KR20190093901A - Cosmetic ingredients using plum distillation extract - Google Patents

Abstract

Cosmetic ingredients using a plum distillation extract according to an embodiment of the present invention are prepared by the following steps: a first step of extracting the plum distillate by putting purified water and fresh raw plum including seeds in a distillation extractor; a second step of producing a plum distillate concentrate in an inner pot of the distillation extractor when the plum distillate is cooled to produce 30 liters of plum hydrosol; and a third step of diluting the acidic plum distillation concentrate. In the first step, the mixing ratio of the fresh raw plum and purified water is 10 kg : 35 L.

Description

Cosmetic ingredients using plum distillation extract {Cosmetic ingredients using plum distillation extract}

The present invention relates to a cosmetic raw material using a plum distillation extract.

Plum is widely used as a raw material for producing plum wine, pickles and juices. The pharmacological properties of plum are known to be effective in improving constitution by anti-alkali, anti-allergic and anti-allergic effects, and are known to be effective in hypertension, tablet diabetes, diarrhea, and high in dietary fiber. It is known to be excellent and good for hangover removal effect.

However, plums do not have many opportunities to be more easily accessible, despite the above-mentioned useful advantages.

In addition, although plums are commercially available in high concentration, the development of new types of value-added products is insufficient. As a result, it is difficult to generate profits in plum farms.

Republic of Korea Patent Publication No. 10-1105539 (2012.01.05.) Republic of Korea Patent Publication No. 10-0959653 (2010.05.17.) Republic of Korea Patent Publication No. 10-1110548 (2012.01.19.) Republic of Korea Patent Publication No. 10-1541892 (2015.07.29.)

Accordingly, an object of the present invention is to provide a cosmetic raw material using a plum distillation extract for the development of high value-added products for increasing the income of plum farmers by using the high functionality of plum.

In addition, another object of the present invention is to provide a cosmetic raw material using a plum distillation extract to be produced at an optimum ratio for improving the functionality.

In addition, another object of the present invention is to provide a cosmetic raw material using a plum distillation extract with an increase in the content of the active ingredient of aroma water commonly used as a cosmetic raw material.

Cosmetic raw material using a plum distillation extract according to an embodiment of the present invention for achieving the above technical problem, a first step of extracting the plum distillate by putting the fruit pastry and purified water including seeds in a distillation extractor; A second step of producing a plum distillate concentrate in an inner pot of the distillation extractor when the plum distillate is cooled to produce 30 l of plum hydrosol; And a third step of diluting the acidity of the plum distillation concentrate.

In the first step, the mixing ratio of the fresh raw plum and purified water includes 10 kg: 35 L.

In addition, the cosmetic raw material using plum distillation extract according to an embodiment of the present invention, 0.2% by weight of turmeric extract may be mixed with the plum distillation concentrate.

In addition, the cosmetic raw material using a plum distillation extract according to an embodiment of the present invention, may be added by mixing 0.5% by weight of hyaluronic sodium.

In addition, the cosmetic raw material using a plum distillation extract according to an embodiment of the present invention, HACE-200 may be further added by mixing 0.5% by weight.

In addition, in the cosmetic raw material using a plum distillation extract according to an embodiment of the present invention, the plum fresh fruit, the purified water, the turmeric extract, the hyaluronic acid sodium and the HACE-200 is 3% or less to the numerical value presented to 3 It can be applied to the error range of more than% value.

Specific details of other embodiments are included in the detailed description.

Cosmetic raw material using a plum distillation extract according to an embodiment of the present invention made as described above, can provide a high value-added products using plum, in particular can be used to manufacture a plum-related products that are not popularly rejected .

In addition, by developing additional products using plum can contribute to increase the profit of the plum farmer.

In particular, the cosmetic raw material using a plum distillation extract according to an embodiment of the present invention, when evaluating the development value of the aromatic lotion by steam distillation extraction using plum and flowers, the results of the investigation of functional content of the active ingredient for the cosmetic raw material In summary, the fragrance component of fragrance water contains the excellent fragrance component as a fragrance, and it contains many beneficial ingredients for health, high antioxidant content and excellent moisturizing properties. It can be used as a main raw material or additive of cosmetics and household goods such as textile rinse, so the adequacy of development as a cosmetic material can be very high.

1 is a drawing substitute photograph for confirming the precipitate in the cosmetic raw material using a plum distillation extract according to an embodiment of the present invention.

Advantages and features of the present invention, and methods for achieving them will be apparent with reference to the embodiments described below.

Embodiments described below are shown by way of example in order to help understanding of the present invention, it will be understood that the present invention can be implemented in various modifications different from the embodiments described herein. However, in the following description of the present invention, if it is determined that the detailed description of the related known functions or components may unnecessarily obscure the subject matter of the present invention, the detailed description thereof will be omitted.

Meanwhile, terms to be described below are terms set in consideration of functions in the present invention, which may vary depending on the intention or custom of the producer, and the definitions thereof should be made based on the contents throughout the present specification.

Embodiment of the present invention is to provide a plum distillation extract using the plum, to provide a cosmetic raw material and the composition using the plum distillation extract.

<Saturation, Salinity and Acidity of Cosmetic Ingredients Produced by Plum Distillation Extracts>

An embodiment of the present invention is to produce a distillation extract of plum by distilling the plum in distilled extraction method. This is described with reference to [Table 1]. Table 1 shows the sugar content, salinity and acidity of the cosmetic raw material extracted when the plum was distilled off.

When distillate extraction for cosmetic raw materials, 25 liters and 35 liters of purified water were added for each sample, and the sugar and salinity of distilled extracts according to the input amount of purified water were examined. You may not.

Plum aroma water has a sweetness of 0.2 (Brix%) with only 25 liters of distilled purified water input.

The sweetness of the fresh plum and the yellow plum was the distilled concentrate, the amount of distilled extract purified water was 25 to 6.6 (Brix%) to 6.7 (Brix%), and the amount of purified water to be extracted was 35 to 5.6 (Brix%) to 8.4 (Brix%). .

Extraction of the distillate concentrate by removing the seeds of the blue plum and the yellow plum showed a sugar content of 3.7 (Brix%) to 6.7 (Brix%), and 6.0 (Brix) when extracting the distillate concentrate including the seeds of the blue and yellow plum. %) To 8.4 (Brix%).

In addition, the sugar content appears to be high when the amount of distilled extract purified water input or extract including the seed.

Salinity was not measured in the aromatic water of fresh plum and yellow plum and plum, but only in distilled concentrate. Distilled concentrate extracted by removing seeds ranged from 1.9 (Salt%) to 2.7 (Salt%). 3 (Salt%) to 3.5 (Salt%) showed a higher salinity of the distillate concentrate extracted from the seed including the seed tends to be similar to the measured sugar content of the plum distillation extract.

In case of extracting including seeds, the sugar or salinity of seeds is higher than plum flesh, and the more distilled and purified water is added, the longer the extraction time and the more sugar and salt in the seed is extracted, resulting in higher sugar and salinity. Can be.

The acidity (pH) for the aromatic water was measured at 35 L where the amount of purified plum and yellow plum was high in the amount of distilled extract purified water, and when the amount of purified water was increased, the concentration of the plum was diminished during distillation, indicating that the acidity slightly decreased.

The acidity (pH) value of the aroma of plum water is measured to be lower than 35 liters of distilled distilled purified water, so that the acidity is higher as the amount of purified water is increased.

After distillation and extraction, the concentrated liquid remaining in the distillation extract was examined for sugar and salinity, and as a result, the sugar content and salinity of 25 liters of which the amount of purified water was decreased in the flesh without seeds was high. At high sugar content and salinity are measured differently.

When distilling the plums from which seeds were removed, if distillation was performed by varying the input amount of purified water, when the amount of distilled concentrate was the same when distillation was finished, the distilled concentrate increased in concentration as the amount of distilled concentrate decreased and the sugar and salinity increased. can do.

When distilled extracts of plums with seeds with different amounts of purified water were added, the higher the sugar content and the higher the salt content of the distillate extract in the same state of distillate concentrate in the pot after the distillation. It can be presumed that the heat distillation in many conditions played a role in raising the sugar and salinity.

Plum fragrance water was measured only at 25 liters of distilled distilled purified water and had a weak sugar content of 0.2 (Brix%). Other fragrance water was not measured for sugar and salinity.

The pH value of cosmetic fragrance water extracted by steam distillation was pH 3.27 to pH 4.46 for both blue and yellow plum and plum, and the distillate was pH 2.64 to pH 3.91. To be used, the acid is strong and needs to be diluted.

The acidity (pH) values of the aromatic waters of the fresh and yellow plums showed a lower acidity (pH) value compared to the 35 liters of purified water input with less purified water input and the lower acidity (pH) value of distilled extraction. Higher pH.

The amount of aromatic water of the plum was found to be slightly higher in acidity when the input of 35 liters of purified water was added to the distilled extract.

Fragrance containing seeds tended to have higher acidity than fragrances without seeds.

Distilled concentrate is distilled by removing the seed or distilled extraction, the higher the purified water input, the lower the acidity (pH) value appears, the acidity seems to be a little stronger.

In the same distilled extract, the acidity of the aromatic water increased when the acidity of the distillate concentrated in the plum decreased, and the acidity of the aromatic water decreased when the acidity of the distilled concentrate in the plum increased. It can be seen that the components are also distilled together, and as the components are distilled more, the acidity of the aromatic water increases, but the acidity of the distillate concentrate remaining after the distillation extraction decreases.

<Organic Acid Content of Cosmetic Ingredients Produced by Plum Distillation Extract>

An embodiment of the present invention is to produce a distillation extract of plum by distilling the plum in distilled extraction method. The result of examining the organic acid content of the distilled extract is described with reference to [Table 2]. [Table 2] shows the organic acid content of the cosmetic raw material extracted when distilled plum.

After distillation extraction, the organic acid can only be detected in the distillation concentrate remaining in the pot in the distillation extractor. Oxalic acid, malic acid, and citric acid are higher in distilled concentrates of distilled plums, including seeds, than the seed removed in each treatment. At many 35 liters these component contents can increase.

When the seed is removed and distilled, the total amount of organic acid may be high in 25 l of the purified plum water and 35 l of the purified plum oil.

That is, when distilled extraction, distillation of blue plum and yellow plum containing seeds may increase the organic acid content, and distillation may be advantageous to increase the organic acid content of the distillation concentrate by distillation by adding more than 35 liters of purified water per 10 kg of plum during distillation extraction. have.

By organic acid content, citric acid content may be the highest, followed by malic acid content, followed by oxalic acid content. In addition, the contents of organic acids are increased in the immature fresh plums rather than the mature yellow plums, so the total organic acid content is the highest in the fresh plums, and as the plums mature, the total organic acid content may decrease.

The highest organic acid content by maturity and sample processing was the distilled concentrate distilled from the fresh water containing 35% of the purified water in 35 liters of purified water, followed by the total organic acid content of 1,793 (mg / 100g). The distillation concentrate distilled at 25 L of the charged amount was 1,311 (mg / 100g), and the fresh plum distillate concentrated after removing the seed distilled at 35 L of the purified water was increased in the order of 1,211 (mg / 100g).

In general, the method of increasing the organic acid content of the plum distillate concentrate may be best extracted by adding 35 liters of purified water when distilled extraction in 10 kg of plum containing seeds. In other words, when distilled by using plum, the sugar, salinity, etc. shows a similar tendency, so when distilling extract without removing the seeds of plum when producing cosmetic raw materials can increase the content of various components and improve the work efficiency It can be a good way.

Antioxidant of Cosmetic Ingredients Produced by Plum Distillation Extract

An embodiment of the present invention is to produce a distillation extract of plum by distilling the plum in distilled extraction method. The result of examining the antioxidant value of the distilled extract after distillation extraction is described with reference to [Table 3]. Table 3 shows the antioxidant properties of the cosmetic raw material extracted when the plum was distilled off.

The antioxidant value was higher in the distillation concentration remaining in the pot after distillation extraction, the highest in the fresh fruit room without extracting the fruit than the flesh from which the seed was removed, and showed the same tendency as the organic acid content change. .

Perfume, the most commonly used lotion or cosmetic ingredient, can be measured for antioxidant value. The amount of aromatic water of plum was 25 liters and 35 liters of distilled water, respectively, and the distillation and extraction showed anti-oxidation values of 0.030 (mg / ml) and 0.027 (mg / ml), respectively. The antioxidant content value is shown.

The antioxidant content of the aromatic water of the plum may be the highest, especially in fresh plums without seed removal. In the distillation of the plum, the antioxidant content was generally high in 25 liters of small amount of purified water input.These results were the same in fresh plum, yellow plum, and plum. The dilution rate of one active ingredient may be evaluated to increase the content of functional components of the distillate extract.

The problem of the present invention is to increase the content of the active ingredient of aroma water commonly used as a cosmetic raw material, and based on these results, it is possible to control the content of the functional ingredient according to the amount of purified water input when distilled extraction is applied to the development of cosmetic raw material production Can be.

The high antioxidant value among fragrance raw materials is an expensive raw material that is widely used for anti-aging and wrinkle improvement, and it is widely used as a high value-added fragrance material. Plum fragrance water developed through this research service has high antioxidant value which is hard to appear in distillate extract, and can be developed as a high value-added fragrance raw material.

<Scent Strength of Cosmetic Ingredients Produced by Plum Distillation Extract>

The degree of plum maturity and the fruit strength by fruit processing method will be described with reference to [Table 4]. [Table 4] shows the strength of the cosmetic raw material extracted with a steam distillation extractor.

All of the fresh plum, yellow plum, and plum blossoms were found to be almost the same or similar in the same sample, even if they were extracted by different fruit processing methods, and it could be proved that they were extracted from the same raw material, thereby verifying the extract. In this case, it can be used as a judgment data about the application of specific raw materials.

The fragrance intensity of the aromatic water distilled and extracted is higher than the embodiment extracted from the seed including the seed removed. In the same example, all the examples except the yellow plum with the seed removed showed high fragrance intensity at 35 L having a large amount of purified water input when distilled extraction.

Distilled concentrate is shown to have a high strength of the embodiment extracted from the seed, including the seed, in the same embodiment it can be seen that the fragrance is very strong because of a very high intensity of the embodiment with a small amount of purified water to be distilled extraction.

On the other hand, the yellow plum containing seeds, the highest fragrance strength 4814 (A.I.) at 25 liters of purified water input, the strong fragrance, on the contrary, the fragrance of fragrance water is 1443 (A.I.) may be the weakest fragrance.

When the fruit of ripe fruit, such as yellow plum, is extracted with 25 ℓ of small amount of purified water including seeds, the fragrance of fragrance water shows the lowest fragrance intensity in all the examples, and the distillate concentrate shows the highest fragrance intensity. .

The aroma intensity of the aroma water of the yellow plum with the seed removed was 25ℓ with less input of purified water, and the aroma intensity of the extracted side was 2439 (AI), while the fragrance intensity of the extracted distilled concentrate was the lowest as 1012 (AI). It shows that the fragrance strengths of the aromatic water and the distillate concentrate are opposite.

In general, the fresh plum and plum were distilled extract, the more the amount of purified water added, the fragrance intensity of the aromatic water increased, and the fragrance intensity of the distillate concentrate tended to decrease.

On the other hand, the yellow plums from which the seeds were removed have a high fragrance of fragrance water regardless of the distilled distilled water input amount, so that the fragrance water can be produced with strong fragrance. .

In other words, as the ripened fruit is crushed well and the amount of purified water is added, the water-soluble substance or fragrance component is better distilled when distilled extraction, so that the extraction is performed efficiently. Plum blossoms can be seen that the fragrance becomes stronger by increasing the fragrance strength of the embodiment with a large amount of purified water input.

<Anti-air Characteristics of Cosmetic Ingredients Produced by Plum Distillation Extract>

After extracting the fragrance component of the distilled extract of the distilled aromatic water after distillation extraction as a sample, the results of analyzing the fragrance component by mass spectrometry (GC / Mass) will be described with reference to [Table 5] to [Table 7]. Tables 5 and 6 show the fragrance components of plum hydrosol, which is a cosmetic raw material, and Table 7 shows the efficacy of the main fragrance components of plum hydrosol, a cosmetic raw material.

Representative major ingredients showing the unique aroma characteristics of aroma from the aromatic waters of ume and plum plum are Eugenol, Terpineol, Benzyl Benzoate, Decalin, and oleic acid. The fragrance characteristics and efficacy for these components are shown in [Table 7]. Most of these ingredients are ingredients that can be used for medical purposes such as daily necessities, ointments, creams, or fragrances that are frequently used in fragrances, cosmetics, spices, etc. The plum aroma is a raw material for cosmetics, household goods, food flavoring additives, spices, etc. It can be seen that it can be used as.

Eugenol, which can be used as a food, is a scent like a special spice and can be mainly used in daily necessities such as toothpaste, soap, detergent, and medicines such as ointments and creams, rather than cosmetics. Can be identified at

1-Tetracosanol (1-Tetracosanol) is a functional ingredient that lowers bad cholesterol (LDL) levels and raises good cholesterol (HDL) levels. It is an indicator that helps remove blood fat and cholesterol and improves blood circulation. It is a functional ingredient known as the main ingredient of policosanol, and it can be seen that it is a good raw material to be developed as a functional drink as it is confirmed in all other fragrance water except the fragrance water of the yellow plum.

Palmitoleic acid (9-Hexadecenoic acid, palmitoleic acid) is widely distributed in animal and plant systems and is contained in many fish oils such as fish oil and whale oil, but it is contained in small amounts in vegetable oil. It is known as an ingredient that helps prevent cardiovascular health and gastrointestinal health by preventing the body from accumulating and helping healthy weight management.

Palmitic acid (n-Hexadecanoic acid, Palmitic acid) is a skin-related effect that inhibits skin inflammation, and is known as an ingredient that helps healthy skin care by alleviating troubles and problem skin. Since it contains many flavors of these ingredients, it can be evaluated as being very suitable as a functional cosmetic raw material.

After distillation extraction, the representative flavor components and efficacy of the by-product heating concentrate will be described with reference to [Table 8] and [Table 8]. Table 8 shows the fragrance components of the plum heating concentrate as a cosmetic raw material. [Table 9] shows the efficacy and use of the main fragrance components of plum heating concentrate as a cosmetic raw material.

Acetophenone, 1,2,4-triazolo [4,3-a] pyrazine, benzyl alcohol, benzaldehyde, benzoic acid, oleic acid, n-Hexadecanoic acid And the like are identified as main ingredients.

Acetophenone is an aromatic substance found in the green tea and lemon of orange flower, 1,2,4-triazolo [4,3-a] pyrazine, and is often used to steer green tea, honey, and fruit aromas. . Benzyl alcohol, which is reminiscent of fresh fruit and soft floral scents of jasmine, gardenia, and lilac, sweet scent of almonds, and benzaldehyde, benzoic, benzoic, cherries. Benzoic acid and spicy oleic acid, which are used as food fragrances, can be detected and used as fragrances and food fragrances, and high quality fragrances that can be used in fragrances and perfumes are detected. It can be variously used as a raw material for flavoring additives and spices.

Vegetable phenol (Phenol) fragrance is the main ingredient found in the heating concentration of the yellow plum room containing seeds, and the phenolic polyphenols (polyphenols) have an antioxidant effect by removing the active oxygen (harmful oxygen) in our body. It protects DNA from damage by exposure to free radicals, protects cellular proteins and enzymes, and prevents various diseases. Along with anticancer activity, it is a useful ingredient known to prevent heart disease.

Oleic acid contained in plum heating concentrate was found to be a large amount of aromatic substance found in all heating concentrates of Cheongmaesil and Hwangmaesil. The main effect is a type of omega-9 fatty acid, which lowers the LDL level, which is the advantage of monounsaturated fatty acid. Increases the level of HDL cholesterol that protects the liver. It is known to be effective in preventing cardiovascular system diseases and aging, and oleic acid is also effective in strengthening the weakening of breast cancer drugs such as Herceptin. Its main use is as an emulsifier of soap, and it strengthens colon peristalsis movement to smooth the barrier, improving constipation and preventing colon cancer, and it is used as cosmetics, pharmaceutical additives, and fabric softeners.

n-Hexadecanoic acid is palmitic acid, which is the main ingredient identified in plum hydrosol, and it has been found to contain a large amount in plum heating concentrate, improves skin's moisturizing and penetrating ability. It has anti-atopic and staphylococcal inhibitory effect on the skin and is used as fatty acid, viscosity, and hardness increasing agent used in the saponification of cleansing foam, and it has direct use which shows the cleaning effect of soap and cleansing foam that cleans the skin. The produced heating concentrate can also be used in various ways as a functional cosmetic raw material.

<Aroma Characteristics and Efficacy of Distilled Plum Hydrosol>

Representative fragrance components and efficacy of the aromatic water of the plum produced after distillation extraction will be described with reference to [Table 10] and [Table 11]. Table 10 shows the fragrance components of plum hydrosol which is a cosmetic raw material. Table 11 shows the efficacy and use of the main fragrance ingredients of plum hydrosol, a cosmetic raw material.

Typical fragrance components for aromatic water of plum produced after distillation extraction are benzoic acid, acetic acid, benzyl alcohol, eugenol, phenol and benzoic acid benzyl. Benzoate), oleic acid (oleic acid), n-Hexadecanoic acid, etc. Most of the components found in the main plum fragrance can be identified as the main component.

In particular, Benzyl Benzoate, the main ingredient that accounts for more than 60% of plum blossom water, is the main ingredient of Balsam Peru, which is contained in many flowers of concrete and absolut, and is a fragrance mixed with weak balsam and floral scents. It is an important raw material as it is used a lot

Benzyl alcohol is reminiscent of the soft floral scent found in jasmine, gardenia, lilac, etc. It is widely used in various natural flavors and is a useful fragrance that is widely used commercially. It also contains benzoic acid and acetic acid. acid), Eugenol, and Benzyl Benzoate, which is a blend of peach flavors with a strong floral sweetness, can be found to be an excellent fragrance.

In addition, oleic acid and n-Hexadecanoic acid are effective for preventing cardiovascular disease and aging, and have anti-cancer effect and strong anti-oxidant anti-inflammatory effect. It has a good cleansing effect, and it is widely used in cosmetics, pharmaceutical additives, and fabric softeners. It can be confirmed as an excellent cosmetic raw material for skin by containing a large amount of plum in aromatic water and argan plum oil.

It can be confirmed that abundant phenol components, which are vegetable polyphenols, are contained in plum fragrance water and argan plum oil, and phenol component has antioxidant effect by removing active oxygen (harmful oxygen) to prevent skin aging. Exposure to free radicals has been reported to provide excellent protection against damaged DNA, cellular proteins and enzymes. In the embodiment of the present invention, even in the antioxidant measurement of these raw materials showed a high antioxidant content, the same result can be obtained, while the plum fragrance contains an elegant fragrance unique to the plum, while anti-aging, wrinkle improvement cosmetics with argan plum oil It can be used as a functional cosmetic raw material with high preservation and fragrance such as raw materials or perfume and lotion, and thus can be evaluated as a very good cosmetic raw material.

<Skin moisturizing effect of cosmetic ingredients>

In order to measure the skin moisturizing effect on the distilled extract, as a control, immediately after washing the skin, take a 0.5cm size with a cotton swab on the fore and axe, measure skin reactions over time for 6 hours at an interval of 1 hour. This will be described with reference to [Table 12] to [Table 14]. Table 12 shows the male skin moisturizing effect of each cosmetic raw material, Table 13 shows the female skin moisturizing effect of each cosmetic raw material. Table 14 shows the average growth rate for the skin moisturizing effect of men and women.

The best ingredients for skin moisturizing were fringed lavender aroma of 7.25 (AU), the highest rate of increase of 19.9%, followed by yellow plum aroma of 5.1 (AU) of 15.1%, followed by plum sap of 5.6 (AU). Increased 15%, fringed lavender essential oil to 5.45 (AU) 14.3%, fresh plum fragrance to 4.25 (AU) to 13.6%, argan plum oil to 4.35 (AU) to 12.3%, plum fragrance to 4.25 (AU) Most of the aromatic distillate extracts are highly moisturized, increasing by 10.9%.

Moisturizing effect by men and women showed higher moisturizing effect on the left and right side of the forehead than men, especially in plum sap, fresh plum aroma water, yellow plum aroma water, and fringed lavender oil, after moisturizing, 23.2% to 26.3% Shows a high rate of increase.

Most of the aromatic water of plum and plum, which are the main raw materials of the embodiment of the present invention, are excellent in moisturizing properties for both men and women, and especially women are more effective than men. In addition, plum aroma and sap of plum have good fragrance and excellent moisturizing effect, and also have anti-aging and anti-aging effects related to anti-wrinkle, which can be a very useful cosmetic ingredient for skin.

Therefore, when evaluating the development value of aromatic lotion by steam distillation extraction using plums and flowers, the results of the investigation of functional content of functional ingredients for cosmetic raw materials were reviewed. Among the fragrance components of aromatic water, In addition, it contains a lot of ingredients that are beneficial for health, has high antioxidant content and excellent moisturizing properties, so it can be used as a main ingredient or additive for cosmetics and daily necessities such as skin, mist, shampoo, body products, and textile rinses. The development adequacy can be evaluated as very high.

<Efficacy of skin elasticity of cosmetic raw materials>

Elasticity of each cosmetic raw material will be described with reference to [Table 15] to [Table 17]. Table 15 shows the elasticity efficacy of male skin by cosmetic raw materials. Table 16 shows the efficacy of the elasticity of women skin by cosmetic raw materials. [Table 17] shows the average increase rate according to the elasticity effect of the male and female skin.

For men, elasticity was increased in all cosmetic ingredients except right fringed fringed lavender fragrance, and in women, elasticity was increased in all cosmetic ingredients except for left sap plum sap.

As a result of measuring the efficacy of skin elasticity by cosmetic raw materials for men and women, the increase rate of fringed lavender essential oil was 6.0 to 10.6% compared to the untreated right after cleansing of jeon, and then the fringed lavender fragrance was 7.6 The percentage increased, but decreased -1.5% in the right night. The fresh plum aroma water showed an increase rate of 3.0% to 7.3% in the left and right forearms, followed by a plum sap of 3.5% to 5.8%. Aromas of yellow plum and plum showed an increase rate of 1.4% to 3.3%, indicating that distilled extracts of plum and plum have a firming effect on the skin of men.

In women's skin, all cosmetic ingredients increase the skin's elasticity, except for plum sap, which decreased the elasticity by -1.1%. The raw material with the greatest increase in elasticity of the skin is plum argan oil, showing 0.3% to 5.5% increase in the aroma of plum, 1.4% to 4.0% of the aroma of plum, and 2.9% to 3.9% of the aroma of plum and yellow plum. Although the rate of increase is higher, the elasticity growth rate of most cosmetic raw materials is lower than that of men.

The average increase in elasticity of cosmetic raw materials for both men and women was the highest with fringed lavender essential oil (5.8%), followed by fresh plums (4.2%), followed by fringes of 3.4% and yellow plums (3.2%). Was done. The elasticity of the argan oil and the argan plum oil is the lowest increase rate of 1.8% to 2.8%, indicating that the base oil argan oil has a low elasticity effect on the skin, and thus the elasticity of the argan plum oil extracted plum is inferior.

Efficacy of each cosmetic raw material for increasing skin elasticity shows high elasticity in the aromatic water of fresh plum, yellow plum and plum, and it can be seen that it can be used for anti-aging or wrinkle improvement when developing cosmetics. It can be seen that it can be usefully used as a high cosmetic raw material.

<Skin melanin (whitening) effect of cosmetic raw materials>

 The result of measuring melanin with respect to a distillate extract is demonstrated with reference to [Table 18]-[Table 20]. Table 18 shows the melanin inhibitory effect of male skin by cosmetic raw materials. Table 19 shows the melanin inhibitory effect of women's skin by cosmetic raw materials. Table 20 shows the average rate of increase for melanin inhibitory effect on the skin of men and women.

In males, the melanin-inhibiting effect in the left sap and right plum plum aromas was -7.8% and -1.4%, respectively, compared to the bare skin immediately after washing, and all of them showed a whitening effect only in the cosmetic raw materials of plum. All were ineffective in the cosmetic raw materials.

In the case of jeonjeonbak, the melanin inhibitory effect was reduced from -0.4 to -2.2% in Argan oil and fringed lavender oil and the essential oils of flower oil. All cosmetic ingredients except oil show melanin inhibitory effect of -1.0 to -6.7%, which may be whitening effect, and the difference of whitening effect on skin of left and right jeonjeonbak. The cosmetic ingredient that showed the highest whitening effect in the left jeonbak is the fragrance of fringed lavender and natural essential oils, showing a high reduction rate of -5.4% to -6.7%, which shows the best melanin inhibitory effect.

Plum aroma and fresh plum aroma also showed a high reduction rate of -5% and -4.1%, respectively, indicating that the whitening effect was good, and that plum plum and plum could be a cosmetic raw material with whitening effect.

The average increase rate according to the skin melanin suppression effect, which is the average of men and women, was the highest decrease of -2.7% in natural essential oil of fringed lavender, followed by the decrease of -1.4% in aromatic plum fragrance and -1.1% in plum sap. There is a greater melanin inhibitory effect than men, so there may be a difference in the efficacy of the skin on men and women.

Overall, the melanin inhibitory effect is the highest in the natural essential oil of fringed lavender, plum aroma and fresh plum aroma also shows a high melanin inhibitory effect and all of these cosmetic raw materials have a good whitening effect. In addition, it can be confirmed through the embodiment of the present invention that the plum and plum are not limited to the raw material of the processed food for food, but can be extended to the raw material of the cosmetic industry.

Therefore, the area of plum farms can be fostered as a cosmetic raw material industry using plum. On the other hand, not only the plums but also the cultivation of lavender together to improve the local landscape, promote the useful functionality of the plum and lavender skin together to secure local resources, and introduce the herb resources to the plum farmer's area It can contribute to the expansion and development of the cosmetic raw material industry.

<Effect of inhibiting skin erythema of cosmetic raw materials>

The erythema test showing inflammation relief or sedative effect is described with reference to [Table 21] to [Table 23]. Table 21 shows the erythema suppression efficacy of male skin by cosmetic raw materials. Table 22 shows the erythema suppression efficacy of women's skin by cosmetic raw materials. Table 23 shows the average rate of increase in erythema suppression efficacy of men and women skin.

In the erythema test showing inflammation relief or sedative effect, both males and females show partial erythema efficacy rather than distinct erythema efficacy in fresh plum fragrance and yellow plum fragrance.

Men's erythema suppression effect on the cosmetic raw material showed a high decrease rate of -2.71% to -8.69% in the left and right skin of the plum aroma, followed by -1.39% to -8.86% of the yellow plum and -3.90 It shows the effect of erythema suppression in the order of% to -4.38%, and the effect of erythema suppression is excellent in the order of plum fragrance> yellow plum fragrance> fringed fragrance.

On the other hand, the erythema inhibitory effect is weak, but the argan plum oil is reduced from -0.27% to -2.14%, males appear to have the most effective erythema suppression effect.

Efficacy of erythema suppression in women is the most excellent in the effect of fringed lavender fragrance water -4.01% to -8.58% in the skin of left and right forearms.

Plum sap shows a high reduction rate of -5.4% to -6.57%, and both fringed lavender fragrant water and plum sap have distinct erythema suppressing effect.

Cosmetic ingredients that showed erythema suppression effect on women's right chestnut skin were reduced by -4.67% and -3.96% by fresh plum oil and argan plum oil, respectively. Natural oils of fringed and fringed oil showed a weak reduction rate of -0.34% and -0.94%, respectively. In the whole cosmetic raw materials, women have a clear effect of erythema in fringed lavender and plum sap.

The average increase rate according to the effect of skin erythema suppression of male and female was the lowest with fringed lavender fragrance -5.2%, followed by yellow plum aroma -2.1%, plum sap -0.6%, plum aroma -0.55%. The most effective cosmetic ingredients are listed in order of fringed lavender fragrance> yellow plum fragrance> plum sap> plum fragrance.

In general, fringed lavender fragrance, yellow plum fragrance, plum sap, plum fragrance fragrance in the skin of both men and women with cosmetic raw materials showed erythema suppression effect, and most cosmetic raw materials were found to have excellent inflammation-relieving effects or general effects. It may be valuable as a cosmetic ingredient as an emollient.

<Measurement of skin acidity (pH) of cosmetic raw materials>

The acidity of skin by cosmetic raw materials will be described with reference to [Table 24] to [Table 26]. Table 24 shows the acidity of male skin by cosmetic raw material. Table 25 shows the acidity (pH) of female skin by cosmetic raw material. Table 26 shows the average increase rate according to the acidity (pH) of the skin of men and women.

In order to measure the acidity of skin by cosmetic raw materials, the acidity immediately after cleansing, which is untreated by both men and women before measurement, is in the range of pH 4.16 to pH 4.48 in men, and the acidity of normal skin in humans is lower than in the range of pH 4.5 to pH 5.5. . Women range from pH 4.83 to pH 5.33 and fall within the normal range of skin acidity of humans to show optimal skin conditions, which can be assessed by women using more cosmetics than men.

Both men and women measured skin acidity every hour for 6 hours after applying it to the left and right forearms by cosmetic ingredients, and men showed an increase and decrease by an average of -4.82% to 3.18% for each raw material after application, immediately after washing, before control. In women, the pH was decreased from -10.22 to -2.33% after application of all raw materials compared to just after washing, and there was a difference in skin acidity after application of raw materials between men and women. In women, the acidity just after washing the face is lower than that of the cosmetics because the acidity is higher than that of the cosmetics, and in men, the acidity of the skin is higher than that of the cosmetics. It can be understood as a difference in skin care.

Changes in skin acidity by cosmetic raw materials showed that the acidity decreased from -1.71% to -4.82% in men's aroma and sap, and sap in sap and plum, and -1.88% to-. The decrease is as high as 4.82%. In contrast, the base oils of argan, argan plum oil, fringed lavender, fragrance water, and natural essential oils increased the skin acidity from 0.47% to 3.18% after application, rather than immediately after washing. Can be.

The acidity increase / decrease rate of each cosmetic raw material of both sexes decreases from -2.65% to -5.10% after application, rather than immediately after washing. By raw material, the aroma and sap of plum blossoms decreased most to an average of -5.1%, and then the plum water of yellow plums decreased to -4.08% in order.

The optimal condition of skin is to maintain proper acidity and moisturizing may be the first to inhibit skin aging. The acidity of the aromatic waters of the embodiment of the present invention, such as blue plum, yellow plum, plum, is slightly lower than normal skin acidity in the range of about pH 3.3 to pH 4.5, but can be adjusted to an acidity suitable for skin when distilled and mostly moisturizing by raw material This excellent and increased elasticity, the inhibitory effect of melanin and erythema are evenly represented by each raw material can be evaluated as very suitable as a cosmetic raw material, it can be an excellent cosmetic material that combines the functionality and efficacy of the skin.

<Skin Stability Study of Cosmetic Ingredients>

Skin stability by cosmetic raw materials will be described with reference to [Table 27]. Table 27 shows the stability evaluation for each cosmetic raw material.

As a result of the stability test for 9 hours or more, the most of the steam distilled extracted raw materials showed no allergy, skin irritation, inflammation, etc., and thus the safety of cosmetics can be evaluated as good.

<The first formulation method of cosmetic raw materials with enhanced anti-inflammatory>

Step-by-step description of the first formulation method of anti-inflammatory enhanced cosmetic raw materials.

First step: The first step is to prepare a turmeric extract, a mixture of 2% turmeric essential oil and 98% turmeric distillate concentrate.

Second step: The second step is to determine the appropriate concentration of functional raw material addition amount. Functional raw materials may include turmeric extract, secondary hyaluronic acid and ceramide.

Turmeric extract may be added in an amount of 0.2%, 0.5%, 1%, 10%, 20% and 30%, respectively, based on the weight percentage of the mixed cosmetic raw material.

Secondary hyaluronic acid may be added in amounts of 0%, 0.01%, 3% and 5%, respectively, relative to the weight percent of the mixed cosmetic raw material.

Tertiary ceramides may be added in amounts of 0%, 0.01%, 1%, 2% and 3%, respectively, relative to the weight percent of the mixed cosmetic raw material.

Step 3: In step 3, a suitable ratio can be selected when applying the cosmetic raw material as a finished product. That is, a specific addition amount can be selected from the addition amount of the functional raw material described in the second step.

Looking at the first formulation, it can be seen that all of the turmeric concentrate added 0.5% to 30% by weight of turmeric extract, the precipitate is confirmed, the turmeric concentrate content should be further reduced.

Turmeric concentrate added 0.2% by weight of turmeric extract in the weight ratio is not formed because it is most preferable to add less than 0.2% turmeric concentrate as a functional raw material.

On the other hand, by adding the strong extracts to the lotion by the content in the lotion process step to find the time when the oil component layer and the water layer is not separated from each other well emulsified and described with reference to [Table 28]. Table 28 shows the degree of emulsification for the preparation of cosmetic raw material primary formulations for the amount of turmeric extract added.

When turmeric extract is added up to 0.5% to 30%, sediment is confirmed in all of the lotion, so that the proper concentration may be inadequate, but turmeric concentrate containing 0.2% turmeric extract may not be emulsified and may be set to an appropriate amount of functional concentrate.

Therefore, the appropriate amount of turmeric extract, which is a primary functional additive, may be preferably added in an amount of 0.2% based on the weight% of the perfumed water formulation.

<Second Formulation Method Added Second Functional Ingredients for Strengthening Moisturizing and Aging Prevention>

First, an appropriate amount of sodium hyaluronate (functional hyaluronate) is selected. The selection of the amount of sodium hyaluronate added is described below.

Sodium hyaluronate contains a large amount of water between the collagen fibers present in the reticular structure in the dermis to give elasticity to the lattice-like collagen layer.This prevents wrinkles caused by the collapse of the collagen layer, thereby creating blood vessels in the epidermis. Instead, it is a functional ingredient that acts as a metabolism (prevents keratin / atopy) such as oxygen and nutrient supply and prevents aging by maintaining sufficient moisture in the skin. Sodium hyaluronate is mainly used in cosmetics, serums, lotions, cosmetic packs, shampoos, etc. It is used as an anti-wrinkle and moisturizer for skin.

In the embodiment of the present invention can be used to increase the efficacy of elasticity and moisturizing, wrinkle prevention in perfumed water by reinforcing sodium hyaluronate excellent in elasticity, wrinkle prevention and moisturizing enhancement effect.

As a result of the addition of sodium hyaluronate to the example in which the turmeric extract, based on the perfumed water formulation, was added in an amount of 0.5% to 30%, all the precipitates were confirmed, and the color was dark, which may be inappropriate for the cosmetic preparation. On the other hand, addition of 0.02% of turmeric extract and 0.5% of sodium hyaluronate does not cause precipitation and is considered suitable, and this component combination can be selected as a basic material for the development of the second cosmetic formulation.

<Selection of the appropriate amount of hyaluronic acid addition to the secondary cosmetic base material>

Based on the cosmetic raw material selected as the base material, sodium hyaluronate (Na Hyaluronate) is added for each content to examine the suitability of the formulation through a feeling test, which will be described with reference to [Table 29]. Table 29 shows the degree of stabilization of the secondary perfumed water base formulation with sodium hyaluronate added.

As shown in Table 29, the molecular weight of Sodium Hyaluronate used in A-1 to A-2 (3% to 5% Na Hyaluronate) to which 3% to 5% sodium hyaluronate was added in the second formulation was 10,000. The higher the sodium hyaluronate content of about 18,000 to 18,000, the more slippery the skin is, so it may be excluded as it is not suitable as a lotion by interfering with the skin absorption rate.

As a result of applying the formulation containing 0.5% sodium hyaluronate of A-3, which is the remaining example excluded, to the skin and examining the absorbency and application of the skin, the absorbency of the skin is good without being slippery and the amount of sodium hyaluronate added is 0.5 Can be selected in%.

<Third formulation fragrance added with HACE-200, a functional ingredient>

An embodiment of the formulation invention will be described with reference to Table 30 and FIG. 1 by adding HACE-200, a functional substance containing ceramide having high formulation stability, by content, based on Example A-3 of Table 29. Table 30 shows the degree of stabilization of the third formulation formulation by the amount of HACE-200 added to the formulation of the second base material. 1 is a drawing substitute photograph for confirming the precipitate in the cosmetic raw material using a plum distillation extract according to an embodiment of the present invention.

The higher the HACE-200 content, the heavier the feeling and the slighter the suspension, resulting in a transparent formulation of the final G-4 embodiment can be selected as the optimal embodiment.

The HACE-200 can be known by Korean Patent Registration No. 10-1175193 "composition for skin diseases comprising a ceramide-containing hyaluronic acid complex", and more specifically Water, Glycerin, Butylene Glycol, Acrylates / Stearyl Methacrylate Copolymer , Tremella Fuciformis Extract, Phenoxyethanol, Hyaluronic Acid, Xanthan Gum, Ethylhexylglycerin, and Ceramide 3 (0.025%).

<Evaluation of Skin Feeling for the Third Formulation Perfume G-4>

For the evaluation of skin feel of the third formulation, perfume water, 0.01% of hyaluronic acid sodium and 0.1% of HACE-200 were added as functional substances in the first selected basic material formulation, and the aqueous layer was prepared with pure purified water. It is called A formulation. A formulations are shown in Table 31. Table 31 shows the preparation stability of the third formulation according to the amount of HACE-200 added to the secondary base material.

The formulation A shown in [Table 31] was treated untreated, and 100% pure plum hydrosol was added instead of distilled water of the aqueous phase in the embodiment of the present invention, and 35 wt% of turmeric extract and 0.5 hyaluronic sodium as a functional raw material. A formulation prepared by adding 0.5% by weight and 0.5% by weight of HACE-200, respectively, will be used as a G-4 example to examine skin feel. Table 32 shows the usability evaluation of cosmetic formulations added with plum hydrosol and functional substances.

In the embodiment of Formulation A described in Table 32, the use of perfume may be necessary to mush the smell of the formulation due to the slight mixing of the odor, such as vinyl, which is a raw material of the product. In addition, the formulation A embodiment shows that there is no significant difference from the general cosmetics in the skin feeling evaluation, and the user may hardly recognize that the natural raw material is used.

Example G-4 described in Table 32 may be prepared by adding a distillation extract of a mixture of natural essential oil and turmeric concentrate of turmeric and adding plum hydrosol instead of distilled water of the aqueous phase.

The fragrance water of the G-4 embodiment has a good response to the image incidence using natural ingredients because the herbal flavor mixed with natural fragrance is strong, and it is confirmed through the examination that the aroma treatment effect is obtained by obtaining the evaluation that the herbal flavor gives comfort of mind and body. Can be. However, some young people and males may also have a reaction to dislike herbal, so there are differences in various palatability according to aroma.

In the evaluation of the feeling of use of the perfume of G-4 of Example G-4, which is an embodiment of the present invention, it can be seen that the skin is softly absorbed without being oily and absorbed without moisture, thereby increasing the skin flexibility and elasticity, and having excellent contrast with no treatment.

On the other hand, in the examples and claims of the present invention, the numerical values presented may be modified in a small amount when reproduced, and more specifically, in the examples of the present invention, the plum raw and the purified water presented. , The turmeric extract, the hyaluronic acid sodium and the HACE-200 can be applied in the error range of 3% or less to 3% or more with respect to the numerical values presented.

While the embodiments of the present invention have been described above, those skilled in the art will appreciate that the present invention can be implemented in other specific forms without changing the technical spirit or essential features thereof.

Therefore, the embodiments described above are to be understood as illustrative and not restrictive in all respects, and the scope of the present invention is represented by the following claims, which are derived from the meaning and scope of the claims and their equivalent concepts. All changes or modifications should be construed as being included in the scope of the present invention.

Cosmetic raw material using a plum distillation extract according to an embodiment of the present invention can be used to prepare an additional product using plum.

Claims (5)

A first step of extracting a plum distillate by adding fresh fruit and purified water including seeds to a distillation extractor;
A second step of producing a plum distillate concentrate in an inner pot of the distillation extractor when the plum distillate is cooled to produce 30 l of plum hydrosol; And
And diluting the acidity of the plum distillation concentrate;
In the first step, the mixing ratio of the fresh raw plum and purified water is 10 kg: 35 L
Cosmetic raw materials using plum distillation extract containing.
The method of claim 1,
0.2% by weight of turmeric extract in the plum distillate concentrate
Cosmetic raw materials using plum distillation extract containing.
The method of claim 2,
Added by adding 0.5% by weight of hyaluronic sodium
Cosmetic raw materials using plum distillation extract containing.
The method of claim 3,
0.5% by weight of HACE-200 is added and mixed.
Cosmetic raw materials using plum distillation extract containing.
The method of claim 4, wherein
The plum raw fruit, the purified water, the turmeric extract, the hyaluronic acid sodium and the HACE-200 is applied to an error range of 3% or less to 3% or more with respect to the numerical values given.
Cosmetic raw materials using plum distillation extract containing.

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