KR20100059428A - Method for preparing lip make-up cosmetic composition containing herb medicines - Google Patents

Abstract

PURPOSE: A method for manufacturing a cosmetic composition for lip make-up containing herbal materials is provided to ensure a moisturizing effect. CONSTITUTION: A method for manufacturing a cosmetic composition for lip make-up comprises: a step of inputting herbal materials into oil and wax and extracting the composition to obtain an extract containing active ingredients; a step of dispersing pigment to the extract; a step of adding ethanol and water and evaporating solvent to obtain a gel having a high viscosity; a step of emulsifying the gel to obtain a W/O emulsification type gel; and a step of adding the W/O emulsification type gel to the extract and mixing.

Description

Method for preparing cosmetic composition for lip makeup containing herbal medicine {Method for preparing lip make-up cosmetic composition containing herb medicines}

The present invention relates to a method for producing a cosmetic composition for lip makeup containing a herbal medicine, and more particularly, to extract the extract of the useful ingredient by adding the herbal medicine to oils and waxes used in the preparation of the cosmetic composition for lip makeup, ethanol and The present invention relates to a method for preparing a cosmetic composition for lip makeup prepared by preparing a water-soluble component obtained by extracting a medicinal herb to a mixed solvent of water with a W / O emulsion type gel and then mixing the extract with an oil-soluble component. The cosmetic composition for lip makeup prepared according to the present invention contains both the oil-soluble component and the water-soluble component of the medicinal herb and provides a moisturizing and excellent moisturizing effect when used on the lips while having a unique herbal odor.

Existing conventionally useful products containing herbal medicines include extracts extracted with water, oil, alcohol or organic solvents, extracts extracted using CO ₂ supercritical method, or methods using extracted extracts dissolved only in certain medicinal ingredients from herbal medicines. There is this. However, these methods have the disadvantage of not being excessively used in the product, and therefore, there is a possibility that the desired level of skin efficacy may not be exhibited. When extracted as a water-soluble ingredient, it is difficult to mix a large amount because it is not mixed with the oil-soluble ingredient. When the supercritical method is used, the stability of the raw material is improved, but due to the expensive manufacturing cost and the complicated process, it is difficult to be used in a variety of lip cosmetic products. In addition, since only the oil-soluble raw material is extracted in the herbal medicine, there is a problem in that it is difficult to obtain a variety of water-soluble components included in the actual herbal medicine. When only a specific ingredient is extracted, it is difficult to obtain all the various ingredients included in the herbal medicine, and most of them are difficult to dissolve in actual oil components. Therefore, there is an urgent need for research on a cosmetic composition for lip makeup that can stably contain a large amount of all ingredients included in herbal medicines in useful lip products.

Therefore, the present inventors have solved the above problems and researched a manufacturing method that can contain a large amount of herbal ingredients in oil-soluble lip products, by extracting the extract of the oil-soluble ingredients by adding a herbal medicine to oils and waxes used in the manufacture of lipstick After obtaining and stabilizing a high viscosity gel of a water-soluble component obtained by extracting the herbal medicine in a mixed solvent of ethanol and water with a W / O emulsifying type gel, the cosmetic composition for lip makeup prepared by mixing with the extract of the oil-soluble ingredient is useful for the herbal medicine. And the discovery that it can contain a large amount of water-soluble components has completed the invention.

Accordingly, it is an object of the present invention to provide a method for preparing a cosmetic composition for lip makeup that can be moisturized and moisturized immediately after application to the lips by containing a large amount of the usefulness and water-soluble components of the herbal medicine.

In order to achieve the above object, in the present invention

a) extracting the herbal medicines into oils and waxes to obtain extracts containing the useful ingredients of the herbal medicines;

b) dispersing the pigment in an extract of the oil soluble component of a);

c) extracting the medicinal herb in a mixed solvent of ethanol and water and evaporating the solvent to obtain a high viscosity gel containing water-soluble components of the medicinal herb;

d) emulsifying the high viscosity gel of c) to prepare a W / O emulsion gel; And

e) putting the W / O emulsion gel of d) into b) and mixing with a mixer;

It provides a method of manufacturing a cosmetic composition for lip makeup comprising a.

Since the cosmetic composition for lip makeup prepared according to the present invention may stably contain a large amount of the usefulness and water-soluble components of the herbal medicine, it can improve the lip condition by providing a moisturizing and excellent moisturizing effect when used on the lips.

The present invention

a) extracting the herbal medicines into oils and waxes to obtain extracts containing the useful ingredients of the herbal medicines;

b) dispersing the pigment in an extract of the oil soluble component of a);

c) extracting the medicinal herb in a mixed solvent of ethanol and water and evaporating the solvent to obtain a high viscosity gel containing water-soluble components of the medicinal herb;

d) emulsifying the high viscosity gel of c) to prepare a W / O emulsion gel; And

e) putting the W / O emulsion gel of d) into b) and mixing with a mixer;

It provides a method of manufacturing a cosmetic composition for lip makeup comprising a.

Hereinafter, the present invention will be described in detail step by step.

a) extracting the herbal medicines into oils and waxes to obtain extracts containing the useful ingredients of the herbal medicines;

Herbal medicine of the present invention can be used in most of the herbal herbal medicine, specific examples, for example, clove, rhubarb, baekryeoksaengseolcho, Hyunsam, Jiyu, Angelica, safflower, Root, sewage, sesame, passerby, baekyeop, gojija, bokyeong, Turmeric, rhubarb, ginseng, cheongung, licorice, hyssop, baekbuja, half, branch man, gyeolja, mackmundong, astronomical dong, red peony, hojang, chrysanthemum, baekbaek, cheonmundong, horseback riding, dermis, copper confectionery, presbytery, kyokyo, manor, gold silver flower, daechung, Loquat leaf, red ginseng, cheoncho, gilsheng, golden, astragalus, imperial, japonica, uiin, hawthorn, sesame, donggle, ginkgo, cheonjaja, black bean, onion, apple, hazelnut, pogongyoung, mung bean, red ginseng, yam, plum, lotus, green tea , Motherwort, raw turmeric, sessin, leachate, powder, or a mixture thereof. More preferably, it is effective for wound healing and dermatitis such as golden, yellow, yellow lotus, gold and silver, dermis, donkey, licorice, licorice, duct, horse riding, gangan, baekbaek, hyunsam, Daecheong, makmun-dong, cheonmun-dong, donggle, saenghwanghwang, sesin, cheongung All suitable herbal medicines may be used, such as whitening or mixtures thereof.

Herbal medicine used in step a) is preferably used in 2 to 33.3% by weight based on the total weight of the composition. If the content is less than 2% by weight of the amount of herbal medicine is small and the effect and aroma is insignificant, and if it exceeds 33.3% by weight, the possibility that the herbal medicine will absorb a large amount of oil is because the extraction of the useful ingredients of the herbal medicine is not efficient.

Herbal medicine of the present invention is preferably used by using a general dried herbal medicine in order to prevent instability by water and milled to a diameter of 1mm ~ 2cm for effective extraction. If the diameter is less than 1mm, fine particles are not removed during filtration, so the usability of the formulation is not good. If the diameter exceeds 2 cm, the extraction is not performed efficiently.

Waxes usable in the present invention include ozokerite, beeswax, candelillanab, ceresin, carnauba wax, paraffin wax, montan wax, zepen wax, rice wax, microcrystalline wax, synthetic wax, polyethylene wax, and various kinds of silicone. All waxes suitable for cosmetics such as waxes can be used. The wax is used in an amount of 1 to 20% by weight, more preferably 5 to 15% by weight, based on the total weight of the composition in consideration of stability and usability of the formulation.

As oils usable in the present invention, vegetable oils, ester oils, ether oils, mineral oils, animal oils, or gel components may be used in various ways. In particular, vegetable oils may be suitable for the herbal natural concept, and it is also advantageous to use polymer components such as high viscosity oils, polybutenes or rosin for cohesive application. The oil is contained in 1 to 80% by weight based on the total weight of the composition.

When the herbal medicines are added to oils and waxes used in preparing cosmetic compositions and mixed, the mixing ratio is preferably 1:50 to 1: 3. This is because when the mixing ratio is less than 1:50, the effects and aromas of the herbal medicines are insignificant, and when the mixing ratio is greater than 1: 3, the herbal medicines absorb a lot of oil so that the extraction of useful components is not efficiently performed. In addition, it is preferable to maintain the temperature at the time of mixing at 50-90 degreeC. If it is below 50 ℃, it is difficult to extract useful ingredients of herbal medicine, extraction time is too long, and if it exceeds 90 ℃, it is possible to denature temperature sensitive components (deodorization, discoloration, deterioration of efficacy, etc.) and extract water together. Because there is.

After adding herbal medicines to oils and waxes, leave them for 1 hour to 5 days to extract the active ingredients. If the time is less than 1 hour, the extraction amount of the active ingredient is too small, and if it exceeds 5 days, the preparation time is too long. In addition, to shorten the time to leave the herbal medicine to increase the temperature within the above preferred temperature range. After the extraction is completed, by removing the medicinal herbs by filtering the sieve of 150 mesh (mesh) to obtain an extract containing the useful components of the herbal medicines.

b) dispersing the pigment in an extract of the oil soluble component of a);

The extract of the oil-soluble component of a) is heated to 80-90 ° C. while maintaining a liquid state, and the pigment is added and mixed for about 30 minutes to be dispersed.

Pigments usable in the present invention are pigments customary in the art, for example, powders such as white mica, synthetic mica, hardness, kaolin, titanium dioxide, titanium oxide coated mica, aluminum powder, iron sulfate, iron oxide black, barium sulfate, etc. Or pigments for coloring such as yellow 203, yellow 4, yellow 5, yellow 201, yellow 204, red 103 and the like. The pigment is contained in 1 to 30% by weight based on the total weight of the composition.

c) extracting the medicinal herb in a mixed solvent of ethanol and water and evaporating the solvent to obtain a high viscosity gel containing water-soluble components of the medicinal herb;

Into the mixed solvent of ethanol and water in a ratio of 7: 3, the same or different kinds of herbal medicines are added and allowed to stand at room temperature for 1-2 days so that the water-soluble components of the herbal medicines can be extracted. This is because if the time is less than 1 day, the amount of extraction of the active ingredient is too small and if it exceeds 2 days, the preparation time is too long.

After extracting the water-soluble component of the herbal medicine, a method known in the art may be used to evaporate the solvent, and generally a vacuum distillation apparatus is used. Evaporation of water and ethyl alcohol yields a highly viscous gel extract containing the water-soluble components of the herbal medicine.

d) emulsifying the high viscosity gel of c) to prepare a W / O emulsion type gel;

In order to stabilize the water-soluble component of the herbal medicine in the oil-soluble lip cosmetic composition, a W / O emulsion gel is prepared. Selected from the group consisting of a high viscosity gel and agar, hyaluronic acid, cellulose gum, hydroxyethylcellulose, pectin, starch and xantan gum of the water-soluble medicinal herbs obtained in c) 10-70% by weight of a mixture with at least one water-soluble polymer; 2-20% by weight of waxes; 20 to 60% by weight of oils; Emulsifier 0.5-10% by weight; And preservatives 0.05 to 0.2% by weight; to prepare a W / O emulsion type gel containing.

The high viscosity gel of the medicinal herb water-soluble component is contained in an amount of 0.1 to 50% by weight, more preferably 3 to 20% by weight, based on the total weight of the mixture with the water-soluble polymer. If the content is less than 0.1% by weight, the effect is too small in a small amount, if it exceeds 50% by weight because the stability of the W / O emulsion type gel may be lowered.

W / O emulsion gel of the present invention can be prepared as follows. Waxes, oils, emulsifiers and preservatives are dissolved while heating to 75 ~ 80 ℃. Thus, a mixture of the high viscosity gel and the water-soluble polymer of the medicinal herb water-soluble ingredient (a mixture of the high viscosity gel and the water-soluble polymer of the herb water-soluble ingredient is heated to 75-80 ° C. and mixed) is added and emulsified by mixing with a mixer. It is then cooled to 30 ° C. with a paddle mixer and stored at room temperature.

e) putting the W / O emulsion gel of d) into b) and mixing with a mixer;

The extract of the oil-soluble component in which the pigment of b) is dispersed is heated to 80-90 ° C., and the W / O emulsion type gel of d) is added thereto. A cosmetic composition for lip makeup is prepared while mixing and dispersing for about 30 minutes.

W / O emulsion type gel containing the water-soluble component of the herbal medicine is contained in 0.1 to 20% by weight based on the total weight of the composition. If the content exceeds 20% by weight, pigment dispersing of lipstick is not performed properly, so pigment separation, sinking, pigment band generation and pearl entanglement are severe. If the amount is less than%, the effect is too small.

Other components usable in the cosmetic composition of the present invention may further contain a moisturizing agent, antioxidant, ultraviolet absorbent, preservative or fragrance within a range that does not impair the effects of the present invention.

The cosmetic composition of the present invention can be prepared in a cosmetic composition for lip makeup such as lipstick, lip gloss, lip bob or lip pencil by a process such as heating, mixing, stirring by a conventional manufacturing method.

Hereinafter, the present invention will be described in more detail with reference to Examples and Test Examples, but the present invention is not limited only to these examples.

Example 1 and Comparative Example 1

In order to evaluate the emulsion stability of the W / O emulsion type gel containing the herbal medicine water-soluble component of the present invention was prepared Example 1 and Comparative Example 1 having the composition of Table 1. Appearance of emulsion stability was evaluated as (circle) when surface state was smooth, (triangle | delta) as normal, and X when rough. The high temperature stability of the emulsion stability was evaluated as X when the composition was stored at 45 ° C. for 7 days, and if no separation occurred, △ if a little separation occurred, and completely separated. The results are shown in Table 2 below.

ingredient Example 1
(weight%) Comparative Example 1
(weight%) 1. Candelilla Nap 10 10 2. Caprylic / Capric Triglyceride 50 30.5 3. Sorbitan isostearate 0.5 0.5 4. Mica 2 2 5. Glycerin 14.5    0 6. Aga Powder 2.0 2.0 7. Medicinal Herb Water Soluble Extract 10 55

<Production method of Example 1 and Comparative Example 1>

1) Dried medicinal herbs (Dangui 20%, Golden 10%, Licorice 10%, Astragalus 10%, Hwangnyeon 5%, Cheonmun-dong 5%, Licorice 20%, Hyunsam 5%, Gold and Silver Coins 5%, Cheongung 5% and Baekchul 5%) Was extracted in a mixed solvent of water / ethanol (3: 7) for 2 days and the solvent is completely evaporated to prepare a herbal extract.

2) The components 5-6 are heated to 90 ° C. or higher to dissolve completely, and then 1) above is added to disperse.

3) The components 1 to 4 were heated to 90 ° C. in a vessel and dispersed for 15 minutes to be completely dissolved.

4) Add 2) to 3) and emulsify at 70 ° C. and 3600 rpm for 5 minutes using a mixer.

5) Cool slowly to 35 ° C. while slowly agitating 4) above.

Item Example 1 Comparative Example 1 color Beige bright brown Oil Painting Stability-Appearance O △ Emulsification stability-high temperature stability (45 ℃, 7 days) O X

As can be seen in Table 2, Comparative Example 1 containing an excessive amount of the water-soluble extract of the herbal medicine is not smooth in appearance and unstable at high temperature due to the layer separation occurs low emulsification stability, while Example 1 of the present invention is smooth in appearance and stable even at high temperatures No separation occurred. Therefore, Example 1 of the present invention was found to be excellent in emulsion stability at appearance and high temperature.

[Examples 2-3 and Comparative Examples 2-4]

To prepare a lipstick composition of Examples 2 to 3 and Comparative Examples 2 to 4 having the composition of Table 3. Examples 2 to 3 were prepared to include both the oil-soluble component and the water-soluble component of the herbal medicine according to the present invention. Comparative Examples 2 to 3 contain a small amount or an excess of an emulsified type gel of the herbal medicine water-soluble component, Comparative Example 4 was prepared not to contain both the oil-soluble component and the water-soluble component of the herbal medicine.

ingredient Example 2
(weight%) Example 3
(weight%) Comparative Example 2
(weight%) Comparative Example 3
(weight%) Comparative Example 4
(weight%) 1. Beeswax 2.1 2.1 2.1 2.1 2.1 2. Candelilla Nap 4.0 4.0 4.0 4.0 4.0 3. Ozokerite 2.0 7.0 2.0 7.0 2.0 4. Micro Crystalline Wax 5.0 5.0 5.0 5.0 5.0 5. Shea Butter 11.0 11.0 11.0 11.0 11.0 6. Olive oil 10.0 10.0 10.0 10.0 10.0 7. Diisostearyl maleate To 100 To 100 To 100 To 100 To 100 8. Polybutene 5.0 5.0 5.0 5.0 5.0 9. Jojoba oil 10.0 10.0 10.0 10.0 10.0 10. Tocopherol Acetate 2.0 2.0 2.0 2.0 2.0 11. Preservative 0.04 0.04 0.04 0.04 0.04 12. Dried medicinal herbs (Dangui 20%, Golden 10%, Licorice 10%, Astragalus 10%, Yellow Lotus 5%, Cheonmun-dong 5%, Licorice 20%, Hyunsam 5%, Gold and Silver Coins 5%, Cheongung 5% and Baekchul 5%) 20 10 20 20 - 13. Mica 1.0 4.0 4.0 1.0 1.0 14. Pigment 15.0 15.0 15.0 15.0 15.0 15.Titanated Mica 3.0 3.0 3.0 3.0 3.0 16. Emulsified Type Gel of Water-Soluble Components Prepared in Example 1 20 5 0.1 55 -

<The manufacturing method of Examples 2-3 and Comparative Examples 2-4>

1) The components 1-12 were put together in the vessel and left to stand at 50 degreeC for 3 days.

2) After filtering the herbal medicines using a 150 mesh sieve, the extract of the remaining useful ingredient was re-injected into a vessel and heated to 90 ° C.

3) Components 13-15 were added to 2) and dispersed for 15 minutes at 3600 rpm with a homogener.

4) Add Component 16 to 3) above and disperse at 85 ° C for 10 minutes.

5) The above 4) was vacuumed at 85 ° C. to remove bubbles to prepare a lipstick composition.

[Test Example 1]

Ten females in their 20s and 30s were evaluated to evaluate the odor, moisture retention, contents and molding state of Examples 2 to 3 and Comparative Examples 2 to 4, and evaluated as O, normal △, and X if bad. . The results are shown in Table 4 below.

Item Example 2 Example 3 Comparative Example 2 Comparative Example 3 Comparative Example 4 Odor Chinese medicine strong Chinese medicine weak Chinese medicine weak Chinese medicine very strong No herbal medicine Moisturizing O O △ O X Content status O O O X O Molding condition O O O X O

As can be seen in Table 4, Example 2 has a suitable herbal medicine and a lot of water-soluble moisturizing ingredients, the moist feeling is strong and the state after separation or molding on the contents was good, in the case of Example 3, the herbal medicine was weak but moisturizing power, contents And the stability of the molded state was excellent. In Comparative Example 2, the herbal medicinal herb was weak and contained too small a water-soluble component, which was insufficient to give a moist feeling. In Comparative Example 3, the herb medicine ingredient was contained in a large amount, the herbal medicine was too strong, and the amount of the water-soluble ingredient was too high, so that the separation of the wax layer occurred, and the pigment and pearl particles were agglomerated on the surface, and thus did not have a uniform appearance color. In addition, it can be seen that Comparative Example 4, which does not contain the active ingredient of the present invention, does not have a herbal medicinal effect and has a poor moisturizing power, thereby imparting moisturization to the lips.

Claims (9)

a) extracting the herbal medicines into oils and waxes to obtain extracts containing the useful ingredients of the herbal medicines; b) dispersing the pigment in an extract of the oil soluble component of a); c) extracting the medicinal herb in a mixed solvent of ethanol and water and evaporating the solvent to obtain a high viscosity gel containing water-soluble components of the medicinal herb; d) emulsifying the high viscosity gel of c) to prepare a W / O emulsion gel; And e) putting the W / O emulsion gel of d) into b) and mixing with a mixer; Method for producing a cosmetic composition for lip makeup comprising a. The method of claim 1, wherein the herbal medicine is clove, rhubarb, earl, baekryeoksaeng, Hyunsam, Jiyu, Dangui, safflower, Root, sewage, sesame, passerby, baekryeop, wolfberry, Fuling, turmeric, rhubarb, ginseng, Cheongung, licorice , Walrus, baekbuja, half, branch, glitches, malokdong, astronomical dong, red peony, hojang, chrysanthemum, yellow white, astronomical dong, horseback riding, dermis, copper confectionery, presbytery, fellowship, manor, gold and silver, daecheong, loquat leaf, ginseng, cheoncho, gilyeong, golden , Astragalus, imperial herb, uiyiin, hawthorn, sesame, roundworm, ginkgo, monarch, black bean, onion, apple, hazelnut, pogongyoung, mung bean, red ginseng, yam, plum, lotus, green tea, motherwort Method for producing a cosmetic composition for lip makeup, characterized in that at least one member selected from the group consisting of acid. According to claim 1, wherein the herbal medicine is a method for producing a cosmetic composition for lip makeup, characterized in that it is used by grinding to a diameter of 1mm ~ 2cm. The method according to claim 1, wherein the a) herbal medicine is contained in an amount of 2 to 33.3% by weight based on the total weight of the composition. The method of claim 1, wherein the mixing ratio of the herbal medicine and oil and wax of a) is 1:50 to 1: 3. According to claim 1, wherein the W / O emulsified gel is a high viscosity gel and agar, hyaluronic acid, cellulose gum (hydroxy gum), hydroxyethylcellulose (pectin), starch and xantan gum 10 to 70% by weight of a mixture with at least one water-soluble polymer selected from the group consisting of; 2-20% by weight of waxes; 20 to 60% by weight of oils; Emulsifier 0.5-10% by weight; And 0.05 to 0.2% by weight of preservatives; Method for producing a cosmetic composition for lip makeup comprising a. The method of claim 6, wherein the high viscosity gel is contained in an amount of 0.1 to 50% by weight based on the total weight of the mixture with the water-soluble polymer. The method of claim 1, wherein the W / O emulsified gel is contained in an amount of 0.1 to 20% by weight based on the total weight of the composition. Cosmetic composition for lip makeup prepared according to any one of claims 1 to 8.