that it is generally not available for the preparation of alkaline solutions. However, in the present invention, an appropriate amount of calcium can be added to make an aqueous solution that maintains alkalinity with other mineral components in a short time. Therefore, in view of such a point, it is preferable that the composition of this invention contains 10-20 g of calcium lactates with respect to 1000 ml of purified water.
마그네슘은 물속에서 물과 반응하여 마그네슘이 산화됨으로써 수산화이온을 형성하게 되고 형성된 수산화이온에 의해 물은 알칼리성을 띄게 되며 동시에 형성된 수소분자에 의해 환원력을 갖게 된다. 따라서 이러한 마그네슘이 본 발명의 조성물에 너무 많은 양으로 포함될 경우, 물속에서 쉽게 산화마그네슘으로 산화되어 마그네슘 표면에 산화막을 형성하기 때문에 물을 알칼리성으로 만드는 능력이 급속이 낮아지게 되며, 반면 너무 적은 양으로 포함될 경우 용액을 알칼리화하는 효과가 미미한 문제점이 있다. 이와 같은 점을 고려하여 본 발명의 조성물은 정제수 1000ml에 대하여 염화마그네슘을 10~20g 포함하는 것이 바람직하다.Magnesium reacts with water in water to form hydroxide ions as the magnesium is oxidized, and water is alkaline due to the hydroxide ions formed and at the same time has a reducing power by the hydrogen molecules formed. Therefore, when such magnesium is included in the composition of the present invention in too large a quantity, the ability to make water alkaline is rapidly lowered, because it is easily oxidized to magnesium oxide in water to form an oxide film on the surface of magnesium, while in a small amount If included, the effect of alkalizing the solution is insignificant. In view of such a point, the composition of the present invention preferably contains 10 to 20 g of magnesium chloride with respect to 1000 ml of purified water.
나아가, 포도당 및 정백당은 이온화된 미네랄 성분들이 재결합하는 것을 방지하여 용액을 안정화시키는 역할을 한다. 따라서 본 발명의 조성물은 정제수 1000ml에 대하여 정백당을 150~300g 포함하는 것이 바람직하고, 정제포도당은 20~50g 포함하는 것이 바람직하다. Furthermore, glucose and white sugar serve to stabilize the solution by preventing the ionized mineral components from recombining. Therefore, it is preferable that the composition of this invention contains 150-300 g of white sugar with respect to 1000 ml of purified water, and 20-50 g of refined glucose is preferable.
본 발명에서 기술된 상기 “원적외선”은 파장이 4㎛ 이상인 적외선을 말하는 것으로, 가시광선보다 파장이 길어서 눈에 보이지 않고 열작용이 크며 침투력이 강하다. 또, 눈에 보이지 않고 물질에 잘 흡수되며 유기화합물 분자에 대한 공진 및 공명 작용이 강한 것이 특징이다. 이러한 열작용은 각종 질병의 원인이 되는 세균을 없애는 데 도움이 되고, 모세혈관을 확장시켜 혈액순환과 세포조직 생성에 도움을 준다. 또 세포를 구성하는 수분과 단백질 분자에 닿으면 세포를 1분에 2,000번씩 미세하게 흔들어줌으로써 세포조직을 활성화하여 노화방지, 신진대사 촉진, 만성피로 등 각종 성인병 예방에 효과가 있다. 그밖에도 발한작용 촉진, 통증완화, 중금속 제거, 숙면, 탈취, 방균, 곰팡이 번식방지, 제습, 공기정화 등의 효과가 있어 다양한 산업, 의료 분야에 응용되고 있다.The term “far infrared rays” described in the present invention refers to infrared rays having a wavelength of 4 μm or more. The wavelengths are longer than visible light, and thus, are invisible, thermal action is large, and penetration is strong. In addition, it is invisible, absorbed well by the material, and has strong resonance and resonance effects on organic compound molecules. This heat action helps to eliminate the bacteria that cause various diseases, and helps to expand the capillaries and blood circulation and tissue formation. In addition, by touching the water and protein molecules that make up the cells, the cells are shaken finely 2,000 times per minute to activate cell tissue, which is effective in preventing various adult diseases such as aging, promoting metabolism, and chronic fatigue. In addition, it promotes sweating, pain relief, heavy metal removal, sleep, deodorization, antibacterial, mold propagation prevention, dehumidification, air purification, etc., and is applied to various industrial and medical fields.
상기 제조된 본 발명에 따른 원적외선 방사용 섬유유연제 조성물은 섬유 유연 효과가 뛰어나고, 정전기방지에 효과적이며, 원적외선을 방출함으로써 체내의 신진대사를 원활히 하고, 혈액순환을 증진시키며, 피부 보습효과도 나타내는 효과가 있다.The far-infrared radiation softening agent composition according to the present invention has excellent fiber softening effect, is effective in preventing static electricity, and emits far infrared rays to smooth the metabolism in the body, improve blood circulation, and also have a skin moisturizing effect. There is.
또한, 본 발명에 따른 원적외선 방사용 섬유유연제 조성물은 인체에 무해하고 친환경적이며 안전해 피부에 자극적이지 않으며, 의류에 대한 흡착성과 섬유유연성을 동시에 만족시킬 수 있는 효과가 있다.In addition, the far-infrared radiation softener composition according to the present invention is harmless to the human body, environmentally friendly and safe, not irritating to the skin, and has the effect of satisfying the adsorption and fiber flexibility for clothing at the same time.
또한, 본 발명에 따른 원적외선 방사용 섬유유연제 조성물은 항균 및 냄새제 거에 효과적이고, 세탁효능이 증대되어 따로 쓰는 세탁세제의 사용량을 줄일 수 있고 나아가 세탁제와 유연제를 일원화시킬 수 있는 효과가 있다.In addition, the far-infrared radiation softener composition according to the present invention is effective in removing the antibacterial and odor, and the washing effect is increased to reduce the amount of the laundry detergent used separately and further unify the laundry and softening agent.
본 발명에 따른 원적외선 방사용 섬유유연제 조성물은 섬유유연제의 첨가제로서 일반적으로 사용되는 향료, 방부제, 살균제, 형광증백제, 색소, 산화방지제, 소포제 등을 제품 안정성에 영향을 미치지 않는 범위 내에서 0.01 내지 5중량%로 첨가할 수 있다.Far-infrared radiation softener composition according to the present invention is a fragrance, preservatives, fungicides, fluorescent brighteners, pigments, antioxidants, antifoaming agents and the like commonly used as additives of the fabric softener within 0.01 to within the range that does not affect product stability It can be added at 5% by weight.
본 발명에 따른 섬유 유연제 조성물은 유연 성분으로서 공지의 섬유 유연제에 사용되는 양이온 계면활성제를 조성물 총중량 기준으로 5 내지 15 중량 % 포함한다. 비이온 계면활성제로는 보편적으로 섬유 유연제 조성물에 사용될 수 있는 것이면 특별히 한정되는 것은 아니며, 예를 들면 폴리옥시에틸렌 알킬에테르, 코코넛 디에탄올 아미드, 지방산 알카놀아민, 아민 옥사이드, 알킬 폴리글루코시드, 메틸 폴리에틸렌 알킬 에테르, 슈거 에테르 등으로 이루어진 군에서 선택된 1종 이상의 것을 사용할 수 있다. 상기 비이온 계면활성제는 본 발명의 섬유유연제 조성물의 총 중량을 기준으로 2 내지 15 중량 % 정도 포함하는 것이 바람직하다. 비이온 계면활성제를 2 중량 % 미만으로 사용하는 경우, 유연 효과나 정전기 방지효과 등이 미약하고, 15 중량% 초과하여 사용하는 경우에는 비경제적이기 때문이다.The fabric softener composition according to the present invention contains 5 to 15% by weight, based on the total weight of the composition, of the cationic surfactant used in the known fabric softener as the softening component. The nonionic surfactant is not particularly limited as long as it can be generally used in the fabric softener composition, for example, polyoxyethylene alkyl ether, coconut diethanol amide, fatty acid alkanolamine, amine oxide, alkyl polyglucoside, methyl One or more selected from the group consisting of polyethylene alkyl ethers, sugar ethers and the like can be used. The nonionic surfactant is preferably included in about 2 to 15% by weight based on the total weight of the fabric softener composition of the present invention. This is because, when the nonionic surfactant is used at less than 2% by weight, the softening effect or the antistatic effect is weak, and when the nonionic surfactant is used at more than 15% by weight, it is uneconomical.
특히, 본 발명에 따른 섬유유연제 조성물은 소취 또는 탈취 효과를 구비하도록, 은행잎, 녹차, 키토산의 혼합추출물을 더 포함할 수도 있다. 상기 녹차추출물은 후라보노이드 유도체인 탄닌성분과 폴리페놀류, 축합형 탄닌, 유기 고분자류 등의 복합작용에 의해 세탁후 의류에 남아있는 오염 및 암모니아, 트리메틸아민, 황 화수소, 메틸머캅탄 등의 냄새 성분을 중화 및 부가, 치환, 환원등의 화학적 탈취작용과 물리적인 포접이나 흡착, 흡수 작용등으로 냄새물질을 제거한다. 이러한 천연 혼합추출물을 사용할 경우 소취, 살균, 항균 효과의 상승작용을 나타낸다. 이러한 혼합추출물은 조성물의 총 중량을 기준으로 0.2 내지 3.0 중량 % 인 것이 바람직하다. 이 범위의 천연추출 혼합물을 포함하는 경우에 유기오염물질 등의 분해력, 소취력, 살균력 및 항균력 등이 우수한 것으로 나타난다. 상기 천연추출물의 함량이 0.2 중량 % 미만인 경우에는 소취 및 항균효과가 미미하며, 3.0 중량 % 초과하는 경우에는 함량 증가에 따른 효과의 상승이 미미하여 비경제적이다. In particular, the fabric softener composition according to the present invention may further include a mixed extract of ginkgo biloba, green tea, chitosan to have a deodorizing or deodorizing effect. The green tea extract is a complex of the tannin component of the flavonoid derivatives and polyphenols, condensed tannins, organic polymers, etc. Odor substances are removed by chemical deodorization such as neutralization, addition, substitution and reduction, and physical inclusion, adsorption and absorption. When using such a natural extract extract shows a synergistic effect of deodorant, bactericidal, antibacterial. Such mixed extract is preferably 0.2 to 3.0% by weight based on the total weight of the composition. In the case of including the natural extraction mixture in this range, it appears that the degrading power, deodorizing power, bactericidal power and antibacterial activity of organic pollutants and the like are excellent. When the content of the natural extract is less than 0.2% by weight, the deodorizing and antimicrobial effects are insignificant, and when it exceeds 3.0% by weight, the effect of increasing the content is insignificant, which is uneconomical.
본 발명에 따른 섬유유연제 조성물은 분산안정제를 더 포함한다. 분산안정제는 섬유 유연제 조성물에 사용되는 공지의 것을 사용한다. 예를 들면, 유기 화합물로서는 탄소수 8 미만의 저급 알콜 또는 글리콜류, 탄소수 11 이상의 고급알콜류, 요소 등이 있고, 무기화합물로서는 염화마그네슘, 염화나트륨, 염화칼슘, 질산나트륨 등이 있는데, 이들은 단독 또는 2종 이상의 혼합물로 포함될 수 있다. 바람직하게는, 에탄올, 이소프로필알콜, 에틸렌글리콜, 프로필렌글리콜, 헥실렌글리콜, 세틸알콜, 스테아릴알콜, 염화마그네슘, 염화나트륨, 염화칼슘, 질산나트륨 등을 단독으로 또는 2종 이상 혼합하여 사용한다.The fabric softener composition according to the present invention further comprises a dispersion stabilizer. The dispersion stabilizer uses a known one used in the fabric softener composition. For example, organic compounds include lower alcohols or glycols having less than 8 carbon atoms, higher alcohols having 11 or more carbon atoms, urea, and the like, and inorganic compounds include magnesium chloride, sodium chloride, calcium chloride, sodium nitrate, and the like. It can be included as a mixture. Preferably, ethanol, isopropyl alcohol, ethylene glycol, propylene glycol, hexylene glycol, cetyl alcohol, stearyl alcohol, magnesium chloride, sodium chloride, calcium chloride, sodium nitrate and the like are used alone or in combination of two or more thereof.
또한, 본 발명에 따른 섬유유연제 조성물에는 본 발명의 목적범위 내에서 소량의 첨가제가 더 포함될 수 있다. 예를 들면, 소취 후에 섬유에 기분 좋은 향취를 부여하기 위하여 신선하고 은은한 향을 내는 향료가 더 첨가될 수 있으며, 항균 효과를 더욱 향상시키기 위하여 항균 성분이 더 첨가될 수 있다. 이외에도, 색소, 방 부제, 산화방지제, 소포제 등이 더 포함될 수 있다.In addition, the fabric softener composition according to the present invention may further include a small amount of additives within the scope of the present invention. For example, fresh and subtle fragrances may be added to impart a pleasant odor to the fibers after deodorization, and antibacterial ingredients may be further added to further enhance the antibacterial effect. In addition, pigments, preservatives, antioxidants, defoamers may be further included.
또한 본 발명의 조성물은 각각의 제형에 상기 기재한 성분들 이외에 일반적으로 섬유유연제에 배합되는 유분, 물, 계면활성제, 보습제, 저급알코올, 증점제, 킬레이트제, 색소, 방부제, 또는 향료 등을 필요에 따라 적절히 배합하여 사용할 수 있다.In addition, the composition of the present invention, in addition to the components described above in each formulation, oil, water, surfactants, humectants, lower alcohols, thickeners, chelating agents, pigments, preservatives, or fragrances generally formulated in the fabric softener, It can mix | blend suitably according to the use.
상기 본 발명에 따른 조성물은 당업계에 공지된 방법을 이용하여 분말, 과립화하여 사용할 수 있으며, 액체상태로 제조하여 사용할 수도 있다.The composition according to the present invention may be used by powder, granulated using a method known in the art, may be prepared in a liquid state.
이하, 본 발명을 실시예에 의해 상세히 설명하기로 한다. 그러나 이들 실시예는 본 발명을 보다 구체적으로 설명하기 위한 것으로서, 본 발명의 범위가 이들 실시예에 한정되는 것은 아니다.Hereinafter, the present invention will be described in detail by way of examples. However, these examples are intended to illustrate the present invention in more detail, and the scope of the present invention is not limited to these examples.
<< 실시예Example 1 내지 3> 1 to 3
본 발명에 따른 원적외선 방사용 Far infrared ray radiation according to the present invention 섬유유연제Fabric softener 조성물의 제조 Preparation of the composition
하기 표 1과 같은 조성비로 본 발명에 따른 원적외선 방사용 섬유유연제 조성물을 제조하였다. 먼저, 정제수 1000ml을 50~60℃로 가온 유지한 후에, 염화칼륨, 탄산칼륨, 염화마그네슘, 구연산나트륨, 젖산칼슘, 정백당 및 정제포도당을 하기 조성 비율에 맞춰 차례로 넣고 서서히 교반하여 용해시킨 다음, 정치하여 안정화시킨 후 구멍 직경이 0.2㎛인 멤브레인 필터로 여과하여 불순물이 제거된 맑은 연한 미색의 액상 혼합액을 수득함으로써 본 발명의 조성물을 제조하였다.To the far-infrared spinning fiber softener composition according to the present invention was prepared in a composition ratio as shown in Table 1. First, 1000 ml of purified water was kept at 50 to 60 ° C., and then potassium chloride, potassium carbonate, magnesium chloride, sodium citrate, calcium lactate, white sugar and refined glucose were added in turn according to the following composition ratio, and gradually stirred to dissolve. After stabilization, the composition of the present invention was prepared by filtering with a membrane filter having a pore diameter of 0.2 μm to obtain a clear pale off-white liquid mixture in which impurities were removed.
<< 비교예Comparative example >>
비교예1로 통상의 섬유유연제(피죤)를 사용하였다.In Comparative Example 1, a conventional fibrous softener (Pigeon) was used.
<실험예 1>Experimental Example 1
본 발명의 조성물에 따른 원적외선 방사량 측정 실험Far Infrared Radiation Measurement Experiment According to the Composition of the Present Invention
본 발명의 실시예 1 내지 3에 따른 원적외선 방사용 섬유유연제 조성물로 처리한 피복에 대하여 원적외선 방사량을 측정하였다. 실험조건은 FT-IR Spectrometer를 이용한 BLACK BODY 대비 그 방사율 및 방사에너지를 측정하였다.Far-infrared radiation dose was measured for the coating treated with the fiber softener composition for far-infrared radiation according to Examples 1 to 3 of the present invention. Experimental conditions were measured emissivity and radiation energy compared to BLACK BODY using FT-IR Spectrometer.
그 결과, 하기 표 2에 나타낸 바와 같이, 실시예 1 내지 3의 원적외선 방사용 섬유유연제 조성물로 처리한 피복의 경우 원적외선을 100% 방출하는 BLACK BODY 대비 90.7% 가까운 높은 원적외선 방사율을 보였으며, 그로 인하여 방사에너지도 높게 측정되었음을 알 수 있었다. 따라서 본 발명에 따른 섬유유연제 조성물로 처리한 피복이나 침구류 사용 시 그 피복이나 침구류부터 방출되는 원적외선으로 인하여 신체의 혈액순환이 증대되고 신진대사가 활발해지는 등의 건강증진효과를 기대할 수 있으리라는 것을 확인할 수 있었다.As a result, as shown in Table 2 below, the coating treated with the fiber softener composition for far-infrared radiation of Examples 1 to 3 showed a high far-infrared emissivity close to 90.7% compared to BLACK BODY emitting 100% of far infrared rays. Radiation energy was also measured high. Therefore, when the coating or bedding treated with the fabric softener composition according to the present invention can be expected to improve the health, such as increased blood circulation of the body due to the far infrared rays emitted from the coating or bedding, active metabolism I could confirm that.
그 결과, 하기 표 2에 나타낸 바와 같이, 본 발명의 실시예 1 내지 3의 무독성 소취제 조성물은 비교예과 비교하여 암모니아, 트리메틸아민, 메킬머캅탄의 3대 악취제에 대하여 우수한 소취 효과를 나타냄을 알 수 있었다.As a result, as shown in Table 2 below, the non-toxic deodorant composition of Examples 1 to 3 of the present invention showed an excellent deodorizing effect against the three major odorants of ammonia, trimethylamine, and mechelmercaptan compared to the comparative example. Could.
구분
division
Far Infrared Ray (5 ~ 20㎛)
<< 실험예Experimental Example 2> 2>
본 발명의 조성물에 따른 According to the composition of the present invention 소취효과Deodorant effect 실험(기기 평가) Experiment (device evaluation)
일상생활에서 쉽게 접할 수 있는 불쾌취인 염기성 취기, 휘산성 취기, 산성 취기 등에 대해 각 조성물로서 검지관법에 의한 소취 효과를 3회 이상 반복하여 평가하였다. 염기성 취기로는 대표적인 암모니아, 트리메틸아민, 휘산성 취기로는 아세트알데히드, 산성 취기로는 메틸머캅탄 등에 대해 실험을 실시하였다. 본 실험에 사용된 검지관은 GASTEC 사제, no.71, 92, 180으로써 각각 메틸머캅탄, 아세트 알데히드, 아민류용의 지정 검지관을 사용하였다. 소취효과는 다음과 같이 판정하였다. 냄새제거율 80%이상(매우우수:◎), 60%이상(우수 :○), 40%이상(보통:△), 20%미만(불량:×)The deodorizing effect by the detection tube method was repeatedly evaluated three times or more as the composition for the basic odor, volatilized odor, acid odor and the like which are easily encountered in daily life. Representative ammonia, trimethylamine as the basic odor, acetaldehyde as the volatile odor, methyl mercaptan as the acidic odor and the like were tested. The detection tubes used in this experiment were Nos. 71, 92, and 180 manufactured by GASTEC Corporation, and designated detection tubes for methylmercaptan, acetaldehyde, and amines were used, respectively. Deodorant effect was determined as follows. Odor removal rate 80% or more (very good: ◎), 60% or more (good: ○), 40% or more (usually △), less than 20% (bad: x)
<< 실험예Experimental Example 3> 3>
본 발명의 조성물에 따른 항균력 실험Antimicrobial activity test according to the composition of the present invention
KS 0693 - 1990 시험법에 의거 Staphylococcus aureus를 균주로 하여 106마리를 면, PET에 대해 접종하고 이에 대한 직물의 항균도를 측정하였다. 항균 효과는 다음과 같이 판정하였다. 미생물의 양 103이하(매우우수:◎), 104이하(우수 :○), 105 이하(보통:△), 변화없음(불량:×)According to the KS 0693-1990 test method, 10 6 animals were inoculated against cotton, PET with Staphylococcus aureus as a strain, and the antimicrobial activity of the fabric was measured. The antimicrobial effect was determined as follows. Amount of microorganism 10 3 or less (very good: ◎), 10 4 or less (excellent: ○), 10 5 or less (usually: △), no change (bad: X)
<< 실험예Experimental Example 4> 4>
본 발명의 조성물에 따른 유연 효과 실험Softening effect experiment according to the composition of the present invention
시판 100%의 면타올을 상기 실험예 2의 방법과 동일하게 유연 처리한 다음 탈수하여 20℃, 65% RH조건에서 24시간 컨디셔닝(conditioning) 시킨 다음 숙련된 패널(panelist)의 관능 평가 시험에 의하여 촉감 정도를 유연 점수로써 최저 1점에서 5점까지 부여하게 하고 이것을 3회 이상 반복하여 그 평균값으로써 유연 효과를 측정하였다. 유연성 평가 기준은 비교예의 제품에 대한 유연 효과를 유연 점수로 부여하고 다음과 같이 판정하였다. 유연효과 점수 4.5이상(매우우수:◎), 3.5~4.5이상(우수 :○), 2.5~3.5이상(보통:△), 2.5미만(불량:×)A commercially available 100% cotton towel was flexibly treated in the same manner as in Experimental Example 2 and then dehydrated and conditioned at 20 ° C. and 65% RH for 24 hours, followed by a sensory evaluation test by an experienced panel. Tactile touch was given at least 1 to 5 points as the softness score, and this was repeated three or more times to measure the softness effect as the average value. The softness | flexibility evaluation criteria gave the softening effect with respect to the product of a comparative example by the softness | flexibility score, and determined as follows. Softness score 4.5 or more (very good: ◎), 3.5 to 4.5 or more (good: ○), 2.5 to 3.5 or more (usually △), less than 2.5 (bad: x)
<< 실험예Experimental Example 5> 5>
본 발명의 조성물에 따른 정전기 Static electricity according to the composition of the present invention 방지성Preventive 실험(마찰 대전압) Experiment (friction large voltage)
KS K-0950의 염색 견뢰도 시험용 백 면포, 백 폴리에스테르포, 나일론포(한국의류시험연구원 제작)를 각각 4×6cm의 크기로 절단하고, 상기 실험예 2의 방법과 동일하게 유연 처리하고 20℃, 상대습도 65% 조건에서 24시간 conditioning시킨 다음 시료포를 일본 DAIEI KAGAKU사 제품인 Rotary Static Tester 기기를 이용하여 KS K-0555B 시험방법으로 60초 동안 600RPM으로 회전 마찰시켜 발생된 대전압을 측정하고 3회 이상 반복 실험하여 정전기 방지성을 측정하였다. 정전기 방지성은 다음과 같이 판정하였다. 상기 백 면포에 대하여 발생한 대전압이 100V이하(매우우수:◎), 100~300V이하(우수 :○), 300~500V이하(보통:△), 500V이상(불량:×), 상기 백 폴리에스테르포, 및 나 일론포에 대하여 발생한 대전압이 800V미만(매우우수:◎), 800~1200V미만(우수 :○), 1200~1800V미만(보통:△), 1800V이상(불량:×)으로 표기하였다.KS K-0950 dyeing fastness test cotton cloth, white polyester cloth, nylon cloth (manufactured by Korea Apparel Testing & Research Institute) were cut into sizes of 4 × 6 cm, respectively, and flexibly treated in the same manner as in Experimental Example 2 above at 20 ° C. After conditioning for 24 hours at 65% RH, measure the large voltage generated by rotating friction at 600 RPM for 60 seconds using KS K-0555B test method using Rotary Static Tester device manufactured by DAIEI KAGAKU of Japan. The experiment was repeated more than once to determine the antistatic properties. Antistatic property was determined as follows. 100 V or less (excellent: ◎), 100 to 300 V or less (excellent: ○), 300 to 500 V or less (usually △), 500 V or more (bad: x), and the back polyester The high voltages generated for guns and nylon guns are indicated as less than 800 V (very good: ◎), less than 800 to 1200 V (excellent: ○), less than 1200 to 1800 V (usually △), and 1800 V or more (bad: x). It was.
<< 실험예Experimental Example 6> 6>
본 발명의 조성물에 따른 피부자극성 시험Skin irritation test according to the composition of the present invention
본 발명에서 실시한 피부 자극성 시험은 건강한 남, 녀 10명씩의 상박에 섬유 유연제 시료를 매일 10시간씩 첩포(patch)한 후 첩포 부위의 피부자극성을 평가하였다. 모든 피부자극 실험값은 물에 의한 피부자극수치와 비교하였으며, 물에의한 피부자극은 '매우 좋음' 값을 갖는 기준으로 설정하고 다음과 같이 판정하였다. 홍반 발생 정도 흔적이 거의 없음(우수 :○), 약한 홍반(보통:△), 심한 홍반(불량:×)In the skin irritation test conducted in the present invention, the fabric softener sample was patched every 10 hours on the upper arm of 10 healthy men and women, and the skin irritation of the patch was evaluated. All skin irritation test values were compared with skin irritation values by water, and skin irritation by water was set as a criterion having a 'very good' value and determined as follows. Almost no trace of erythema development (excellent: ○), weak erythema (usually: △), severe erythema (bad: ×)
상기 각각의 실험예 2 내지 6에 대한 결과를 하기의 표 3에 나타내었다.The results for each of Experimental Examples 2 to 6 are shown in Table 3 below.
이제까지 본 발명에 대하여 그 바람직한 실시예들을 중심으로 살펴보았다. 본 발명이 속하는 기술 분야에서 통상의 지식을 가진 자는 본 발명이 본 발명의 본질적인 특성에서 벗어나지 않는 범위에서 변형된 형태로 구현될 수 있음을 이해할 수 있을 것이다. 그러므로 개시된 실시예들은 한정적인 관점이 아니라 설명적인 관점에서 고려되어야 한다. 본 발명의 범위는 전술한 설명이 아니라 특허청구범위에 나타나 있으며, 그와 동등한 범위 내에 있는 모든 차이점은 본 발명에 포함된 것으로 해석되어야 할 것이다.So far I looked at the center of the preferred embodiment for the present invention. Those skilled in the art will appreciate that the present invention can be implemented in a modified form without departing from the essential features of the present invention. Therefore, the disclosed embodiments should be considered in an illustrative rather than a restrictive sense. The scope of the present invention is shown in the claims rather than the foregoing description, and all differences within the scope will be construed as being included in the present invention.
Claims (3)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| KR1020090030145A KR20100111775A (en) | 2009-04-08 | 2009-04-08 | Fabric softener composition for radiating far-infrared ray |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1020090030145A KR20100111775A (en) | 2009-04-08 | 2009-04-08 | Fabric softener composition for radiating far-infrared ray |
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| KR1020090030145A KR20100111775A (en) | 2009-04-08 | 2009-04-08 | Fabric softener composition for radiating far-infrared ray |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR102027726B1 (en) * | 2019-01-16 | 2019-11-14 | 김은주 | Manufacturing method of mineral water with increased mineral content |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR102027726B1 (en) * | 2019-01-16 | 2019-11-14 | 김은주 | Manufacturing method of mineral water with increased mineral content |
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